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Very-High-Cycle-Fatigue Property of IN 718 Manufactured by Selective Laser Melting at Elevated Temperature: Microstructure-Related Failure Behavior and Life Prediction

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Abstract

The high- and very-high-cycle-fatigue properties of IN718 Ni-based superalloy manufactured by selective laser melting (SLM) were investigated by axially loaded fatigue tests at room temperature (25 °C) and elevated temperature (650 °C) with a stress ratio of R = −1. Due to the high energy density and rapid cooling rate of the SLM process, the grains grew as dendrites surrounded by chain and dotted Laves phases. Subsequently, the results of monotonic tensile tests show that the SLMed IN718 has good resistance to elevated temperature. The stress–life characteristic curves revealed a continuous decline with no conventional fatigue limit. The fracture observation illustrated that surface flaw-induced failure is predominant at 25 °C, while internal failure, caused by crystallographic facets cracking, is prevalent at 650 °C under lower stress. Furthermore, the internal failure mechanism related with microstructure was summarized. Based on the evaluation of stress intensity factor ranges, the threshold values of long and small crack growth can be obtained, as well as the transition lengths from small to long cracks can also be calculated. Finally, a model based on fatigue indicator parameter was proposed to predict the fatigue life, and the predicted results were acceptable.

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References

  1. X.F. Ding, Q. Feng, Y.R. Zheng, and X.F. Ding, Formation of Hole-Edge Cracks in a Combustor Liner of an Aero Engine, Eng. Fail. Anal., 2015, 55, p 148–156.

    Article  Google Scholar 

  2. T.D. Ngo, A. Kashani, G. Imbalzano, K. Nguyen, and D. Hui, Additive Manufacturing (3D Printing): A Review of Materials, Methods, Appl. Chall. Compos. Part B Eng., 2018, 143, p 172–196.

    Article  CAS  Google Scholar 

  3. E. Hosseini and V.A. Popovich, A Review of Mechanical Properties of Additively Manufactured Inconel 718, Addit. Manuf., 2019, 30, p 100877.

    CAS  Google Scholar 

  4. D.S. Watring, J.T. Benzing, N. Hrabe, and A.D. Spear, Effects of Laser-Energy Density and Build Orientation on the Structure-Property Relationships in as-Built Inconel 718 Manufactured by Laser Powder Bed Fusion, Addit. Manuf., 2020, 36, p 101425.

    CAS  Google Scholar 

  5. G.C. Huang, G.Q. Liu, M.N. Feng, M. Zhang, B.F. Hu, and H. Wang, The Effect of Cooling Rates from Temperatures Above the γ’ Solvus on the Microstructure of a New Nickel-Based Powder Metallurgy superalloy, J. Alloy Compd., 2018, 747, p 1062–1072.

    Article  CAS  Google Scholar 

  6. A. Yadollahi, N. Shamsaei, S.M. Thompson, and D. Seely, Effects of Process Time Interval and Heat Treatment on the Mechanical and Microstructural Properties of Direct Laser Deposited 316L Stainless Steel, Mater. Sci. Eng. A, 2015, 644, p 171–183.

    Article  CAS  Google Scholar 

  7. T.M. Smith, T.P. Gabb, C.A. Kantzos, A.C. Thompson, C.K. Sudbrack, B. West, D.L. Ellis, and C.L. Bowman, The Effect of Composition on Microstructure and Properties for Additively Manufactured Superalloy 718, J. Alloy Compd., 2021, 873, p 159789.

    Article  CAS  Google Scholar 

  8. M. Mahmoudi, A. Elwany, A. Yadollahi, S. Thompson, L. Bian, and N. Shamsaei, Mechanical Properties and Microstructural Characterization of Selective Laser Melted 17-4 PH Stainless Steel, Rapid Prototyp. J., 2017, 23, p 280–294.

    Article  Google Scholar 

  9. Y.C. Wang, J. Shi, and Y. Liu, Competitive Grain Growth and Dendrite Morphology Evolution in Selective Laser Melting of Inconel 718 Superalloy, J. Cryst. Growth, 2019, 521, p 15–29.

    Article  CAS  Google Scholar 

  10. S. Sui, H. Tan, J. Chen, C.L. Zhong, Z. Li, W. Fan, A. Gasser, and W.D. Huang, The influence of Laves Phases on the Room Temperature Tensile Properties of Inconel 718 Fabricated by Powder Feeding Laser Additive Manufacturing, Acta Mater., 2019, 164, p 413–427.

