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Microstructure and mechanical properties of as-cast Mg-8Sn-1Al-1Zn-xNi alloys

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Abstract

Mg-8Sn-1Al-1Zn-xNi (x=0.5%, 1.0%, 1.5%, 2.0%, mass fraction) alloys were designed and prepared. The microstructures and the mechanical properties were studied by using optical microscope, scanning electronic microscope, energy dispersive X-ray spectroscope, X-ray diffraction and a standard universal testing machine. The results show that the microstructure of Ni-containing alloys consist of α-Mg, Mg2Sn, β-Mg-Ni-Al and γ-AlNi phases. No β-Mg-Ni-Al phase was observed in TAZ811-2.0Ni alloy due to its 1:1 atomic ratio of Ni/Al. The addition of Ni refines the α-Mg dendrites and suppresses the formation of coarse Mg2Sn phase. The tensile properties results show that the TAZ811-0.5Ni alloy presented the best mechanical properties, which is due to the rod-like β-Mg-Ni-Al phase, refined α-Mg dendrites and Mg2Sn phase, as well as γ-AlNi phase. The tensile fracture mechanism transits from cleavage to quasi-cleavage fracture with the increasing Ni addition.

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References

  1. CHENG W L, PARK S S, YOU B S, KOO B H. Microstructure and mechanical properties of binary Mg-Sn alloys subjected to indirect extrusion [J]. Materials Science and Engineering: A, 2010, 527(18/19): 4650–4653.

    Article  Google Scholar 

  2. KOZLOV A, OHNO M, ARROYAVE R, LIU Z K. SCHMID-FETZER R, Phase equilibria, thermodynamics and solidification microstructures of Mg-Sn-Ca alloys, Part 1: Experimental investigation and thermodynamic modeling of the ternary Mg-Sn-Ca system [J]. Intermetallics, 2008, 16: 299–315.

    Article  Google Scholar 

  3. SON H T, LEE J B, JEONG H G, KONNO T J. Effects of Al and Zn additions on mechanical properties and precipitation behaviors of Mg-Sn alloy system [J]. Materials Letters 2011, 65: 1966–1969.

    Article  Google Scholar 

  4. LIU H, CHEN Y, TANG Y, HUANG D, NIU G. The microstructure and mechanical properties of permanent-mould cast Mg-5 wt.% Sn-(0-2.6) wt.% Di alloys [J]. Materials Science and Engineering: A, 2006, 437: 348–55.

    Article  Google Scholar 

  5. NAYYERI G, MAHMUDI R. The microstructure and impression creep behavior of cast, Mg-5Sn-xCa alloys [J]. Materials Science and Engineering: A, 2010, 527: 2087–2098.

    Article  Google Scholar 

  6. HORT N, HUANG Y, LEIL T A, MAIER P, KAINER K U. Microstructural investigations of the Mg-Sn-xCa system [J]. Adv Eng Mater, 2006, 8: 359–364.

    Article  Google Scholar 

  7. KIM D H, LEE J Y, LIM H K, KYEONG J S, KIM W T, KIM D H. The effect of microstructure evolution on the elevated temperature mechanical properties in Mg-Sn-Ca system [J]. Mater Trans, 2008, 49: 2405–24013.

    Article  Google Scholar 

  8. LEIL T A, HUANG Y, DIERING H, HORT N, KAINER K U, BURSIK J. Effect of heat treatment on the microstructure and creep behavior of Mg-Sn-Ca alloys [J]. Material Science Forum, 2007, 546-549: 69–72.

    Article  Google Scholar 

  9. HUANG X F, ZHANG W Z. Microstructure and mechanical properties of conventional cast and rheocast Mg-Sn based alloys [J]. Materials Science and Engineering: A, 2012, 552: 211–221.

    Article  Google Scholar 

  10. PODDAR P, SAHOO K L. Effects of cooling rate and pressure on microstructure and mechanical properties of sub-rapidly solidified Mg-Zn-Sn-Al-Ca alloy [J]. Materials and Design, 2012, 545: 103–110.

