Skip to main content
Log in

Dependence of Microstructure on Solution and Aging Treatment for Near-β Forged TA15 Ti-Alloy

  • Published:
Journal of Materials Engineering and Performance Aims and scope Submit manuscript

Abstract

For TA15 Ti-alloy, a tri-modal microstructure was obtained via near-β forging combined with solution and aging treatment (SAT) with a short time of air cooling (AC) during forgings transferring before water quenching (WQ). The influence of SAT conditions on final microstructures via 970 °C/0.1 s−1/60%/(AC + WQ) and SAT was investigated. Solution temperature determined the proportion of α and β phases and mainly affected the volume fraction of secondary lamellar α. Solution time mainly influenced the morphology of secondary lamellar α. Solution cooling method was the main factor affecting the thickness of lamellar α. Lower cooling rate resulted in more and thicker lamellar α. Aging treatment had little influence on the volume fraction, size, and morphology of each phase in the microstructure. The main function of aging treatment was to homogenize and stabilize the microstructure. The volume fraction and thickness of lamellar α were increased, and the distribution homogeneity became better during aging. Under the given forging condition, the reasonable solution and aging conditions to obtain tri-modal microstructure were determined as 930 °C/1~2 h/AC + 550~600 °C/5 h/AC.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Fig. 1
Fig. 2
Fig. 3
Fig. 4
Fig. 5
Fig. 6
Fig. 7
Fig. 8
Fig. 9
Fig. 10
Fig. 11
Fig. 12
Fig. 13
Fig. 14

Similar content being viewed by others

References

  1. C. Wu, H. Yang, and H.W. Li, Simulated and Experimental Investigation on Discontinuous Dynamic Recrystallization of a Near-α TA15 Titanium Alloy During Isothermal Hot Compression in β Single-Phase Field, Trans. Nonferrous Met. Soc. China, 2014, 24(6), p 1819–1829

    Article  Google Scholar 

  2. Z.C. Sun, L. Liu, and H. Yang, Microstructure Evolution of Different Loading Zones During TA15 Alloy Multi-Cycle Isothermal Local Forging, Mater. Sci. Eng. A, 2011, 528(15), p 5112–5121

    Article  Google Scholar 

  3. Y.G. Zhou, W.D. Zeng, and H.Q. Yu, An Investigation of a New Near-Beta Forging Process for Titanium Alloys and its Application in Aviation Components, Mater. Sci. Eng. A, 2005, 393(1-2), p 204–212

    Article  Google Scholar 

  4. G.E. Totten and D.S. MacKenzie, Handbook of Aluminum: Vol. 1: Physical Metallurgy and Processes, CRC Press, Boca Raton, 2003

    Book  Google Scholar 

  5. J.C. Zhu, Y. Wang, Y. Liu, Z.H. Lai, and J.J. Zhan, Influence of Deformation Parameters on Microstructure and Mechanical Properties of TA15 Titanium Alloy, Trans. Nonferrous Met. Soc. China, 2007, S1, p 490–494

    Google Scholar 

  6. X.G. Fan, H. Yang, and P.F. Gao, Prediction of Constitutive Behavior and Microstructure Evolution in Hot Deformation of TA15 Titanium Alloy, Mater. Des., 2013, 51, p 34–42

    Article  Google Scholar 

  7. X.G. Fan, H. Yang, S.L. Yan, and J.H. Zhou, Mechanism and Kinetics of Static Globularization in TA15 Titanium Alloy with Transformed Structure, J. Alloy. Compd., 2012, 533, p 1–8

    Article  Google Scholar 

  8. J.W. Xu, W.D. Zeng, Z.Q. Jia, X. Sun, and J.H. Zhou, Microstructure Coarsening Behavior of Ti-17 Alloy with Equiaxed Alpha During Heat Treatment, J. Alloy. Compd., 2015, 618, p 343–348

    Article  Google Scholar 

  9. X.G. Fan, H. Yang, P.F. Gao, and S.L. Yan, Dependence of Microstructure Morphology on Processing in Subtransus Isothermal Local Loading Forming of TA15 Titanium Alloy, Mater. Sci. Eng. A, 2012, 546, p 46–52

