Abstract
The Mg-10Gd-0.4Zr rare-earth magnesium alloy was joined by ultrasonic vibration-assisted electron beam welding for the first time. The microstructures, pore defects, element segregation and mechanical properties of the ultrasonic vibration-assisted electron beam welding Mg-10Gd-0.4Zr joints were studied. The microstructure of the weld zone of the electron beam welded joint was uniform and fine equiaxed grains, and the precipitated Mg2Gd phase was distributed at the grain boundary. The pore defects were eliminated by ultrasonic cavitation and acoustic flow effects. The grain diameter of the fusion zone was further refined by 19.05% by the ultrasonic vibration. The precipitates of Mg3Gd phases continuously distributed at grain boundaries were effectively inhibited, and the solid solution of Gd atoms was promoted by the action of ultrasonic vibration. The tensile strength of the ultrasonic-assisted electron beam welding joints was 255 MPa, 8.1% higher than that of the electron beam welding joints.
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References
Y. Cai, H. Yan, M. Zhu, K. Zhang, X. Yi, and R. Chen, High-Temperature Oxidation Behavior and Corrosion Behavior of High Strength Mg-xGd Alloys with High Gd Content, Corros. Sci., 2021, 193, 109872. https://doi.org/10.1016/j.corsci.2021.109872
Y. Liu, M. Ma, X. Li, Y. Li, G. Shi, J. Yuan et al., Homogenization Treatment of Mg-6Zn-3Sn (wt.%) Alloy and Its Effects on Microstructure and Mechanical Properties, Trans. Nonferr. Met Soc. China, 2023, 33, p 67–78. https://doi.org/10.1016/s1003-6326(22)66091-6
Y. Sun, R. Wang, C. Peng, and X. Wang, Effect of Gd on Microstructure, Mechanical Properties, and Corrosion Behavior of as-Homogenized Mg−8Li−3Al−2Zn−0.2Zr alloy, Trans. Nonferr. Met. Soc. China, 2022, 32, p 2494–509. https://doi.org/10.1016/S1003-6326(22)65961-2
C. He, M. Yuan, B. Jiang, L. Liu, Q. Wang, Y. Chai et al., Anomalous Effect of Grain Size on the Room-Temperature Bendability of Mg–Gd Alloy Sheet, Mater. Sci. Eng. A, 2022, 832, 142397. https://doi.org/10.1016/j.msea.2021.142397
J. Zhao, B. Jiang, J. Xu, W. He, G. Huang, and F. Pan, The Influence of Gd on the Recrystallisation, Texture and Mechanical Properties of Mg Alloy, Mater. Sci. Eng. A, 2022, 839, 142867. https://doi.org/10.1016/j.msea.2022.142867
X. Wu, C. Li, C. Guo, and Z. Du, Thermodynamic Re-Assessment of the Mg–Gd–Y Ternary System Coupling with the Driving Forces for Phase Precipitations During Aging Process, J Magnes Alloy, 2022 https://doi.org/10.1016/j.jma.2022.01.008
J. Song, J. She, D. Chen, and F. Pan, Latest Research Advances on Magnesium and Magnesium Alloys Worldwide, J Magnes Alloy, 2020, 8, p 1–41. https://doi.org/10.1016/j.jma.2020.02.003
Z. Jiang, D. Yin, Y. Wan, R. Ni, H. Zhou, J. Zheng et al., Operating Slip Modes and Inhomogeneous Plastic Deformation of Mg-10Gd-3Y-0.5Zr Alloy During Compression, Trans. Nonferr. Met Soc China, 2023, 33, p 79–94. https://doi.org/10.1016/s1003-6326(22)66092-8
Y. Liu, J. Wen, H. Li, and J. He, Effects of Extrusion Parameters on the Microstructure, Corrosion Resistance, and Mechanical Properties of Biodegradable Mg–Zn–Gd–Y–Zr Alloy, J. Alloys Compd., 2022, 891, 161964. https://doi.org/10.1016/j.jallcom.2021.161964
G. Li, L. Zhou, J. Zhang, S. Luo, and N. Guo, Macrostructure, Microstructure and Mechanical Properties of Bobbin Tool Friction Stir Welded ZK60 Mg Alloy Joints, J Mater Res Technol, 2020, 9, p 9348–9361. https://doi.org/10.1016/j.jmrt.2020.05.067
V. Subravel, N. Alagappan, and N. Babu, Influence of Arc Oscillation Frequency on Tensile Properties and Microstructural Characteristics of Magnetic Arc Oscillation Welded AZ31B Magnesium Alloy Joints, Mater Today Proc, 2020, 22, p 606–613. https://doi.org/10.1016/j.matpr.2019.09.001