    Article  CAS  Google Scholar 

  11. Y.H. Liu, Y. Wu, J.W. Yu, J. Ju, Z. Zhang, M.D. Kang, J. Wang, B.D. Sun, and Y. Ning, Temperature-Dependent Deformation Mechanisms and Microstructural Degradation of a Polycrystalline Nickel-Based Superalloy, J. Alloy Compd., 2019, 775, p 181–192.

    Article  CAS  Google Scholar 

  12. J.J. Xu, X. Lin, P.F. Guo, H.O. Yang, L. Xue, W.D. Huang, L. Xue, and W.D. Huang, The Microstructure Evolution and Strengthening Mechanism of a γ’-Strengthening Superalloy Prepared by Induction-Assisted Laser Solid Forming, J. Alloy Compd., 2019, 780, p 461–475.

    Article  CAS  Google Scholar 

  13. S. Kumari, D.V.V. Satyanarayana, and M. Srinivas, Failure Analysis of Gas Turbine Rotor Blades, Eng. Fail. Anal., 2014, 45, p 234–244.

    Article  CAS  Google Scholar 

  14. A. Burov and E. Fedorova, Modeling of Interface Failure in a Thermal Barrier Coating System on Ni-Based Superalloys, Eng. Fail. Anal., 2021, 123, p 105320.

    Article  CAS  Google Scholar 

  15. D. Shi, Z. Cheng, Z. Li, X. Yang, and M. Wang, Viscoplastic Constitutive Model for Ni-Based Directionally Solidified Superalloy: Experimental Validation on Notched Specimen, Eng. Fail. Anal., 2020, 118, p 104930.

    Article  CAS  Google Scholar 

  16. Y.L. Hu, X. Liu, Y.L. Li, Y.C. Ou, X.H. Gao, Q. Zhang, W. Li, and W.D. Huang, Microstructural Evolution and Anisotropic Mechanical Properties of Inconel 625 Superalloy Fabricated by Directed Energy Deposition, J. Alloy Compd., 2021, 870, p 159426.

    Article  CAS  Google Scholar 

  17. Z.H. Jiao, L.M. Lei, H.C. Yu, F. Xu, R.D. Xu, and X.R. Wu, Experimental Evaluation on Elevated Temperature Fatigue and Tensile Properties of one Selective Laser Melted Nickel Based Superalloy, Int. J. Fatigue, 2019, 121, p 172–180.

    Article  CAS  Google Scholar 

  18. D. Pradhan, G.S. Mahobia, K. Chattopadhyay, and V. Singh, Effect of Pre Hot Corrosion on High Cycle Fatigue Behavior of the Superalloy IN718 at 600 °C, Int. J. Fatigue, 2018, 114, p 120–129.

    Article  CAS  Google Scholar 

  19. P.D. Nezhadfar, A.S. Johnsonc, and N. Shamsaei, Fatigue Behavior and Microstructural Evolution of Additively Manufactured Inconel 718 under Cyclic Loading at Elevated Temperature, Int. J. Fatigue, 2020, 136, p 105598.

    Article  CAS  Google Scholar 

  20. Y. Yamashita, T. Murakami, R. Miharaa, M. Okadab, and Y. Murakami, Defect Analysis and Fatigue Design Basis for Ni-Based Superalloy 718 Manufactured by Selective Laser Melting, Int. J. Fatigue, 2018, 117, p 485–495.

    Article  CAS  Google Scholar 

  21. Z.W. Xu, A. Liu, and X.S. Wang, The Influence of Building Direction on the Fatigue Crack Propagation Behavior of Ti6Al4V Alloy Produced by Selective Laser Melting, Mater. Sci. Eng. A, 2019, 767, p 138409.

    Article  CAS  Google Scholar 

  22. Z.W. Xu, A. Liu, and X.S. Wang, Fatigue Performance and Crack Propagation Behavior of Selective Laser Melted AlSi10Mg in 0°, 15°, 45° and 90° Building Directions, Int. J. Fatigue, 2021, 812, p 141141.

    CAS  Google Scholar 

  23. T. Murakami and Y. Murakami, Effects of Small Defects and Nonmetallic Inclusions on the Fatigue Strength of Metals, Key Eng. Mater., 1991, 51–52, p 37–42.

    Article  Google Scholar 

  24. T. Sakai, A. Nakagawa, N. Oguma, Y. Nakamura, and A. Ueno, A Review on Fatigue Fracture Modes of Structural Metallic Materials in Very High Cycle Regime, Int. J. Fatigue, 2016, 93, p 339–351.

    Article  Google Scholar 

  25. S. Shao, M.M. Khonsari, S. Guo, W.J. Meng, and N. Li, Overview: Additive Manufacturing Enabled Accelerated Design of Ni-Based Alloys for Improved Fatigue Life, Addit. Manuf., 2019, 29, p 100779.

