Skip to main content
Log in

Microstructure, texture and tensile properties of Mg-10Sn alloys extruded in different conditions

  • Published:
Journal of Central South University Aims and scope Submit manuscript

Abstract

Indirect extrusion of Mg-10%Sn (mass fraction) alloys was performed at three different working temperatures. The effect of working temperature on the microstructure, texture and tensile properties of the extruded alloys was investigated by optical microscope (OM), scanning electronic microscope (SEM), X-ray diffraction (XRD) and a standard universal testing machine. Grain size, area fraction of second phase particles and texture of the alloys are found to be significantly influenced by working temperature. The grain size refinement is greatly dependent on processing conditions with the low working temperature being the most effective. While the high working temperature results in a coarser grain size and a stronger fiber texture and the reason for this phenomenon was examined in terms of second phase particle, grain type and dynamic recrystallization mechanism. Tested in the different conditions, the tensile strengths of the Mg-10Sn alloys extruded at the high working temperature are remarkably better than those of the other studied alloys. This significant improvement in tensile properties is mainly due to the particle strengthening and texture strengthening resulted from the more and finer primary dispersed particles and stronger texture, respectively.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Similar content being viewed by others

References

  1. UEMATSU Y, TOKAJI K, KAMAKURA M, UCHIDA K, SHIBATA H, BEKKU N. Effect of extrusion conditions on grain refinement and fatigue behavior in magnesium alloys [J]. Mater Sci Eng A, 2006, 434: 131–140.

    Article  Google Scholar 

  2. MENDIS C L, OHISHI K, KAWAMURA Y, HONMA T, KAMADO S, HONO K. Precipitation-hardenable Mg-2.4Zn-0.1Ag-0.1Ca-0.16Zr (at.%) wrought magnesium alloy [J]. Acta Mater, 2009, 57: 749–760.

    Article  Google Scholar 

  3. YAMASHITA A, HORITA A, LANGDON T G. Improving the mechanical properties of magnesium and a magnesium alloy through severe plastic deformation [J]. Mater Sci Eng A, 2001, 300: 142–147.

    Article  Google Scholar 

  4. MUKI T, HIGDSHI K. Ductility enhancement of ultra fine-grained aluminum under dynamic loading [J]. Scripta Mater, 2001, 44: 1493–1496.

    Article  Google Scholar 

  5. KIM H K LEE Y I CHUNG C S. Fatigue properties of a fine-grained magnesium alloy produced by equal channel angular pressing [J]. Scripta Mater, 2005, 52: 473–477.

    Article  Google Scholar 

  6. SASAKI T T YAMAMOTO K, HONMA T, KAMADO S, HONO K. A high-strength Mg-Sn-Zn-Al alloy extruded at low temperature [J]. Scripta Mater, 2008, 59: 1111–1114.

    Article  Google Scholar 

  7. PARK S S TANG W N YOU B S. Microstructure and mechanical properties of an indirect-extruded Mg-8Sn-1Al-1Zn alloy [J]. Mater Letters, 2010, 64: 31–34.

    Article  Google Scholar 

  8. CHENG W L PARK S S YOU B S KOO B H. Microstructure and mechanical properties of binary Mg-Sn alloys subjected to indirect extrusion [J]. Mater Sci Eng A, 2010, 527: 4250–4253.

    Article  Google Scholar 

  9. KANG D H PARK S S KIM N J. Development of creep resistant die cast Mg-Sn-Al-Si alloy [J]. Mater Sci Eng A, 2005, 413–414: 555–560.

    Google Scholar 

  10. MENDIS C L BETTLES C J GIBSON M A HUTCHINSON C R. An enhanced age hardening response in Mg-Sn based alloys containing Zn [J]. Mater Sci Eng A, 2006, 435/436: 163–171.

