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Separation of esbiothrin and D-acetylene C permethrin in electric-mosquito coils by gas chromatography

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Abstract

A simple and sensitive gas chromatography method for the simultaneous determination of esbiothrin and D-acetylene C permethrin in electric-mosquito coils using palmitic acid isopropyl as an internal standard was developed. The electric-mosquito coil samples were extracted with petroleum ether (60–90 °C) and then centrifuged at 2,000 r/min for 2.0 min. The supernatant liquids were collected into a glass bottle and 2.0 µL of it was injected into the gas chromatograph. The results showed that the means recoveries of esbiothrin and acetylene c permethrin ranged from 100.2% to 99.8%. The relative standard deviation (n=10) of allylic permethrin and acetylene C permethrin was 0.44% and 0.26%, respectively. This method is a viable alternative tool to the existing gas chromatography methods for analyzing the content of allylic permethrin and D-acetylene C permethrin in electric-mosquito coil samples.

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Authors and Affiliations

  1. Department of Chemical Engineering, Inha University, 253 Yonghyun-dong, Nam-gu, Incheon, 402-751, Korea

    Junyu Liu & Kyung Ho Row

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  1. Junyu Liu
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  2. Kyung Ho Row
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Correspondence to Kyung Ho Row.

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Liu, J., Row, K.H. Separation of esbiothrin and D-acetylene C permethrin in electric-mosquito coils by gas chromatography. Korean J. Chem. Eng. 27, 228–230 (2010). https://doi.org/10.1007/s11814-009-0288-2

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  • DOI: https://doi.org/10.1007/s11814-009-0288-2

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