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Effect of Heat Treatment on Microstructure and Mechanical Properties of Extruded Mg-4Zn-1.5Al-2Sn Alloy

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Abstract

The microstructure and mechanical properties of extruded Mg-4Zn-1.5Al-2Sn (ZAT422) alloy under different heat treatments were investigated by optical microscopy, scanning electron microscopy, x-ray diffraction, transmission electron microscopy, micro-hardness tests, and tensile tests. The results show that the as-extruded and heat-treated ZAT422 alloys mainly consisted of α-Mg and Mg2Sn, and no ternary phase was detected. After aging, the amount of secondary phase precipitates increased significantly and the mechanical properties were improved. Among all the heat treatments, T5 heat treatment at 150 °C for 25 h resulted in the best combination of strength and ductility for ZAT422 alloy. The ultimate tensile strength, yield strength, and elongation (εf) were found to be 290, 182 MPa, and 20%, respectively. Based on microstructural characterization, the variations in mechanical properties of the alloy subjected to heat treatment were analyzed in detail.

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References

  1. S. Richmire, K. Hall, and M. Haghshenas, Design of Experiment Study on Hardness Variations in Friction Stir Welding of AM60 Mg Alloy, J. Magnes. Alloys, 2018, 6, p 215–228

    Article  Google Scholar 

  2. B.C. Suh, J.H. Kim, J.H. Bae, J.H. Hwang, M.S. Shim, and N.J. Kim, Effect of Sn Addition on the Microstructure and Deformation Behavior of Mg-3Al Alloy, Acta Mater., 2018, 124, p 268–279

    Article  Google Scholar 

  3. S.Y. Gao, X.H. Chen, F.S. Pan, K. Song, C.Y. Zhao, L.Z. Liu, X.F. Liu, and D. Zhao, Effect of Secondary Phase on the Electromagnetic Shielding Effectiveness of Magnesium Alloy, Sci. Rep., 2018, 8, p 1–14

    Article  Google Scholar 

  4. P. Poddar, A. Kamaraj, A.P. Murugesan, S. Bagui, and K.L. Sahoo, Microstructural Features of Mg-8%Sn Alloy and Its Correlation with Mechanical Properties, J. Magnes. Alloys, 2017, 5, p 348–354

    Article  Google Scholar 

  5. F.S. Pan, J.J. Mao, G. Zhang, A.T. Tang, and J. She, Development of High-Strength, Low-Cost Wrought Mg-2.0 mass% Zn Alloy with High Mn Content, Prog. Nat. Sci.: Mater., 2016, 26, p 630–635

    Article  Google Scholar 

  6. C.Y. Zhao, X.H. Chen, F.S. Pan, J.F. Wang, S.Y. Gao, T. Tu, C.Q. Liu, J.H. Yao, and A. Atrens, Strain Hardening of As-Extruded Mg-x Zn (x = 1, 2, 3 and 4 wt.%) Alloys, J. Mater. Sci. Technol., 2019, 35, p 142–150

    Article  Google Scholar 

  7. D.K. Xu, E.H. Hou, and Y.B. Xu, Effect of Long-period Stacking Ordered Phase on Microstructure, Mechanical Property and Corrosion Resistance of Mg Alloys: A Review, Prog. Nat. Sci.: Mater., 2016, 26, p 117–128

    Article  Google Scholar 

  8. L.Z. Liu, X.H. Chen, J.F. Wang, L.Y. Qiao, S.Y. Gao, K. Song, C.Y. Zhao, X.F. Liu, D. Zhao, and F.S. Pan, Effects of Y and Zn Additions on Electrical Conductivity and Electromagnetic Shielding Effectiveness of Mg-Y-Zn Alloys, J. Mater. Sci. Technol., 2019, 35, p 1074–1080

    Article  Google Scholar 

  9. Y.M. Kim, C. Mendis, T. Sasaki, D. Letzig, F. Pyczak, K. Hono, and S.B. Yi, Static Recrystallization Behaviour of Cold Rolled Mg-Zn-Y Alloy and Role of Solute Segregation in Microstructure Evolution, Scr. Mater., 2017, 136, p 41–45

    Article  Google Scholar 

  10. B. Wang, F.S. Pan, X.H. Chen, W. Guo, and J.J. Mao, Microstructure and Mechanical Properties of As-extruded and As-Aged Mg-Zn-Al-Sn Alloys, Mater. Sci. Eng., A, 2016, 656, p 165–173

    Article  Google Scholar 

  11. G.H. Zhang, J.H. Chen, H.G. Yan, B. Su, X. He, and M. Ran, Effects of Artificial Aging on Microstructure and Mechanical Properties of the Mg-4.5Zn-4.5Sn-2Al alloy, J. Alloys Compd., 2014, 592, p 250–257

    Article  Google Scholar 

  12. B. Wang, X.H. Chen, F.S. Pan, and J.J. Mao, Effects of Sn Addition on Microstructure and Mechanical Properties of Mg-Zn-Al Alloys, Prog. Nat. Sci. Mater., 2017, 27, p 695–702

    Article  Google Scholar 

  13. F.R. Elsayed, T.T. Sasaki, C.L. Mendis, T. Ohkubo, and K. Hono, Compositional Optimization of Mg-Sn-Al Alloys for Higher Age Hardening Response, Mater. Sci. Eng., A, 2013, 566, p 22–29

