Journal of Food Measurement and Characterization

, Volume 11, Issue 4, pp 1559–1568 | Cite as

Assessment of antioxidant properties, instrumental and sensory aroma profile of red and white Karkade/Roselle (Hibiscus sabdariffa L.)

  • Haroon Elrasheid Tahir
  • Zou XiaoboEmail author
  • Abdalbasit Adam Mariod
  • Gustav Komla Mahunu
  • Mohammed A. Y. Abdualrahman
  • William Tchabo
Original Paper


The antioxidant properties of the water extract of Hibiscus sabdariffa L. as well as their aroma profile were investigated. The samples analyzed were three red (Al-Rahad, Al-Fashir, Al-Gezira) and one white varieties. Total phenolic content, total flavonoid content, total anthocyanin content, ferric reducing antioxidant power and radical scavenging activity (RSA %) were measured spectrophotometrically. The red varieties of Karkade showed better overall antioxidant properties and aroma profile compared to the white variety. Conversely, the white H. sabdariffa might also be used in antioxidants applications, as its extract exhibited the highest RSA % compared to other varieties. Nineteen volatile compounds were detected in the H. sabdariffa extracts, including aldehydes, alcohols, ketones, esters and phenol. Partial least squares regression (PLSR) was applied to determine the relationship between sensory descriptors and instrumental data. PLSR result showed a good relationship between sensory analysis and instrumental data (t1 and t2 = 94.63%). This indicated that gas chromatography-mass spectrometry (GC/MS) can be used as suitable tools to predict the aroma quality of H. sabdariffa.


Hibiscus sabdariffa L. Antioxidant Volatile compounds Descriptive sensory analysis PLSR 



We are grateful for the support from the department of the National Science and Technology Support Program (2015BAD17B04, 2015BAD19B03), the National Natural Science Foundation of China (Grant No. 61301239), China Postdoctoral Science Foundation (2013M540422, 2014T70483) and Science Foundation for Postdoctoral in Jiangsu Province (1301051C).


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Copyright information

© Springer Science+Business Media New York 2017

Authors and Affiliations

  • Haroon Elrasheid Tahir
    • 1
  • Zou Xiaobo
    • 1
    Email author
  • Abdalbasit Adam Mariod
    • 2
    • 3
  • Gustav Komla Mahunu
    • 4
  • Mohammed A. Y. Abdualrahman
    • 1
    • 5
  • William Tchabo
    • 1
  1. 1.School of Food and Biological EngineeringJiangsu UniversityZhenjiangChina
  2. 2.College of Sciences and Arts-AlkamilUniversity of JeddahAlkamilSaudi Arabia
  3. 3.Department of Food Science & Technology, College of Agricultural StudiesSudan University of Science & TechnologyKhartoum NorthSudan
  4. 4.Department of Food Science & Technology, Faculty of AgricultureUniversity for Development StudiesTamaleGhana
  5. 5.Department of Food TechnologyNyala Technical CollegeNyalaSudan

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