X. Wang, Y. Morisada, and H. Fujii, Interface strengthening in Dissimilar Double-Sided Friction Stir Spot welding of AZ31/ZK60 Magnesium Alloys by Adjustable Probes, J. Mater. Sci. Technol., 2021, 85, p 158–168. https://doi.org/10.1016/j.jmst.2021.01.024
Y. Gao, K. Hao, L. Xu, Y. Han, L. Zhao, W. Ren et al., Microstructure Homogeneity and Mechanical Properties of Laser-Arc Hybrid Welded AZ31B Magnesium Alloy, J Magnes Alloy, 2022 https://doi.org/10.1016/j.jma.2022.09.034
P. Fu, Z. Mao, Y. Wang, C. Zuo, and H. Xu, Mechanical Properties of Ti6.5Al2Zr1Mo1V Titanium Alloy With EBW Under Different Temperatures, Mater. Sci. Eng. A, 2014, 608, p 199–206. https://doi.org/10.1016/j.msea.2014.04.048
M. Cheng, B. Yu, R. Guo, X. Shi, L. Xu, J. Qiao et al., Electron Beam Welding of a Novel Near α High Temperature Titanium Alloy Powder Compact: Effect of Post-welding Heat Treatment on Tensile Properties, J. Mater. Res. Technol., 2021, 10, p 153–163. https://doi.org/10.1016/j.jmrt.2020.12.022
J. Singh and A.S. Shahi, Metallurgical and Corrosion Characterization of Electron Beam Welded Duplex Stainless Steel Joints, J. Manuf. Process., 2020, 50, p 581–595. https://doi.org/10.1016/j.jmapro.2020.01.009
G. Chen, J. Liu, X. Shu, H. Gu, B. Zhang, and J. Feng, Beam Scanning Effect on Properties Optimization of Thick-Plate 2A12 Aluminum Alloy Electron-Beam Welding Joints, Mater. Sci. Eng. A, 2019, 744, p 583–592. https://doi.org/10.1016/j.msea.2018.12.034
Y. Luo and J. Liu, Microstructural Evolution in AZ91D Magnesium Alloy During Electron Beam Welding, Vacuum, 2011, 85, p 1004–1010. https://doi.org/10.1016/j.vacuum.2011.02.009
C.-T. Chi, C.-G. Chao, T.-F. Liu, and C.-C. Wang, A Study of Weldability and Fracture Modes in Electron Beam Weldments of AZ Series Magnesium Alloys, Mater. Sci. Eng. A, 2006, 435–436, p 672–680. https://doi.org/10.1016/j.msea.2006.07.098
Z. Lei, J. Bi, P. Li, Q. Li, Y. Chen, and D. Zhang, Melt Flow and Grain Refining in Ultrasonic Vibration Assisted Laser Welding Process of AZ31B Magnesium Alloy, Opt. Laser Technol., 2018, 108, p 409–417. https://doi.org/10.1016/j.optlastec.2018.07.015
J. Liu, H. Zhu, Z. Li, W. Cui, and Y. Shi, Effect of Ultrasonic Power on Porosity, Microstructure, Mechanical Properties of the Aluminum Alloy Joint by Ultrasonic Assisted Laser-MIG Hybrid Welding, Opt. Laser Technol., 2019, 119, 105619. https://doi.org/10.1016/j.optlastec.2019.105619
Q. Zhu, Y. Lei, Y. Wang, W. Huang, B. Xiao, and Y. Ye, Effects of arc-Ultrasonic on Pores Distribution and Tensile Property in TIG Welding Joints of MGH956 Alloy, Fusion Eng. Des., 2014, 89, p 2964–2970. https://doi.org/10.1016/j.fusengdes.2014.08.012
Y. Tian, J. Shen, S. Hu, Z. Wang, and J. Gou, Effects of Ultrasonic Vibration in the CMT Process on Welded Joints of Al Alloy, J. Mater. Process. Technol., 2018, 259, p 282–291. https://doi.org/10.1016/j.jmatprotec.2018.05.004
X. Zhang, S. Bian, P. Zhao, X. Ding, Y. Li, and Z. Cao, Investigation on Pore Formation in Pulsed Laser Spot Welding of AZ31 Magnesium Alloy, Opt. Laser Technol., 2022, 149, 107894. https://doi.org/10.1016/j.optlastec.2022.107894
F. Iranshahi, M.B. Nasiri, F.G. Warchomicka, and C. Sommitsch, Investigation of the Degradation Rate of Electron Beam Processed and Friction Stir Processed Biocompatible ZKX50 Magnesium Alloy, J Magnes Alloy, 2022, 10, p 707–720. https://doi.org/10.1016/j.jma.2021.08.016
Y. Wang, H. Wang, J. Chen, Y. Zheng, C. Li, T. Liu et al., Achieving Polycrystalline Transformation and Microstructural Segregation Reduction of Nickel-Based Single Crystal Super-Alloys by Ultrasonic Pulse Arc Welding, J. Mater. Res. Technol., 2023, 24, p 2200–2212. https://doi.org/10.1016/j.jmrt.2023.03.114
