Skip to main content
Log in

Effect of Different Rolling Passes on Microstructure and Mechanical Properties of M390 Powder Metallurgy High-Speed Steel

  • Technical Article
  • Published:
Journal of Materials Engineering and Performance Aims and scope Submit manuscript

Abstract

The microstructure and mechanical properties of M 390 powder metallurgy (PM) high-speed steel after rolling processes are systematically investigated and compared by scanning electron microscope microstructure observation, x-ray diffractometer phase analysis and room-temperature tensile experiments. The results found that the microstructure of M390 PM high-speed steel with different rolling passes is composed of ferrite matrix, trace martensite and MC carbides, M7C3 carbides and M23C6 carbides. On the one hand, the rolling deformation refines the microstructure; on the other hand, the high temperature during hot rolling processes causes the carbides to grow and coarsen, so the rolling pass has no regular effect on the carbides of the powder metallurgy high-speed steel. With the increase in the number of the rolling passes, the hardness and strength of the M390PM high‐speed steel plate increase firstly and then do not significantly change. Because the smaller the carbide size is, the higher the roundness is, the more the dispersed carbide is, and the higher the hardness and strength is. The increase in the rolling passes induces the number of carbides distributed on the matrix, which decreases the dispersed strengthening effect.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Fig. 1
Fig. 2
Fig. 3
Fig. 4
Fig. 5
Fig. 6
Fig. 7
Fig. 8
Fig. 9
Fig. 10

Similar content being viewed by others

References

  1. E. Ruiz-Navas, R. García, E. Gordo, and F. Velasco, Development and Characterization of High-speed Steel Matrix Composites Gradient Materials, J. Mater. Process. Technol., 2003, 143, p 769–775.

    Article  Google Scholar 

  2. D. Chatterjee, G. Sutradhar, and B. Oraon, Fuzzy Rule-Based Prediction of Hardness for Sintered HSS Components, J. Mater. Process. Technol., 2008, 200, p 212–220.

    Article  CAS  Google Scholar 

  3. Z. Liu, N. Loh, K. Khor, and S. Tor, Microstructure Evolution During Sintering of Injection Molded M2 High Speed Steel, Mater. Sci. Eng. A, 2000, 293, p 46–55.

    Article  Google Scholar 

  4. J. Badger, Grindability of Conventionally Produced and Powder-Metallurgy High-Speed Steel, CIRP Ann., 2007, 56, p 353–356.

    Article  Google Scholar 

  5. K.C. Hwang, S. Lee, and H.C. Lee, Effects of Alloying Elements on Microstructure and Fracture Properties of Cast High Speed Steel Rolls: Part I: Microstructural Analysis, Mater. Sci. Eng. A, 1998, 254, p 282–295.

    Article  Google Scholar 

  6. H. Qu, B. Liao, L. Liu, D. Li, J. Guo, X. Ren, and Q. Yang, Precipitation Rule of Carbides In a New High Speed Steel for Rollers, Calphad, 2012, 36, p 144–150.

    Article  CAS  Google Scholar 

  7. J. Hidalgo, M. Vittorietti, H. Farahani, F. Vercruysse, R. Petrov, and J. Sietsma, Influence of M23C6 Carbides on the Heterogeneous Strain Development in Annealed 420 Stainless Steel, Acta Mater., 2020, 200, p 74–90.

    Article  CAS  Google Scholar 

  8. J. Saewe, N. Carstensen, P. Kürnsteiner, E.A. Jägle, and J.H. Schleifenbaum, Influence of Increased Carbon Content on the Processability of High-Speed Steel Hs6-5-3-8 by Laser Powder Bed Fusion, Addit. Manuf., 2021, 46, p 102125.

    CAS  Google Scholar 

  9. H. Kim, J.-Y. Kang, D. Son, T.-H. Lee, and K.-M. Cho, Evolution of Carbides in Cold-Work Tool Steels, Mater. Charact., 2015, 107, p 376–385.

    Article  CAS  Google Scholar 

  10. S. Wei and J. Zhu, Effects of Vanadium and Carbon on Microstructures and Abrasive Wear Resistance of High Speed Steel, Tribol. Int., 2006, 39, p 641–648.

    Article  CAS  Google Scholar 

  11. J.W. Park, H.C. Lee, and S. Lee, Composition, Microstructure, Hardness, and Wear Properties of High-Speed Steel Rolls, Metall. Mater. Trans. A, 1999, 30, p 399–409.

    Article  Google Scholar 

  12. N. Yüksel and S. Şahin, Wear Behavior-Hardness-Microstructure Relation of Fe-Cr-C and Fe-Cr-C-B Based Hardfacing Alloys, Mater. Des., 2014, 58, p 491–498.