    Article  Google Scholar 

  14. C.Q. Liu, H.W. Chen, and J.F. Nie, Interphase Boundary Segregation of Zn in Mg-Sn-Zn Alloys, Scr. Mater., 2016, 123, p 5–8

    Article  Google Scholar 

  15. S.H. Park, S.H. Kim, H.S. Kim, J.H. Yoon, and B.S. You, High-speed Indirect Extrusion of Mg-Sn-Al-Zn Alloy and its Influence on Microstructure and Mechanical Properties, J. Alloy. Compd., 2016, 667, p 170–177

    Article  Google Scholar 

  16. T.T. Sasaki, K. Oh-ishi, T. Ohkubo, and K. Hono, Effect of Double Aging and Microalloying on the Age Hardening Behavior of a Mg-Sn-Zn Alloy, Mater. Sci. Eng., A, 2011, 530, p 1–8

    Article  Google Scholar 

  17. L.L. Chang, H. Tang, and J. Guo, Strengthening Effect of Nano and Micro-sized Precipitates in the Hot-extruded Mg-5Sn-3Zn Alloys with Ca Addition, J. Alloy. Compd., 2018, 703, p 552–559

    Article  Google Scholar 

  18. J. She, F. Pan, J. Zhang, A. Tang, S. Luo, Z. Yu, K. Song, and M. Rashad, Microstructure and Mechanical Properties of Mg-Al-Sn Extruded Alloys, J. Alloy. Compd., 2016, 657, p 893–905

    Article  Google Scholar 

  19. H.T. Son, J.B. Lee, H.G. Jeong, and T.J. Konno, Effects of Al and Zn Additions on Mechanical Properties and Precipitation Behaviors of Mg-Sn Alloy System, Mater. Lett., 2011, 65, p 1966–1969

    Article  Google Scholar 

  20. J.F. Nie, X. Gao, and S.M. Zhu, Enhanced Age Hardening Response and Creep Resistance of Mg-Gd Alloys Containing Zn, Scr. Mater., 2005, 53, p 1049–1053

    Article  Google Scholar 

  21. X. Liu, G.Q. Zhao, J.X. Zhou, C.S. Zhang, L. Chen, and S.Q. Tang, Microstructure and Mechanical Properties of Mg-3.0Zn-1.0Sn-0.3Mn-0.3Ca Alloy Extruded at Different Temperatures, J. Alloys Compd., 2018, 732, p 257–269

    Article  Google Scholar 

  22. Z.Z. Shi, J.Y. Xu, J. Yu, and X.F. Liu, Microstructure and Mechanical Properties of As-cast and As-hot-rolled Novel Mg-xSn-2.5Zn-2Al alloys (x = 2, 4 wt.%), Mater. Sci. Eng., A, 2018, 712, p 65–72

    Article  Google Scholar 

  23. X. Gao and J.F. Nie, Characterization of Strengthening Precipitate Phases in a Mg-Zn Alloy, Scr. Mater., 2007, 56, p 645–648

    Article  Google Scholar 

  24. R. Kocich, L. Kunčická, P. Král, and T.C. Lowe, Texture, Deformation Twinning and Hardening in a Newly Developed Mg-Dy-Al-Zn-Zr Alloy Processed with High Pressure Torsion, Mater. Des., 2016, 90, p 1092–1099

    Article  Google Scholar 

  25. L. Kunčická and R. Kocich, Comprehensive Characterisation of a Newly Developed Mg-Dy-Al-Zn-Zr Alloy Structure, Metals, 2018, 8, p 73

    Article  Google Scholar 

  26. R. Kocich, M. Kursa, and A. Macháčková, FEA of Plastic Flow in AZ63 Alloy during ECAP Process, Acta Phys. Polon. A, 2012, 122(3), p 581–587

    Article  Google Scholar 

  27. P. Lukáč, R. Kocich, M. Greger, O. Padalka, and Z. Szaraz, Microstructure of AZ31 and AZ61 Mg Alloys Prepared by Rolling and ECAP, Kovove Mater., 2017, 45, p 115–120

    Google Scholar 

  28. C.Q. Liu, H.W. Chen, H. Liu, X.J. Zhao, and J.F. Nie, Metastable Precipitate Phases in Mg-9.8 wt.%Sn Alloy, Acta Mater., 2018, 144, p 590–600

    Article  Google Scholar 

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Acknowledgment

The authors would like to thank the financial supports from the National Key R&D Program of China (2016YFB0301100), National Natural Science Foundation of China (Projects 51571043, 51675533 and 51701238), and Fundamental Research Funds for the Central Universities (2018CDJDCL0019 and cqu2018CDHB1A08).

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Correspondence to Xianhua Chen.

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Wang, B., Chen, X., Wei, S. et al. Effect of Heat Treatment on Microstructure and Mechanical Properties of Extruded Mg-4Zn-1.5Al-2Sn Alloy. J. of Materi Eng and Perform 28, 4565–4573 (2019). https://doi.org/10.1007/s11665-019-04258-x

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  • DOI: https://doi.org/10.1007/s11665-019-04258-x

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