Skip to main content
Log in

Experimental Study on Microstructure and Hardness of Pure Titanium Subjected to Torsion Deformation at Different Temperatures

  • Published:
Journal of Materials Engineering and Performance Aims and scope Submit manuscript

Abstract

The studies of mechanical property, microstructure evolution and fracture analysis in pure titanium processed by torsion deformation at 298, 673 and 1073 K are conducted systematically. The variations of mechanical property of deformed pure titanium are shown through Vickers hardness evaluation. During torsion at 298 K, the grains are refined and elongated, but the α phase with different shapes precipitates for twisted samples at 673 and 1073 K. The fracture appearance indicates that the elongated dimples occur on fracture surface at 298 K. Besides, a large number of shear facets are arranged. However, typical intergranular fracture appearance with lots of blocks in polyhedral shape covers the fracture surface at 673 and 1073 K, respectively.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Fig. 1
Fig. 2
Fig. 3
Fig. 4
Fig. 5
Fig. 6
Fig. 7
Fig. 8
Fig. 9
Fig. 10

Similar content being viewed by others

References

  1. D. Banerjee and J.C. Williams, Perspectives on Titanium Science and Technology, Acta Mater., 2013, 61(3), p 844–879

    Article  CAS  Google Scholar 

  2. B.R. Chrcanovic and M.D. Martins, Study of the Influence of Acid Etching Treatments on the Superficial Characteristics of Ti, Mater. Res., 2014, 178(17), p 373–380

    Article  Google Scholar 

  3. T.R. Rautray, R. Narayanan, and K.H. Kim, Ion Implantation of Titanium Based Biomaterials, Procedia Mater. Sci., 2011, 56(8), p 1137–1177

    Article  CAS  Google Scholar 

  4. V.V. Stolyarov, Y.T. Zhu, T.C. Lowe, and R.Z. Vali, Microstructure and Properties of Pure Ti Processed by ECAP and Cold Extrusion, Mater. Sci. Eng. A, 2001, 303(1-2), p 82–89

    Article  Google Scholar 

  5. R.Z. Valiev, R.K. Islamgaliev, and I.V. Alexandrov, Bulk Nanostructured Materials from Severe Plastic Deformation, Prog. Mater. Sci., 2000, 45(2), p 103–189

    Article  CAS  Google Scholar 

  6. J.H. Li, F.G. Li, P. Li, Z.C. Ma, C.P. Wang, and L. Wang, Micro-structural Evolution in Metals Subjected to Simple Shear by a Particular Severe Plastic Deformation Method, J. Mater. Eng. Perform., 2015, 24(8), p 2944–2956

    Article  CAS  Google Scholar 

  7. H. Chen, F.G. Li, S.S. Zhou, J.H. Li, C. Zhao, and Q. Wan, Experimental Study on Pure Titanium Subjected to Different Combined Tension and Torsion Deformation Processes, Mater. Sci. Eng. A, 2016, 680, p 278–290

    Article  Google Scholar 

  8. T. Ungár, L.S. Tóth, J. Illy, and I. Kovács, Dislocation Structure and Work Hardening in Polycrystalline OFHC Copper Rods Deformed by Torsion and Tension, Acta Metall., 1986, 34(7), p 1257–1267

    Article  Google Scholar 

  9. A.P. Zhilyaev and T.G. Langdon, Using High-Pressure Torsion for Metal Processing: Fundamentals and Applications, Prog. Mater. Sci., 2008, 53(6), p 893–979

    Article  CAS  Google Scholar 

  10. T. Sakai, A. Belyakov, R. Kaibyshev, H. Miura, and J.J. Jonas, Dynamic and Post-dynamic Recrystallization Under Hot, Cold and Severe Plastic Deformation Conditions, Prog. Mater Sci., 2014, 60(1), p 130–207

    Article  CAS  Google Scholar 

  11. Y.C. Lin, M.S. Chen, and J. Zhong, Constitutive Modeling for Elevated Temperature Flow Behavior of 42CrMo Steel, Comput. Mater. Sci., 2008, 42(3), p 470–477

    Article  CAS  Google Scholar 

  12. S.L. Semiatin, J.F. Thomas, and P. Dadras, Processing-Microstructure Relationships for Ti-6Al-2Sn-4Zr-2Mo-0.1Si, Metall. Trans. A, 1983, 14(11), p 2363–2374

    Article  Google Scholar 

  13. S.V.S.N. Murty, B.N. Rao, and B.P. Kashyap, Instability Criteria for Hot Deformation of Materials, Int. Mater. Rev., 2000, 45(1), p 15–26

    Article  CAS  Google Scholar 

  14. Y.V.R.K. Prasad, T. Seshacharyulu, S.C. Medeiros, W.G. Frazier, and J.C.M. Iii, Hot Deformation Mechanisms in Ti-6Al-4V with Transformed β Starting Microstructure: Commercial Extra Low Interstitial Grade, Mater. Sci. Technol., 2000, 16(9), p 1029–1036