    Article  Google Scholar 

  11. LIU H, CHEN Y, TANG Y, HUANG D, NIU G. The microstructure and mechanical properties of permanent-mould cast Mg-5wt%Sn-(0–2.6)wt%Di alloys [J]. Mater Sci Eng A, 2006, 437: 348–355.

    Article  Google Scholar 

  12. PARK S S YOU B S YOON D J. Effect of the extrusion conditions on the texture and mechanical properties of indirect-extruded Mg-3Al-1Zn alloy [J]. J Mater Processing Tech, 2009, 209: 5940–5943.

    Article  Google Scholar 

  13. SHAHZAD M, WAGNER L. Influence of extrusion parameters on microstructure and texture developments, and their effects on mechanical properties of the magnesium alloy AZ80 [J]. Mater Sci Eng A, 2009, 506: 141–147.

    Article  Google Scholar 

  14. AZEEM M A TEWARI A, MISHRA S, GOLLAPUDI S, RAMAMURTY U. Development of novel grain morphology during hot extrusion of magnesium AZ21 alloy [J]. Acta Mater, 2010, 58: 1495–1502.

    Article  Google Scholar 

  15. BARNETT M R SULLIVAN A, STANFORD N, BEER A. Texture selection mechanisms in uniaxially extruded magnesium alloys [J]. Scripta Mater, 2010, 63: 721–724.

    Article  Google Scholar 

  16. BALL E A PRANGNELL P B. Tensile-compressive yield asymmetries in high strength wrought magnesium alloys [J]. Scripta Mater, 1994, 31: 111–116.

    Article  Google Scholar 

  17. NIE J F. Effects of precipitate shape and orientation on dispersion strengthening in magnesium alloys [J]. Scripta Mater, 2003, 48: 1009–1015.

    Article  Google Scholar 

  18. AL-SAMMAN T, GOTTSTEIN G. Dynamic recrystallization during high temperature deformation of magnesium [J]. Materials Science and Engineering A, 2008, 490: 411–420.

    Article  Google Scholar 

  19. LIU C M LIU Z J ZHU X R ZHOU H T. Research and development progress of dynamic recrystallization in pure magnesium and its alloys [J]. The Chinese Journal of Nonferrous Metals, 2006, 16: 1–12. (in Chinese)

    Article  Google Scholar 

  20. CHANG L L WANG Y N ZHAO X, HUANG J C. Microstructure and mechanical properties in an AZ31 magnesium alloy sheet fabricated by asymmetric hot extrusion [J]. Mater Sci Eng A, 2008, 496: 512–516.

    Article  Google Scholar 

  21. YUAN W, PANIGRAHI S K SU J Q MISHRA R S. Influence of grain size and texture on Hall-Petch relationship for a magnesium alloy [J]. Scripta Materialia, 2011, 65: 994–997.

    Article  Google Scholar 

  22. YUAN G Y SUN Y S DING W J. Effect of Sb addition on the microstructure and mechanical properties of AZ91 magnesium alloy [J]. Scripta Materialia, 2000, 43(11): 1009–1013.

    Article  Google Scholar 

Download references

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to Zhong-ping Que  (阙仲萍).

Additional information

Foundation item: Project(2012R1A1A1012802) supported by the National Research Foundation of Korea Funded by the Ministry of Education, Science and Technology; Project(2013021013-4) supported by Shanxi Province Science Foundation for Youths, China; Project(2012L003) supported by Advanced Programs of Department of Human Resources and Social Security of Shanxi Province for Returned Scholars, China; Project supported by Foundation for Young Scholars of Taiyuan University of Technology, China

Rights and permissions

Reprints and permissions

About this article

Cite this article

Cheng, Wl., Li, Jw., Que, Zp. et al. Microstructure, texture and tensile properties of Mg-10Sn alloys extruded in different conditions. J. Cent. South Univ. 20, 1786–1791 (2013). https://doi.org/10.1007/s11771-013-1673-x

Download citation

  • Received:

  • Accepted:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s11771-013-1673-x

Key words

Navigation