Abstract
For TA15 Ti-alloy, a tri-modal microstructure was obtained via near-β forging combined with solution and aging treatment (SAT) with a short time of air cooling (AC) during forgings transferring before water quenching (WQ). The influence of SAT conditions on final microstructures via 970 °C/0.1 s−1/60%/(AC + WQ) and SAT was investigated. Solution temperature determined the proportion of α and β phases and mainly affected the volume fraction of secondary lamellar α. Solution time mainly influenced the morphology of secondary lamellar α. Solution cooling method was the main factor affecting the thickness of lamellar α. Lower cooling rate resulted in more and thicker lamellar α. Aging treatment had little influence on the volume fraction, size, and morphology of each phase in the microstructure. The main function of aging treatment was to homogenize and stabilize the microstructure. The volume fraction and thickness of lamellar α were increased, and the distribution homogeneity became better during aging. Under the given forging condition, the reasonable solution and aging conditions to obtain tri-modal microstructure were determined as 930 °C/1~2 h/AC + 550~600 °C/5 h/AC.
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References
C. Wu, H. Yang, and H.W. Li, Simulated and Experimental Investigation on Discontinuous Dynamic Recrystallization of a Near-α TA15 Titanium Alloy During Isothermal Hot Compression in β Single-Phase Field, Trans. Nonferrous Met. Soc. China, 2014, 24(6), p 1819–1829
Z.C. Sun, L. Liu, and H. Yang, Microstructure Evolution of Different Loading Zones During TA15 Alloy Multi-Cycle Isothermal Local Forging, Mater. Sci. Eng. A, 2011, 528(15), p 5112–5121
Y.G. Zhou, W.D. Zeng, and H.Q. Yu, An Investigation of a New Near-Beta Forging Process for Titanium Alloys and its Application in Aviation Components, Mater. Sci. Eng. A, 2005, 393(1-2), p 204–212
G.E. Totten and D.S. MacKenzie, Handbook of Aluminum: Vol. 1: Physical Metallurgy and Processes, CRC Press, Boca Raton, 2003
J.C. Zhu, Y. Wang, Y. Liu, Z.H. Lai, and J.J. Zhan, Influence of Deformation Parameters on Microstructure and Mechanical Properties of TA15 Titanium Alloy, Trans. Nonferrous Met. Soc. China, 2007, S1, p 490–494
X.G. Fan, H. Yang, and P.F. Gao, Prediction of Constitutive Behavior and Microstructure Evolution in Hot Deformation of TA15 Titanium Alloy, Mater. Des., 2013, 51, p 34–42
X.G. Fan, H. Yang, S.L. Yan, and J.H. Zhou, Mechanism and Kinetics of Static Globularization in TA15 Titanium Alloy with Transformed Structure, J. Alloy. Compd., 2012, 533, p 1–8
J.W. Xu, W.D. Zeng, Z.Q. Jia, X. Sun, and J.H. Zhou, Microstructure Coarsening Behavior of Ti-17 Alloy with Equiaxed Alpha During Heat Treatment, J. Alloy. Compd., 2015, 618, p 343–348
X.G. Fan, H. Yang, P.F. Gao, and S.L. Yan, Dependence of Microstructure Morphology on Processing in Subtransus Isothermal Local Loading Forming of TA15 Titanium Alloy, Mater. Sci. Eng. A, 2012, 546, p 46–52
D. He, J.C. Zhu, S. Zaefferer, D. Raabe, Y. Liu, Z.L. Lai, and X.W. Yang, Influences of Deformation Strain, Strain Rate and Cooling Rate on the Burgers Orientation Relationship and Variants Morphology During β→α Phase Transformation in a Near α Titanium Alloy, Mater. Sci. Eng. A, 2012, 549, p 20–29
Z.C. Sun, X.Q. Wang, J. Zhang, and H. Yang, Prediction and Control of Equiaxed α in Near-β Forging of TA15 Ti-Alloy Based on BP Neural Network: For Purpose of Tri-Modal Microstructure, Mater. Sci. Eng. A, 2014, 591, p 18–25
J.C. Zhu, D. He, X.W. Yang, and Y. Liu, EBSD Study on Dual Heat Treatment and Microstructure Evolution of TA15 Titanium Alloy, Rare Met. Mater. Eng., 2013, 02, p 382–386 (in Chinese)
Second Editing Office of China standards Press, Test methods for mechanical properties and processing performance of metal, China Standards Press, Xinhua, 2001 (in Chinese)
Y.F. Lv, X.J. Meng, S.K. Li, and W. Yu, Effects of Annealing Heat Treatment on Microstructure and Properties of TA15 Titanium Alloy, Dev. Appl. Mater., 2009, 5, p 7–11 (in Chinese)
Z.C. Sun, S.S. Guo, and H. Yang, Nucleation and Growth Mechanism of α-Lamellae of Ti Alloy TA15 Cooling from An α+β Phase Field, Acta Mater., 2013, 61(6), p 2057–2064
S. Zhu, H. Yang, L.G. Guo, and X.G. Fan, Effect of Cooling Rate on Microstructure Evolution During α/β Heat Treatment of TA15 Titanium Alloy, Mater. Charact., 2012, 70, p 101–110
W.F. Zhang, Y.H. Wang, Y. Li, and J.M. Ma, Phase Transformation, Microstructures and Tensile Properties of TA15 Titanium Alloy, Trans. Nonferrous Met. Soc. China, 2010, 20(S1), p 523–527 (in Chinese)
R. Filip, K. Kubiak, W. Ziaja, and J. Sieniawski, The Effect of Microstructure on the Mechanical Properties of Two-Phase Titanium Alloys, J. Mater. Process. Tech., 2003, 133, p 84–89
G. Lütjering, Influence of Processing on Microstructure and Mechanical Properties of (α+β) Titanium Alloys, Mater. Sci. Eng. A, 1998, 243(112), p 32–45
Acknowledgments
The authors would like to gratefully acknowledge the supports of the National Natural Science Foundation of China(51275560), Research Fund of the State Key Laboratory of Solidification Processing (NWPU) (156-QP-2016), the 111 Project (B08040), and EU Marie Curie Actions-MatProFuture Project (FP7-PEOPLE-2012-IRSES-318968).
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Sun, Z., Wu, H., Ma, X. et al. Dependence of Microstructure on Solution and Aging Treatment for Near-β Forged TA15 Ti-Alloy. J. of Materi Eng and Perform 25, 4549–4560 (2016). https://doi.org/10.1007/s11665-016-2282-2
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DOI: https://doi.org/10.1007/s11665-016-2282-2