    Article  Google Scholar 

  13. S. Sapate, A. Selokar, and N. Garg, Experimental Investigation of Hardfaced Martensitic Steel Under Slurry Abrasion Conditions, Mater. Des., 2010, 31, p 4001–4006.

    Article  CAS  Google Scholar 

  14. X. Meng, C. Li, and W. Chen, Effects of Ti and B Addition on Microstructures and Mechanical Properties of Hot-Rolled High-Strength Nb-Containing Steels, J. Mater. Eng. Perform., 2016, 25, p 3472–3481.

    Article  CAS  Google Scholar 

  15. R. Misra, H. Nathani, J. Hartmann, and F. Siciliano, Microstructural Evolution in a New 770 MPa Hot Rolled Nb-Ti Microalloyed Steel, Mater. Sci. Eng. A., 2005, 394, p 339–352.

    Article  Google Scholar 

  16. J. Guo, L. Liu, Y. Feng, S. Liu, X. Ren, and Q. Yang, Crystallographic Characterizations of Eutectic and Secondary Carbides in a Fe-12Cr-2.5 Mo-1.5 W-3V-1.25 C Alloy, Met. Mater. Int., 2017, 23, p 313–319.

    Article  CAS  Google Scholar 

  17. T. Tsuchiyama, J. Tobata, T. Tao, N. Nakada, and S. Takaki, Quenching and Partitioning Treatment of a Low-Carbon Martensitic Stainless Steel, Mater. Sci. Eng A, 2012, 532, p 585–592.

    Article  CAS  Google Scholar 

  18. Q. Zhu, H. Zhu, A. Tieu, M. Reid, and L. Zhang, In-Situ Investigation of Oxidation Behaviour in High-Speed Steel Roll Material Under Dry and Humid Atmospheres, Corros. Sci., 2010, 52, p 2707–2715.

    Article  CAS  Google Scholar 

  19. Q. Zhu, H. Zhu, A. Tieu, and C. Kong, Three Dimensional Microstructure Study of Oxide Scale Formed on A High-Speed Steel by Means of SEM, FIB and TEM, Corros. Sci., 2011, 53, p 3603–3611.

    Article  CAS  Google Scholar 

  20. S. Ma, J. Xing, Y. He, Y. Li, Z. Huang, G. Liu, and Q. Geng, Microstructure and Crystallography of M7C3 Carbide in Chromium Cast Iron, Mater. Chem. Phys., 2015, 161, p 65–73.

    Article  CAS  Google Scholar 

  21. Q. Zhou, S. Ping, X. Meng, R. Wang, and Y. Gao, Precipitation Kinetics of M23C6 Carbides in the Super304H Austenitic Heat-Resistant Steel, J. Mater. Eng. Perform., 2017, 26, p 6130–6139.

    Article  CAS  Google Scholar 

  22. C. Zhang, X. Xiong, S. Ping, and Y. Gao, Influence of Chemical Composition on Intergranular Corrosion Susceptibility of Novel Super304H Austenitic Heat-Resistant Steel, Corros. Eng. Sci. Technol., 2014, 49, p 624–632.

    Article  CAS  Google Scholar 

  23. K. Wieczerzak, P. Bala, M. Stepien, G. Cios, and T. Koziel, Formation of Eutectic Carbides in Fe-Cr-Mo-C Alloy During Non-equilibrium Crystallization, Mater. Des., 2016, 94, p 61–68.

    Article  CAS  Google Scholar 

  24. A.L.D.M. Costa, A.C.D.C. Reis, L. Kestens, and M.S. Andrade, Ultra Grain Refinement and Hardening of if-Steel During Accumulative Roll-Bonding, Mater. Sci. Eng. A., 2005, 406, p 279–285.

    Article  Google Scholar 

Download references

Acknowledgment

This work was financially supported by National Nature Science Foundation of China (Nos. 52175325, 51961024, 52071170), Key Research Program of Education Department of Gansu Province (GSSYLXM-03) and the Lanzhou Science and Technology Department Project (2019-1-49).

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to Rui Cao.

Ethics declarations

Conflict of interest

The authors declare that they have no known competing financial interests or personal relationships that could have appeared to influence the work reported in this paper.

Ethical Approval

This article does not contain any studies with human participants or animals performed by any of the authors.

Additional information

Publisher's Note

Springer Nature remains neutral with regard to jurisdictional claims in published maps and institutional affiliations.

Rights and permissions

Reprints and permissions

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Xu, H., Shen, Y., Cao, R. et al. Effect of Different Rolling Passes on Microstructure and Mechanical Properties of M390 Powder Metallurgy High-Speed Steel. J. of Materi Eng and Perform 31, 9650–9659 (2022). https://doi.org/10.1007/s11665-022-06988-x

Download citation

  • Received:

  • Revised:

  • Accepted:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s11665-022-06988-x

Keywords

Navigation