Abstract
The present study aimed to characterizing the microstructure evolution of a Ti-6Al-7Nb biomedical type titanium alloy during hot working through hot compression tests. The hot deformation cycles were conducted under the strain rate of 0.0025, 0.025, and 0.25 s−1 in the temperature range of 850-1150 °C where both dual-phase (α + β) and single-phase (β) regions could be accessible. The flow stress behavior of the material for the entire deformation regime was interpreted via microstructural observations. The results indicated that in the single-phase β region (1050-1150 °C), the dynamically recrystallized (DRX) grains were formed at the deformed and elongated beta grain boundaries as a necklace-like structure. The variations in the dynamically recrystallized grain size were determined to follow the Zener-Hollomon relationship where DRX grain size was decreased by reducing the temperature and increasing the strain rate. The alloy deformation characteristics in α + β region were somewhat different. During deformation in the upper α + β temperature range (e.g., 1000 °C), the β phase would accommodate most of the deformation, while α regions remained undeformed. In the lower α + β temperature range (e.g., 850-950 °C), the kinking/bending of α lamellae as well as the subsequent globularization of α layers were postulated to be responsible for the observed flow softening behavior.
Similar content being viewed by others
References
S.L. Semiatin, V. Seetharaman, and I. Weiss, Flow Behavior and Globularization Kinetics During Hot Working of Ti–6Al–4V with a Colony Alpha Microstructure, Mater. Sci. Eng. A, 1999, 263, p 257–271
Y. Han, W. Zeng, Y. Qi, and Y. Zhao, Optimization of Forging Process Parameters of Ti600 Alloy by Using Processing Map, Mater. Sci. Eng. A., 2011, 529, p 393–400
Y. Zong, D.B. Shan, and Y. Lu, Microstructural Evolution of a Ti-4.5 Al-3Mo-1V Alloy During Hot Working, J. Mater. Sci., 2006, 41, p 3753–3760
Y.V.R.K. Prasad, T. Seshacharyulu, S.C. Medeiros, and W.G. Frazier, Influence of Oxygen Content on the Forging Response of Equiaxed (α + β) Preform of Ti–6Al–4V: Commercial vs. ELI, Grade, Eng. Mater. Technol., 2001, 123, p 355–360
R. Ding, Z.X. Guo, and A. Wilson, Microstructural Evolution of a Ti–6Al–4V Alloy During Thermomechanical Processing, Mater. Sci. Eng. A, 2002, 327, p 233–245
J.F. Uginet, Titanium’92 Science and Technology, F.H. Froes and I. Caplan, Ed., TMS, Warrendale, 1993, p 463–471
P.J. Postans and R.H. Jeal, Titanium’80 Science and Technology, H. Kimura and O. Izuma, Ed., AIME, Kyoto, 1980, p 441–455
F. Ma, W. Lu, J. Qin, and D. Zhang, Microstructure Evolution of Near-α Titanium Alloy During Thermomechanical Processing, Mater. Sci. Eng. A, 2006, 416, p 59–65
M. Jackson, R. Dashwood, H. Flower, and V. Christodoulou, The Microstructural Evolution of Near Beta Alloy Ti-10V-2Fe-3Al During Subtransus Forging, Metal. Mater. Trans. A, 2005, 36, p 1317–1327
X. Ma, W. Zeng, F. Tian, Y. Zhou, and Y. Sun, Optimization of Hot Process Parameters of Ti–6.7 Al–2Sn–2.2 Zr–2.1 Mo–1W–0.2 Si Alloy with Lamellar Starting Microstructure Based on the Processing Map, Mater. Sci. Eng. A, 2012, 545, p 132–138
F. Pilehva, A. Zarei-Hanzaki, M. Ghambari, and H.R. Abedi, Flow Behavior Modeling of a Ti–6Al–7Nb Biomedical Alloy During Manufacturing at Elevated Temperatures, Mater. Des., 2013, 51, p 457–465