    CAS  Google Scholar 

  26. J.S. Miao, T.M. Pollock, and J.W. Jones, Crystallographic Fatigue Crack Initiation in Nickel-Based Superalloy Rene′ 88DT at Elevated Temperature, Acta Mater., 2009, 57, p 5964–5974.

    Article  CAS  Google Scholar 

  27. C. Stöcker, M. Zimmermannn, and H.J. Christ, Localized Cyclic Deformation and Corresponding Dislocation Arrangements of Polycrystalline Ni-Base Superalloys and Pure Nickel in the VHCF Regime, Int. J. Fatigue, 2011, 33, p 2–9.

    Article  Google Scholar 

  28. A. Amanov, Y. Pyun, J. Kim, C. Suh, I. Cho, Q.Y. Wang, and M.K. Khan, Ultrasonic Fatigue Performance of High Temperature Structural Material Inconel 718 Alloys at High Temperature After UNSM Treatment, Fatigue Fract. Eng. Mater. Struct., 2015, 38, p 1266–1273.

    Article  CAS  Google Scholar 

  29. S. Utada, L.M.B. Ormastroni, J. Rame, P. Villechaise, and J. Cormier, VHCF Life of AM1 Ni-Based Single Crystal Superalloy After Pre-deformation, Int. J. Fatigue, 2021, 148, p 106224.

    Article  Google Scholar 

  30. K. Yang, Q. Huang, Q.Y. Wang, and Q. Chen, Competing Crack Initiation Behaviors of a Laser Additively Manufactured Nickel-Based Superalloy in High and Very High Cycle Fatigue Regimes, Int. J. Fatigue, 2020, 136, p 105580.

    Article  CAS  Google Scholar 

  31. X.B. Yu, X. Lin, H. Tan, Y.L. Hu, S.Y. Zhang, F.C. Liu, H.O. Yang, and W.D. Huang, Microstructure and Fatigue Crack Growth Behavior of Inconel 718 Superalloy Manufactured by Laser Directed Energy Deposition, Int. J. Fatigue, 2021, 143, p 106005.

    Article  CAS  Google Scholar 

  32. T.J. Zhou, H.S. Ding, X.P. Ma, W. Feng, H.B. Zhou, A.L. Li, Y. Meng, and H.X. Zhang, Effect of Precipitates on High-Temperature Tensile Strength of a High W-Content Cast Ni-Based Superalloy, J. Alloys Compd., 2019, 797, p 486–496.

    Article  CAS  Google Scholar 

  33. W.G. Li, J.Z. Ma, H.B. Kou, J.X. Shao, X.Y. Zhang, Y. Deng, Y. Tao, and D.N. Fang, Modeling the Effect of Temperature on the Yield Strength of Precipitation Strengthening Ni-Base Superalloys, Int. J. Plast., 2019, 116, p 143–158.

    Article  CAS  Google Scholar 

  34. S. Sui, J. Chen, E.X. Fan, H.O. Yang, X. Lin, and W.D. Huang, The Influence of Laves Phases on the High-Cycle Fatigue Behavior of Laser Additive Manufactured Inconel 718, Mater. Sci. Eng. A, 2017, 695, p 6–13.

    Article  CAS  Google Scholar 

  35. X. Li, R.F. Zhang, X.Y. Wang, Y.J. Liu, C. Wang, H. Zhang, L. Li, C. He, and Q.Y. Wang, Effect of High Temperature on Crack Initiation of Super Austenitic Stainless Steel 654SMO in Very High Cycle Fatigue, Mater. Des., 2020, 193, p 108750.

    Article  CAS  Google Scholar 

  36. X.B. Yu, X. Lin, H. Tan et al., Microstructure and Fatigue Crack Growth Behavior of Inconel 718 Superalloy Manufactured by Laser Directed Energy Deposition, Int. J. Fatigue, 2021, 143, p 106005.

    Article  CAS  Google Scholar 

  37. J.C. Stinville, E. Martin, M. Karadge, S. Ismonov, M. Soare, T. Hanlon et al., Competing Modes for Crack Initiation from Nonmetallic Inclusions and Intrinsic Microstructural Features during Fatigue in a Polycrystalline Nickel-Based Superalloy, Metall. Mater. Trans. A, 2018, 49, p 3865–3873.

    Article  CAS  Google Scholar 

  38. J.C. Stinville, E. Martin, M. Karadge, S. Ismonov, M. Soare, T. Hanlon et al., Fatigue Deformation in a Polycrystalline Nickel Base Superalloy at Intermediate and High Temperature: Competing Failure Modes, Acta Mater., 2018, 152, p 16–33.

