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Characterization of Impact Damage in Ultra-High Performance Concrete Using Spatially Correlated Nanoindentation/SEM/EDX

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Abstract

Little work has been done to study the fundamental material behaviors and failure mechanisms of cement-based materials including ordinary Portland cement concrete and ultra-high performance concretes (UHPCs) under high strain impact and penetration loads at lower length scales. These high strain rate loadings have many possible effects on UHPCs at the microscale and nanoscale, including alterations in the hydration state and bonding present in phases such as calcium silicate hydrate, in addition to fracture and debonding. In this work, the possible chemical and physical changes in UHPCs subjected to high strain rate impact and penetration loads were investigated using a novel technique wherein nanoindentation measurements were spatially correlated with images using scanning electron microscopy and chemical composition using energy dispersive x-ray microanalysis. Results indicate that impact degrades both the elastic modulus and indentation hardness of UHPCs, and in particular hydrated phases, with damage likely occurring due to microfracturing and debonding.

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References

  1. S.G. Millard, T.C.K. Molyneaux, S.J. Barnett, and X. Gao, Dynamic Enhancement of Blast-Resistant Ultra High Performance Fibre-Reinforced Concrete Under Flexural and Shear Loading, Int. J. Impact Eng., 2010, 37(4), p 405–413

    Article  Google Scholar 

  2. T.S. Rushing, N. Boone, A. Irizzary, and R. Magee, Independent Effects of Matrix Strength and Fiber Reinforcement on Concrete’s Ballistic Resistance, Proceedings of the 80th Shock and Vibration Symposium (San Diego, CA, USA), 2009

  3. G. Constantinides and F.J. Ulm, The Nanogranular Nature of C-S-H, J. Mech. Phys. Solids, 2007, 55(1), p 65–90

    Article  Google Scholar 

  4. D. Grady, Shock Equation of State Properties of Concrete, Proceedings of Structures Under Shock and Impact IV (Southampton, UK), 1996, p 405–414

  5. K. Velez, S. Maximilien, D. Damidot, G. Fantozzi, and F. Sorrentino, Determination by Nanoindentation of Elastic Modulus and Hardness of Pure Constituents of Portland Cement Clinker, Cem. Concr. Res., 2001, 31(4), p 555–561

    Article  CAS  Google Scholar 

  6. J.J. Hughes and P. Trtik, Micro-Mechanical Properties of Cement Paste Measured by Depth-Sensing Nanoindentation: A Preliminary Correlation of Physical Properties with Phase Type, Mater. Charact., 2004, 53(2–4), p 223–231

    Article  CAS  Google Scholar 

  7. F.J. Ulm, M. Vandamme, C. Bobko, J.A. Ortega, K. Tai, and C. Ortiz, Statistical Indentation Techniques for Hydrated Nanocomposites: Concrete, Bone, and Shale, J. Am. Ceram. Soc., 2007, 90(9), p 2677–2692

    Article  CAS  Google Scholar 

  8. G. Constantinides and F.J. Ulm, The Effect of Two Types of C-S-H on the Elasticity of Cement-Based Materials: Results from Nanoindentation and Micromechanical Modeling, Cem. Concr. Res., 2004, 34(1), p 67–80

    Article  CAS  Google Scholar 

  9. M.J. DeJong and F.J. Ulm, The Nanogranular Behavior of C-S-H at Elevated Temperatures (Up to 700 °C), Cem. Concr. Res., 2007, 37(1), p 1–12

    Article  CAS  Google Scholar 

  10. L. Sorreli, G. Constantinides, F.J. Ulm, and F. Toutlemonde, The Nano-Mechanical Signature of Ultra-High Performance Concrete by Statistical Nanoindentation Techniques, Cem. Concr. Res., 2008, 38(12), p 1447–1456

    Article  Google Scholar 

  11. J.J. Chen, L. Sorreli, M. Vandamme, F.J. Ulm, and G. Chanvillard, A Coupled Nanoindentation/SEM-EDS Study on Low Water/Cement Ratio Portland Cement Paste: Evidence for C-S-H/Ca(OH)2 Nanocomposites, J. Am. Ceram. Soc., 2010, 93(5), p 1484–1493

    CAS  Google Scholar 

  12. MIL-STD-662F, Military Standard: V50 Ballistic Test for Armor, 1997

  13. W.C. Oliver and G.M. Pharr, An Improved Technique for Determining Hardness and Elastic Modulus Using Load and Displacement Sensing Indentation Experiments, J. Mater. Res., 1992, 7(6), p 1564–1583

    Article  CAS  Google Scholar 

  14. D. Davydov, M. Jirasek, and L. Kopecky, Critical Aspects of Nano-Indentation Technique in Application to Hardened Cement Paste, Cem. Concr. Res., 2011, 41(1), p 20–29

    Article  CAS  Google Scholar 

  15. P.K. Mehta and P.J.M. Monteiro, Concrete: Microstructure, Properties, and Materials, McGraw-Hill Companies Ltd., New York, 2006

    Google Scholar 

  16. F. Ren, C. Mattus, J. Wang, and B. DiPaolo, Microstructural Characterization of UHPC Materials Subject to Impact Testing and Heating, 2nd Annual Meeting on Advances in Cement-Based Materials (Nashville, TN, USA), 2011

  17. P. Trtik, B. Munch, and P. Lura, A Critical Examination of Statistical Nanoindentation on Model Materials and Hardened Cement Pastes Based on Virtual Experiments, Cem. Concr. Compd., 2009, 31(10), p 705–714

    Article  CAS  Google Scholar 

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Acknowledgments

The authors would like to thank Dr. Todd Rushing of the Geotechnical and Structures Laboratory, US Army Engineer Research and Development Center (ERDC), for supplying the specimens for this study. Financial support for this work was provided by the ERDC and the U.S. Department of Defense SMART Scholarship Program. Permission to publish was granted by the Director, ERDC Geotechnical and Structures Laboratory.

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Correspondence to P. G. Allison.

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Moser, R.D., Allison, P.G. & Chandler, M.Q. Characterization of Impact Damage in Ultra-High Performance Concrete Using Spatially Correlated Nanoindentation/SEM/EDX. J. of Materi Eng and Perform 22, 3902–3908 (2013). https://doi.org/10.1007/s11665-013-0668-y

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  • DOI: https://doi.org/10.1007/s11665-013-0668-y

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