    Article  Google Scholar 

  10. D. He, J.C. Zhu, S. Zaefferer, D. Raabe, Y. Liu, Z.L. Lai, and X.W. Yang, Influences of Deformation Strain, Strain Rate and Cooling Rate on the Burgers Orientation Relationship and Variants Morphology During β→α Phase Transformation in a Near α Titanium Alloy, Mater. Sci. Eng. A, 2012, 549, p 20–29

    Article  Google Scholar 

  11. Z.C. Sun, X.Q. Wang, J. Zhang, and H. Yang, Prediction and Control of Equiaxed α in Near-β Forging of TA15 Ti-Alloy Based on BP Neural Network: For Purpose of Tri-Modal Microstructure, Mater. Sci. Eng. A, 2014, 591, p 18–25

    Article  Google Scholar 

  12. J.C. Zhu, D. He, X.W. Yang, and Y. Liu, EBSD Study on Dual Heat Treatment and Microstructure Evolution of TA15 Titanium Alloy, Rare Met. Mater. Eng., 2013, 02, p 382–386 (in Chinese)

    Google Scholar 

  13. Second Editing Office of China standards Press, Test methods for mechanical properties and processing performance of metal, China Standards Press, Xinhua, 2001 (in Chinese)

    Google Scholar 

  14. Y.F. Lv, X.J. Meng, S.K. Li, and W. Yu, Effects of Annealing Heat Treatment on Microstructure and Properties of TA15 Titanium Alloy, Dev. Appl. Mater., 2009, 5, p 7–11 (in Chinese)

    Google Scholar 

  15. Z.C. Sun, S.S. Guo, and H. Yang, Nucleation and Growth Mechanism of α-Lamellae of Ti Alloy TA15 Cooling from An α+β Phase Field, Acta Mater., 2013, 61(6), p 2057–2064

    Article  Google Scholar 

  16. S. Zhu, H. Yang, L.G. Guo, and X.G. Fan, Effect of Cooling Rate on Microstructure Evolution During α/β Heat Treatment of TA15 Titanium Alloy, Mater. Charact., 2012, 70, p 101–110

    Article  Google Scholar 

  17. W.F. Zhang, Y.H. Wang, Y. Li, and J.M. Ma, Phase Transformation, Microstructures and Tensile Properties of TA15 Titanium Alloy, Trans. Nonferrous Met. Soc. China, 2010, 20(S1), p 523–527 (in Chinese)

    Google Scholar 

  18. R. Filip, K. Kubiak, W. Ziaja, and J. Sieniawski, The Effect of Microstructure on the Mechanical Properties of Two-Phase Titanium Alloys, J. Mater. Process. Tech., 2003, 133, p 84–89

    Article  Google Scholar 

  19. G. Lütjering, Influence of Processing on Microstructure and Mechanical Properties of (α+β) Titanium Alloys, Mater. Sci. Eng. A, 1998, 243(112), p 32–45

    Article  Google Scholar 

Download references

Acknowledgments

The authors would like to gratefully acknowledge the supports of the National Natural Science Foundation of China(51275560), Research Fund of the State Key Laboratory of Solidification Processing (NWPU) (156-QP-2016), the 111 Project (B08040), and EU Marie Curie Actions-MatProFuture Project (FP7-PEOPLE-2012-IRSES-318968).

Author information

Authors and Affiliations

Authors

Corresponding authors

Correspondence to Zhichao Sun or He Yang.

Rights and permissions

Reprints and permissions

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Sun, Z., Wu, H., Ma, X. et al. Dependence of Microstructure on Solution and Aging Treatment for Near-β Forged TA15 Ti-Alloy. J. of Materi Eng and Perform 25, 4549–4560 (2016). https://doi.org/10.1007/s11665-016-2282-2

Download citation

  • Received:

  • Revised:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s11665-016-2282-2

Keywords

Navigation