B. Liu, Y.P. Li, H. Matsumoto, Y.B. Liu, Y. Liu, and A. Chiba, Thermomechanical Characterization of P/M Ti–Fe–Mo–Y Alloy with a Fine Lamellar Microstructure, Mater. Sci. Eng. A, 2011, 528, p 2345–2352
T. Seshacharyulu, S.C. Medeiros, J.T. Morgan, J.C. Malas, W.G. Frazier, and Y.V.R.K. Prasad, Hot Deformation and Microstructural Damage Mechanisms in Extra-Low Interstitial (ELI) Grade Ti–6Al–4V, Mater. Sci. Eng. A, 2000, 279, p 289–299
L.J. Huang, L. Geng, A.B. Li, X.P. Cui, H.Z. Li, and G.S. Wang, Characteristics of Hot Compression Behavior of Ti–6.5 Al–3.5 Mo–1.5 Zr–0.3 Si Alloy with an Equiaxed Microstructure, Mater. Sci. Eng. A, 2009, 505, p 136–143
Y. Zong, D.B. Shan, M. Xu, and Y. Lu, Flow Softening and Microstructural Evolution of TC11 Titanium Alloy During Hot Deformation, J. Mater. Process. Technol., 2009, 209, p 1988–1994
M.F. López, A. Gutiérrez, and J.A. Jiménez, In Vitro Corrosion Behavior of Titanium Alloys Without Vanadium, Electrochim. Acta, 2002, 47, p 1359–1364
X. Liu, P.K. Chu, and C. Ding, Surface Modification of Titanium, Titanium Alloys, and Related Materials for Biomedical Applications, Mater. Sci. Eng. R, 2004, 47, p 49–121
W.F. Cui, Z. Jin, A.H. Guo, and L. Zhou, High Temperature Deformation Behavior of α + β-type Biomedical Titanium Alloy Ti–6Al–7Nb, Mater. Sci. Eng. A, 2009, 499, p 252–256
Y. Liu, Y. Ning, Z. Yao, and H. Guo, Hot Deformation Behavior of Ti–6.0Al–7.0Nb Biomedical Alloy by Using Processing Map, J. Alloy Compd., 2014, 587, p 183–189
T. Akahori, M. Niinomi, K.I. Fukunaga, and I. Inagaki, Effects of Microstructure on the Short Fatigue Crack Initiation and Propagation Characteristics of Biomedical α/β Titanium Alloys, Metall. Mater. Trans. A, 2000, 31A, p 1949–1958
P. Vo, M. Jahazi, and S. Yue, Recrystallization During Thermomechanical Processing of IMI834, Metal. Mater. Trans. A., 2008, 39A, p 2965–2980
B. Appolaire, L. Héricher, and E. Aeby-Gautier, Modelling of Phase Transformation Kinetics in Ti Alloys–Isothermal Treatments, Acta Mater., 2005, 53, p 3001–3011
P. Wanjara, M. Jahazi, H. Monajati, and S. Yue, Influence of Thermomechanical Processing on Microstructural Evolution in Near-α Alloy IMI834, Mater. Sci. Eng. A, 2006, 416, p 300–311
I. Weiss and S.L. Semiatin, Thermomechanical Processing of Beta Titanium Alloys—An Overview, Mater. Sci. Eng. A, 1998, 243, p 46–65
M. Jafari and A. Najafizadeh, Correlation Between Zener-Hollomon Parameter and Necklace DRX During Hot Deformation of 316 Stainless Steel, Mater. Sci. Eng. A, 2009, 501, p 16–25
W. Jia, W. Zeng, J. Liu, Y. Zhou, and Q. Wang, On the Influence of Processing Parameters on Microstructural Evolution of a Near Alpha Titanium Alloy, Mater. Sci. Eng. A, 2011, 530, p 135–143
W. Peng, W. Zeng, Q. Wang, Q. Zhao, and H. Yu, Effect of Processing Parameters on Hot Deformation Behavior and Microstructural Evolution During Hot Compression of as-Cast Ti60 Titanium Alloy, Mater. Sci. Eng. A, 2014, 593, p 16–23
Y. Han, W. Zeng, Y. Qi, and Y. Zhao, The Influence of Thermomechanical Processing on Microstructural Evolution of Ti600 Titanium Alloy, Mater. Sci. Eng. A., 2011, 528, p 8410–8416
F. Humphreys and M. Hatherly, Recrystallization and Related Annealing Phenomena, 2nd ed., Elsevier, Oxford, 2004
X.G. Fan, H. Yang, and P.F. Gao, Deformation Behavior and Microstructure Evolution in Multistage Hot Working of TA15 Titanium Alloy: on the Role of Recrystallization, J. Mater. Sci., 2011, 46, p 6018–6028