Q. Fan, C. Chen, C. Fan, Z. Liu, X. Cai, S. Lin et al., Ultrasonic Suppression of Element Segregation in Gas Tungsten arc Cladding AlCoCuFeNi High-Entropy Alloy Coatings, Surf. Coat. Technol., 2021, 420, 127364. https://doi.org/10.1016/j.surfcoat.2021.127364
J. Huang, J. Li, C. Li, C. Huang, and B. Friedrich, Elimination of Edge Cracks and Centerline Segregation of Twin-Roll Cast Aluminum Strip by Ultrasonic Melt Treatment, J. Mater. Res. Technol., 2020, 9, p 5034–5044. https://doi.org/10.1016/j.jmrt.2020.03.021
X. Tong, G. You, Y. Wang, H. Wu, W. Liu, P. Li et al., Effect of Ultrasonic Treatment on Segregation and Mechanical Properties of As-Cast Mg–Gd Binary Alloys, Mater. Sci. Eng. A, 2018, 731, p 44–53. https://doi.org/10.1016/j.msea.2018.06.017
J. Kacher, C. Landon, B.L. Adams, and D. Fullwood, Bragg’s Law Diffraction Simulations for Electron Backscatter Diffraction Analysis, Ultramicroscopy, 2009, 109, p 1148–1156. https://doi.org/10.1016/j.ultramic.2009.04.007
S. Merouani, O. Hamdaoui, Y. Rezgui, and M. Guemini, Theoretical Estimation of the Temperature and Pressure Within Collapsing Acoustical Bubbles, Ultrason. Sonochem., 2014, 21, p 53–59. https://doi.org/10.1016/j.ultsonch.2013.05.008
G.S.B. Lebon, I. Tzanakis, K. Pericleous, D. Eskin, and P.S. Grant, Ultrasonic Liquid Metal Processing: The Essential Role of Cavitation Bubbles in Controlling Acoustic Streaming, Ultrason. Sonochem., 2019, 55, p 243–255. https://doi.org/10.1016/j.ultsonch.2019.01.021
B.N. Du, Z.Y. Hu, L.Y. Sheng, D.K. Xu, Y.X. Qiao, B.J. Wang et al., Microstructural Characteristics and Mechanical Properties of the Hot Extruded Mg-Zn-Y-Nd Alloys, J. Mater. Sci. Technol., 2021, 60, p 44–55. https://doi.org/10.1016/j.jmst.2020.05.021
L. Gao, R.S. Chen, and E.H. Han, Effects of Rare-Earth Elements Gd and Y on the Solid Solution Strengthening of Mg Alloys, J. Alloys Compd., 2009, 481, p 379–384. https://doi.org/10.1016/j.jallcom.2009.02.131
W.X. Wu, L. Jin, F.H. Wang, J. Sun, Z.Y. Zhang, W.J. Ding et al., Microstructure and Texture Evolution During Hot Rolling and Subsequent Annealing of Mg–1Gd Alloy, Mater. Sci. Eng. A, 2013, 582, p 194–202. https://doi.org/10.1016/j.msea.2013.05.080
J. Peng, S. Han, Z. Li, J. Zhang, X. Chen, G. Huang et al., Revealing the Microstructure Evolution, Deformation Behavior and Tensile Properties of AZ31/AM60 Dissimilar Mg Alloy Joints Under Different Welding Technologies, J. Mater. Res. Technol., 2024, 28, p 814–830. https://doi.org/10.1016/j.jmrt.2023.11.282
F. Yang, J. Zhou, and R. Ding, Ultrasonic Vibration Assisted Tungsten Inert Gas Welding of Dissimilar Magnesium Alloys, J. Mater. Sci. Technol., 2018, 34, p 2240–2245. https://doi.org/10.1016/j.jmst.2018.06.009
X. He, D. Kong, Y. Zhou, L. Wang, X. Ni, L. Zhang et al., Powder Recycling Effects on Porosity Development and Mechanical Properties of hastelloy X Alloy During Laser Powder Bed Fusion Process, Addit. Manuf., 2022, 55, 102840. https://doi.org/10.1016/j.addma.2022.102840
Acknowledgment
This work was supported by National Key Research and Development Program of China (No. 2022YFB3404700), Taishan Scholars Project (No. tsqn202306136), Fundamental Research Funds for the Central Universities (No. HIT.OCEF.2022043) and National Natural Science Foundation of China (No. 52175308).
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Song, D., Wang, T., Zhao, Y. et al. Microstructural Characteristics and Mechanical Properties of Ultrasonic-Assisted Electron Beam Welding Joints of Rare-Earth Magnesium Alloy. J. of Materi Eng and Perform (2024). https://doi.org/10.1007/s11665-024-09529-w
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DOI: https://doi.org/10.1007/s11665-024-09529-w