    Article  CAS  Google Scholar 

  39. W. Li, R. Sun, P. Wang, X.L. Li, Y.C. Zhang, T.Y. Hu, C. Li, and T. Sakai, Subsurface Faceted Cracking Behavior of Selective Laser Melting Ni-Based Superalloy under Very High Cycle Fatigue, Scr. Mater., 2021, 194, p 113613.

    Article  CAS  Google Scholar 

  40. N. Kawagoishi, Q. Chen, and H. Nisitani, Fatigue Strength of Inconel 718 at Elevated Temperatures, Fatigue Fract. Eng. Mater. Struct., 2000, 23, p 209–216.

    Article  Google Scholar 

  41. Y. Murakami, S. Kodama, and S. Konuma, Quantitative Evaluation of Effect of Nonmetallic Inclusions on Fatigue Strength of High Strength Steel, Trans. Jpn. Soc. Mech. Eng., 1988, 54, p 688–695.

    Article  CAS  Google Scholar 

  42. G. Gao, Q. Xu, H. Guo, X. Gui, B. Zhang, and B. Bai, Effect of Inclusion and Microstructure on the Very High Cycle Fatigue Behavior of High Strength Bainite/Martensite Multiphase Steels, Mater. Sci. Eng. A, 2019, 739, p 404–414.

    Article  CAS  Google Scholar 

  43. Y. Murakami and M. Endo, Effects of Defects, Inclusions and Inhomogeneities on Fatigue Strength, Int. J. Fatigue, 1994, 16, p 163–182.

    Article  CAS  Google Scholar 

  44. D.B. Witkin, D. Patel, T.V. Albright, G.E. Bean, and T. McLouth, Influence of Surface Conditions and Specimen Orientation on High Cycle Fatigue Properties of Inconel 718 Prepared by Laser Powder Bed Fusion, Int. J. Fatigue, 2020, 132, p 105392.

    Article  CAS  Google Scholar 

  45. Y. Murakami, Metal Fatigue Effects of Small Defects and Nonmetallic Inclusions, Elsevier Science, Amsterdam Boston, 2002.

    Google Scholar 

  46. Z.W. Xu, A. Liu, X.S. Wang, B. Liu, and M.H. Guo, Fatigue Limit Prediction Model and Fatigue Crack Growth Mechanism for Selective Laser Melting Ti6Al4V Samples with Inherent Defects, Int. J. Fatigue, 2021, 143, p 106008.

    Article  CAS  Google Scholar 

  47. A. Fatemi and D.F. Socie, A Critical Plane Approach to Multiaxial Fatigue Damage Including Out-of-Phase Loading, Fatigue Eng. Mater., 1988, 11, p 149–165.

    Article  Google Scholar 

  48. M.W. Brown and K.J. Miller, A Theory for Fatigue Failure under Multiaxial Stress and Strain Conditions, Proc. Inst. Mecha. Eng., 1973, 187, p 745–755.

    Article  Google Scholar 

  49. A. Cervellon, J. Cormier, F. Mauget, and Z. Hervier, VHCF Life Evolution After Microstructure Degradation of a Ni-Based Single Crystal Superalloy, Int. J. Fatigue, 2017, 104, p 251–262.

    Article  CAS  Google Scholar 

  50. A. Cervellon, S. Hemery, P. Kurnsteiner, B. Gault, P. Kontis, and J. Cormier, Crack Initiation Mechanisms During Very High Cycle Fatigue of Ni-Based Single Crystal Superalloys at High Temperature, Acta Mater., 2020, 188, p 131–144.

    Article  CAS  Google Scholar 

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Acknowledgments

This work was supported by the Special Project for Seed-Innovation of NIN (grant number: ZZNR2202).

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RS was involved in data curation, methodology, writing—original draft; WZ helped in supervision, writing—review & editing, funding acquisition; HL and YZ contributed to investigation; MX was involved in visualization; RB helped in formal analysis; XC contributed to data curation; FW helped in validation.

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Correspondence to Wen Zhang.

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Sun, R., Zhang, W., Liu, H. et al. Very-High-Cycle-Fatigue Property of IN 718 Manufactured by Selective Laser Melting at Elevated Temperature: Microstructure-Related Failure Behavior and Life Prediction. J. of Materi Eng and Perform 33, 4377–4391 (2024). https://doi.org/10.1007/s11665-023-08327-0

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  • DOI: https://doi.org/10.1007/s11665-023-08327-0

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