S. Roy and S. Suwas, The Influence of Temperature and Strain Rate on the Deformation Response and Microstructural Evolution During Hot Compression of a Titanium Alloy Ti–6Al–4V–0.1B, J. Alloy Compd., 2013, 548, p 110–125
T. Seshacharyulu, S.C. Medeiros, J.T. Morgan, J.C. Malas, W.G. Frazier, and Y.V.R.K. Prasad, Hot Deformation Mechanisms in ELI, Grade Ti-6A1-4V, Scr. Mater., 1999, 41, p 283–288
S.V. Zherebtsov, M.A. Murzinova, M.V. Klimova, G.A. Salishchev, A.A. Popov, and S.L. Semiatin, Microstructure Evolution During Warm Working of Ti–5Al–5Mo–5 V–1Cr–1Fe at 600 and 800 C, Mater. Sci. Eng. A, 2013, 563, p 168–176
S. Roy, A. Sarkar, and S. Suwas, On Characterization of Deformation Microstructure in Boron Modified Ti–6Al–4V Alloy, Mater. Sci. Eng. A, 2010, 528, p 449–458
C. Li, X.Y. Zhang, K.C. Zhou, and C.Q. Peng, Relationship Between Lamellar α Evolution and Flow Behavior During Isothermal Deformation of Ti–5Al–5Mo–5 V–1Cr–1Fe Near β Titanium Alloy, Mater. Sci. Eng. A, 2012, 558, p 668–674
S. Zherebtsov, M. Murzinova, G. Salishchev, and S.L. Semiatin, Spheroidization of the Lamellar Microstructure in Ti–6Al–4 V Alloy During Warm Deformation and Annealing, Acta Mater., 2011, 59, p 4138–4150
I. Weiss, F.H. Froes, D. Eylon, and G.E. Welsch, Modification of Alpha Morphology in Ti-6Al-4 V by Thermomechanical Processing, Metall. Trans., 1986, 17A, p 1935–1947
H.W. Song, S.H. Zhang, and M. Cheng, Dynamic Globularization Kinetics During Hot Working of a Two Phase Titanium Alloy with a Colony Alpha Microstructure, J. Alloy Compd., 2009, 480, p 922–927
X. Ma, W. Zeng, F. Tian, and Y. Zhou, The Kinetics of Dynamic Globularization During Hot Working of a Two Phase Titanium Alloy with Starting Lamellar Microstructure, Mater. Sci. Eng. A, 2012, 548, p 6–11
B. Poorganji, M. Yamaguchi, Y. Itsumi, K. Matsumoto, T. Tanaka, Y. Asa, G. Miyamoto, and T. Furuhara, Microstructure Evolution During Deformation of a Near-α Titanium Alloy with Different Initial Structures in the Two-Phase Region, Scr. Mater., 2009, 61, p 419–422
L. Lei, X. Huang, M. Wang, L. Wang, J. Qin, and S. Lu, Effect of Temperature on Deformation Behavior and Microstructures of TC11 Titanium Alloy, Mater. Sci. Eng. A, 2011, 528, p 8236–8243
T. Seshacharyulu, S.C. Medeiros, W.G. Frazier, and Y.V.R.K. Prasad, Hot Working of Commercial Ti–6Al–4V with an Equiaxed α–β Microstructure: Materials Modeling Considerations, Mater. Sci. Eng. A, 2000, 279, p 184–194
J. Zhang, H. Di, H. Wang, K. Mao, T. Ma, and Y. Cao, Hot Deformation Behavior of Ti-15-3 Titanium Alloy: A Study Using Processing Maps, Activation Energy Map, and Zener-Hollomon Parameter Map, J. Mater. Sci., 2012, 47, p 4000–4011
F. Pilehva, A. Zarei-Hanzaki, S.M. Fatemi-Varzaneh, and A.R. Khalesian, Hot Deformation and Dynamic Recrystallization of Ti-6Al-7Nb Biomedical Alloy in Single-Phase β Region, J. Mater. Eng. Perform., 2015, 24, p 1799–1808
Author information
Authors and Affiliations
Corresponding author
Rights and permissions
About this article
Cite this article
Pilehva, F., Zarei-Hanzaki, A., Moemeni, S. et al. High-Temperature Deformation Behavior of a Ti-6Al-7Nb Alloy in Dual-Phase (α + β) and Single-Phase (β) Regions. J. of Materi Eng and Perform 25, 46–58 (2016). https://doi.org/10.1007/s11665-015-1813-6
Received:
Revised:
Published:
Issue Date:
DOI: https://doi.org/10.1007/s11665-015-1813-6