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Effect of Aging Treatment on the Precipitation Behavior and Mechanical Properties of Mg-9Gd-3Y-1.5Zn-0.5Zr Alloy

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Abstract

Aging heat treatments of an extruded Mg-9Gd-3Y-1.5Zn-0.5Zr (wt.%) alloy at 200, 225, and 250 °C for various times were studied. The results show that dynamic recrystallization (DRX) occurred during the extrusion process and the alloy exhibited a significant aging hardening response at temperatures ranging from 200 to 225 °C. The precipitation sequence of the alloy at 225 °C was supersaturated solid solution (SSSS) → β″ (D019, Mg3RE) → β′ (bco, Mg15RE3), where the β′ phase was the primary precipitated phase. A large amount of discontinuous lamellar-shaped 14H-structure long period stacking ordered (LPSO) phase was also observed in the α-Mg matrix before and after aging treatments. Owing to the combined strengthening effect of fine DRXed grains, β′ nanoparticles, and widespread LPSO phases, the ultimate tensile strength and tensile yield strength of the peak-aged extruded alloy reached 409 and 303 MPa, respectively. The elongation in this circumstance was ~7.1%, which was slightly lower than that of the alloy before aging treatment.

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References

  1. Y. Kawamura, K. Hayashi, A. Inoue, and T. Masumoto, Rapidly Solidified Powder Metallurgy Mg97Zn1Y2 Alloys with Excellent Tensile Yield Strength above 600 MPa, Mater. Trans., 2001, 42(7), p 1172–1176

    Article  Google Scholar 

  2. Q. Wang, J. Chen, Z. Zhao, and S.M. He, Microstructure and Super High Strength of Cast Mg-8.5Gd-2.3Y-1.8Ag-0.4Zr Alloy, Mater. Sci. Eng. A, 2010, 528, p 323–328

    Article  Google Scholar 

  3. Y.K. Kim, S.W. Sohn, D.H. Kim, W.T. Kim, and D.H. Kim, Role of Icosahedral Phase in Enhancing the Strength of Mg-Sn-Zn-Al Alloy, J. Alloys Compd., 2013, 549, p 46–50

    Article  Google Scholar 

  4. L.L. Rohklin and N.I. Nikitina, Magnesium-Gadolinium and Magnesium Gadolinium-Yttrium Alloys, Z. Metallkd., 1994, 85, p 819–823

    Google Scholar 

  5. X. Li, W. Qi, K. Zheng, and N. Zhou, Enhanced Strength and Ductility of Mg-Gd-Y-Zr Alloys by Secondary Extrusion, J. Magnes. Alloys, 2013, 1, p 54–63

    Article  Google Scholar 

  6. C. Xu, M.Y. Zheng, K. Wu, E.D. Wang, G.H. Fan, S.W. Xu, S. Kamado, X.D. Liu, and G.J. Wang, Effect of Aging Treatment on the Precipitation Behavior of Mg-Gd-Y-Zn-Zr Alloy, J. Alloys Compd., 2013, 550, p 50–56

    Article  Google Scholar 

  7. D. Griffiths, Explaining Texture Weakening and Improved Formability in Magnesium Rare Earth Alloys, Mater. Sci. Technol., 2015, 31(1), p 10–24

    Article  Google Scholar 

  8. M. Yamasaki, T. Anan, S. Yoshimoto, and Y. Kawamura, Mechanical Properties of Warm-Extruded Mg–Zn–Gd Alloy with Coherent 14H Long Periodic Stacking Ordered Structure Precipitate, Scripta Mater., 2005, 53, p 799–803

    Article  Google Scholar 

  9. Z. Yang, J.P. Li, Y.C. Guo, T. Liu, F. Xia, Z.W. Zeng, and M.X. Liang, Precipitation Process and Effect on Mechanical Properties of Mg-9Gd-3Y-0.6Zn-0.5Zr Alloy, Mater. Sci. Eng. A, 2007, 454–455, p 274–280

    Article  Google Scholar 

  10. S. Yoshimoto, M. Yamasaki, and Y. Kawamura, Microstructure and Mechanical Properties of Extruded Mg-Zn-Y Alloys with 14H Long Period Ordered Structure, Mater. Trans., 2006, 47, p 959–965

    Article  Google Scholar 

  11. W.Y. Wang, S.L. Shang, Y. Wang, K.A. Darling, L.J. Kecskes, S.N. Mathaudhu, X.D. Hui, and Z.K. Liu, Electronic Structures of Long Periodic Stacking Order Structures in Mg: A First-Principles Study, J. Alloys Compd., 2014, 586, p 656–662

