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Chemical Papers

, Volume 71, Issue 6, pp 1031–1035 | Cite as

Preparation of manganese oxide nanoparticles by thermal decomposition of nanostructured manganese carbonate

  • Jan PincEmail author
  • Ondřej Jankovský
  • Vilém Bartůněk
Original Paper

Abstract

MnO and Mn2O3 nanoparticles were prepared in air and argon atmosphere by thermal decomposition of nanocrystalline manganese carbonate synthesized by reaction of manganese(II) nitrate with glycerol. Samples were characterized using transmission electron microscopy, simultaneous thermal analysis and X-ray diffraction analysis. Average sizes of prepared nanoparticles were calculated from XRD patterns using Scherrer equation. Also, the conditions for decomposition of manganese carbonate were optimized to obtain optimal nanoparticle sizes. Due to suitable sizes of prepared nanoparticles and the initial material, this method can be used in a wide range of industrial applications.

Keywords

Nanoparticles Manganese oxides Thermal decomposition Manganese carbonate 

Notes

Acknowledgements

This work was supported by Czech Science Foundation (No. 15-02843S).

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Copyright information

© Institute of Chemistry, Slovak Academy of Sciences 2016

Authors and Affiliations

  • Jan Pinc
    • 1
    • 2
    Email author
  • Ondřej Jankovský
    • 1
  • Vilém Bartůněk
    • 1
  1. 1.Department of Inorganic Chemistry, Faculty of Chemical TechnologyUniversity of Chemistry and Technology Prague 6Czech Republic
  2. 2.Department of Metallic Materials and Corrosion Engineering, Faculty of Chemical TechnologyUniversity of Chemistry and Technology, PraguePrague 6Czech Republic

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