    Google Scholar 

  11. CHEN J H, WEI J Y, YAN H G, SU B, PAN X Q. Creep behaviour of Mg-8% Sn and Mg-8% Sn-3% Al-1% Si alloys [J]. Materials Science and Engineering: A, 2012, 545: 103–110.

    Article  Google Scholar 

  12. PODDAR P, SAHOO K L, MUKHERJEE S, RAY A K. Microstructure evolution and properties of Mg-3Sn-1Mn (wt%) alloy strip processed by semisolid rheo-rolling [J]. Journal of Materials Processing Technology, 2012, 212: 1430–1436.

    Article  Google Scholar 

  13. NAYYERI G, MAHMUDI R. The microstructure and impression creep behavior of cast, Mg-5Sn-xCa alloys [J]. Materials Science and Engineering: A, 2010, 527: 2087–98.

    Article  Google Scholar 

  14. HUANG X F, ZHANG W Z. Improved age-hardening behavior of Mg-Sn-Mn alloy by addition of Ag and Zn [J]. Materials Science and Engineering: A, 2012, 556: 891–905.

    Article  Google Scholar 

  15. KANG D H, PARK S S, OH Y S, KIM N J. Effect of nano-particles on the creep resistance of Mg-Sn based alloys [J]. Materials Science and Engineering: A, 2007, 449-451: 318–21.

    Article  Google Scholar 

  16. CHEN D, REN Y P, GUO Y, PEI W L, ZHAO H D, QIN G W. Microstructures and tensile properties of as-extruded Mg-Sn binary alloys [J]. Trans. Nonferrous Met. Soc, China 2010, 20: 1321–1325.

    Article  Google Scholar 

  17. CHENGG W L, KIM H S, YOU B S, KOO B H. Strength and ductility of novel Mg-8Sn-1Al-1Zn alloys extruded at different speeds [J]. Materials Letters, 2011, 65: 1525–1527.

    Article  Google Scholar 

  18. PARK S S, KIM Y J, CHENG W L, KIM Y M, YOU B S. Tensile properties of extruded Mg-8Sn-1Zn alloys subjected to different heat treatments [J]. Philosophical Magazine Letters, 2011, 91: 37–44.

    Article  Google Scholar 

  19. LEE S G, JEON J J, PARK K C, PARK Y H, PARK I M. The effects of alloying elements on microstructure and properties of gravity casting Mg-Sn-Al-Si alloy [J]. Materials Chemistry and Physics, 2011, 128: 208–213.

    Article  Google Scholar 

  20. TANG W N, PARK S S, YOU B S. Effect of the Zn content on the microstructure and mechanical properties of indirect-extruded Mg-5Sn-xZn alloys [J]. Materials and Design, 2011, 32: 3537–3543.

    Article  Google Scholar 

  21. PARK S S, TANG W N, YOU B S. Microstructure and mechanical properties of an indirect-extruded Mg-8Sn-1Al-1Zn alloy [J]. Materials Letters 2010, 64: 31–34.

    Article  Google Scholar 

  22. KIM Y K, SOHN S W, KIM D H, KIM W T, KIM D H. Role of icosahedral phase in enhancing the strength of Mg-Sn-Zn-Al alloy [J]. Journal of Alloys and Compounds, 2013, 549: 46–50.

    Article  Google Scholar 

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Correspondence to Zhong-ping Que  (阙仲萍).

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Foundation item: Project supported by the Shanxi Selective Funds for Returned Scholars, China; Project(2013021013-4) supported by the Shanxi Province Science Foundation for Youths China; Projects(2012L053, 2012L003) supported by the Taiyuan University of Technology Funds for Young Scientists, China; Project(2014021017-2) supported by the Natural Science Foundation for Young Scientists for Shanxi Province, China

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Que, Zp., Ma, T., Wang, J. et al. Microstructure and mechanical properties of as-cast Mg-8Sn-1Al-1Zn-xNi alloys. J. Cent. South Univ. 21, 3426–3433 (2014). https://doi.org/10.1007/s11771-014-2318-4

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  • DOI: https://doi.org/10.1007/s11771-014-2318-4

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