    Article  Google Scholar 

  12. X. Liu, Q.C. Le, Z.Q. Zhang, L. Bao, Z.X. Fan, and J.Z. Cui, Effects of Casting Process on Microstructures and Flow Stress Behavior of Mg-9Gd-3Y-1.5Zn-0.8Zr, J. Magnes. Alloys, 2014, 2, p 342–348

    Article  Google Scholar 

  13. C. Xu, M.Y. Zheng, K. Wu, E.D. Wang, G.H. Fan, S.W. Xu, S. Kamado, X.D. Liu, G.J. Wang, and X.Y. Lv, Effect of Cooling Rate on the Microstructure Evolution and Mechanical Properties of Homogenized Mg-Gd-Y-Zn-Zr Alloy, Mater. Sci. Eng. A, 2013, 559, p 364–370

    Article  Google Scholar 

  14. M. Yamasaki, K. Hagihara, S. Inoue, J.P. Hadorn, and Y. Kawamura, Crystallographic Classification of Kink Bands in an Extruded Mg-Zn-Y Alloy Using Intragranular Misorientation Axis Analysis, Acta Mater., 2013, 61, p 2065–2076

    Article  Google Scholar 

  15. T. Honma, T. Ohkubo, S. Kamado, and K. Hono, Effect of Zn Additions on the Age-Hardening of Mg-2.0Gd-1.2Y-0.2Zr Alloy, Acta Mater., 2007, 55, p 4137–4150

    Article  Google Scholar 

  16. J.F. Nie, Y.M. Zhu, and A.J. Morton, On the Structure, Transformation and Deformation of Long-Period Stacking Ordered Phase in Mg-Y-Zn Alloys, Met. Mater. Trans. A, 2014, 45A, p 3338–3348

    Article  Google Scholar 

  17. F.M. Lu, A.B. Ma, J.H. Jiang, D.H. Yang, and Q. Zhou, Review on Long-Period Stacking-Ordered Structures in Mg-Zn-RE Alloys, Rare Met., 2012, 31(3), p 303–310

    Article  Google Scholar 

  18. T. Honma, T. Ohkubo, and K. Hono, Chemistry of Nanoscale Precipitates in Mg-2.1Gd-0.6Y-0.2Zr (at.%) Alloy Investigated by the Atom Probe Technique, Mater. Sci. Eng. A, 2005, 395, p 301–306

    Article  Google Scholar 

  19. Z.Q. Wang, B. Zhang, D.J. Li, R. Fritsch, X.Q. Zeng, H.J. Roven, and W.J. Ding, Effect of Heat Treatment on Microstructures and Mechanical Properties of High Vacuum Die Casting Mg-8Gd-3Y-0.4Zr Magnesium Alloy, Trans. Nonferr. Met. Soc. China, 2014, 24, p 3762–3768

    Article  Google Scholar 

  20. J.H. Li, J. Barrirero, G. Sha, H. Aboulfadl, F. Muchlich, and P. Schumacher, Precipitation Hardening of an Mg-5Zn-2Gd-0.4Zr (wt.%) Alloy, Acta Mater., 2016, 108, p 207–218

    Article  Google Scholar 

  21. J.F. Nie, Precipitation and Hardening in Magnesium alloys, Met. Mater. Trans. A, 2012, 43A, p 3891–3939

    Article  Google Scholar 

  22. C. Xu, M.Y. Zheng, K. Wu, E.D. Wang, G.H. Fan, S.W. Xu, S. Kamado, X.D. Liu, G.J. Wang, and X.Y. Lv, Influence of Rolling Temperature on the Microstructure and Mechanical Properties of Mg-Gd-Y-Zn-Zr Alloy Sheets, Mater. Sci. Eng. A, 2013, 559, p 615–622

    Article  Google Scholar 

  23. C. Antion, P. Donnadieu, F. Perrard, A. Deschamps, C. Tassin, and A. Pisch, Hardening Precipitation in a Mg-4Y-3RE Alloy, Acta Mater., 2003, 51, p 5335–5348

    Article  Google Scholar 

Download references

Acknowledgments

This work is supported by the Program for New Century Excellent Talents in University (NCET-12-0849) and the Fundamental Research Funds for the Central Universities (2014ZZD03) and Youth Science Fund Project of National Natural Science Fund of China (51401070).

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Correspondence to Zhiyong Xue.

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Xue, Z., Ren, Y., Luo, W. et al. Effect of Aging Treatment on the Precipitation Behavior and Mechanical Properties of Mg-9Gd-3Y-1.5Zn-0.5Zr Alloy. J. of Materi Eng and Perform 26, 5963–5972 (2017). https://doi.org/10.1007/s11665-017-2755-y

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  • DOI: https://doi.org/10.1007/s11665-017-2755-y

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