    Article  CAS  Google Scholar 

  15. T. Seshacharyulu, S.C. Medeiros, J.T. Morgan, J.C. Malas, W.G. Frazier, and Y.V.R.K. Prasad, Hot Deformation and Microstructural Damage Mechanisms in Extra-Low Interstitial (ELI) Grade Ti-6Al-4V, Mater. Sci. Eng. A, 2000, 279(1-2), p 289–299

    Article  Google Scholar 

  16. M.J. Luton and C.M. Sellars, Dynamic Recrystallization in Ni and Fe-Ni Alloys During High Temperature Deformation, Acta Metall., 1969, 17(8), p 1033–1043

    Article  CAS  Google Scholar 

  17. W.H.V. Geertruyden, H.M. Browne, W.Z. Misiolek, and P.T. Wang, Evolution of Surface Recrystallization During Indirect Extrusion of 6xxx Aluminum Alloys, Metall. Mater. Trans. A, 2005, 36(4), p 1049–1056

    Article  Google Scholar 

  18. A. Marchattiwar, A. Sarkar, J.K. Chakravartty, and B.P. Kashyap, Dynamic Recrystallization During Hot Deformation of 304 Austenitic Stainless Steel, J. Mater. Eng. Perform., 2013, 22(8), p 2168–2175

    Article  CAS  Google Scholar 

  19. R.L. Xin, X. Zheng, Z. Liu, D.J. Liu, R.S. Qiu, Z.Y. Li, and Q. Liu, Microstructure and Texture Evolution of an Mg-Gd-Y-Nd-Zr Alloy During Friction Stir Processing, J. Alloys Compd., 2015, 659, p 51–59

    Article  Google Scholar 

  20. B. Song, N. Guo, R.L. Xin, H.C. Pan, and C.F. Guo, Strengthening and Toughening of Extruded Magnesium Alloy Rods by Combining Pre-torsion Deformation with Subsequent Annealing, Mater. Sci. Eng. A, 2016, 650, p 300–304

    Article  CAS  Google Scholar 

  21. C.P. Wang, R.L. Xin, D.R. Li, B. Song, M.Y. Wu, and Q. Liu, Enhancing the Age-Hardening Response of Rolled AZ80 Alloy by Pre-twinning Deformation, Mater. Sci. Eng. A, 2016, 680, p 152–156

    Article  Google Scholar 

  22. H. Chen, F.G. Li, J.H. Li, Z. Zhao, S.S. Zhou, and Q. Wan, Experimental Study on Pure Titanium During the Positive-Torsion and Positive-Negative-Torsion, Mater. Sci. Eng. A, 2016, 674, p 552–568

    Article  CAS  Google Scholar 

  23. H. Chen, F.G. Li, J.H. Li, X.K. Ma, J. Li, and Q. Wan, Hardening and Softening Analysis of Pure Titanium Based on the Dislocation Density During Torsion Deformation, Mater. Sci. Eng. A, 2016, 671, p 17–31

    Article  CAS  Google Scholar 

  24. F. Wetscher, A. Vorhauer, and R. Pippan, Strain Hardening During High Pressure Torsion Deformation, Mater. Sci. Eng. A, 2005, 410(12), p 213–216

    Article  Google Scholar 

  25. F. Wetscher, R. Pippan, S. Sturm, F. Kauffmann, C. Scheu, and G. Dehm, TEM Investigations of the Structural Evolution in a Pearlitic Steel Deformed by High-Pressure Torsion, Metall. Mater. Trans. A, 2006, 37(6), p 1963–1968

    Article  Google Scholar 

  26. J.W. Christian and S. Mahajan, Deformation Twinning, Prog. Mater Sci., 1995, 39(1), p 1–157

    Article  Google Scholar 

  27. T. Gloriant, G. Texier, F. Sun, I. Thibon, F. Prima, and J.L. Soubeyroux, Characterization of Nanophase Precipitation in a Metastable β Titanium-Based Alloy by Electrical Resistivity, Dilatometry and Neutron Diffraction, Scripta Mater., 2008, 58(4), p 271–274

    Article  CAS  Google Scholar 

  28. U. Bathini, T.S. Srivatsan, A. Patnaik, and T. Quick, Deformation and Fracture Behavior of Commercially Pure Titanium And Titanium Alloy: Influence of Orientation and Microstructure, J. Mater. Eng. Perform., 2010, 19(8), p 1172–1182

    Article  CAS  Google Scholar 

Download references

Acknowledgment

This work was supported by the National Natural Science Foundation of China (Grant No. 51275414); and the Aeronautical Science Foundation of China (Grant No. 2011ZE53059).

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to Han Chen.

Additional information

Publisher's Note

Springer Nature remains neutral with regard to jurisdictional claims in published maps and institutional affiliations.

Rights and permissions

Reprints and permissions

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Liu, J., Chen, H. Experimental Study on Microstructure and Hardness of Pure Titanium Subjected to Torsion Deformation at Different Temperatures. J. of Materi Eng and Perform 28, 4790–4800 (2019). https://doi.org/10.1007/s11665-019-04247-0

Download citation

  • Received:

  • Revised:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s11665-019-04247-0

Keywords

Navigation