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The effect of tungsten particle size on the processing and properties of infiltrated W-Cu compacts

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Abstract

Three tungsten powders with average particle sizes of 8.7, 23.2, and 65.2 µm were used to make W-15Cu compacts. The compacting pressure and sintering temperature were adjusted for each powder to attain the desired skeleton density. Sintered skeletons were then infiltrated with oxygen-free copper at 1200 °C in hydrogen and in vacuum. Results showed that as the tungsten particle size decreased, higher compacting pressures and sintering temperatures were required for the same desired skeleton density. The processing parameters and the tungsten particle size caused variations in the amount of closed pores and the W-W contiguity, which in turn resulted in different infiltrated densities and resistivities. Direct infiltration on green compacts was also examined, and higher infiltration densities and lower electrical resistivities were obtained compared to those obtained by infiltrating sintered compacts. These results are discussed based on infiltrated density, differences in microstructure, and the W-W contiguity.

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References

  1. C. Zweben: J. Met., 1992, July, pp. 15–23.

  2. J.B. Oenning and I.S.R. Clark: U.S. Patent 4,988,386, Jan. 29, 1991.

  3. P.H. Dawson: GE Co. Rev., 1986, vol. 2 (3), pp. 168–70.

    Google Scholar 

  4. R.M. German, K.F. Hens, and L.J. Johson: Int. J. Powder Metall., 1994, vol. 30 (2), pp. 205–15.

    CAS  Google Scholar 

  5. M.R. Ehlert and E.R. Helderman: U.S. Patent 4,788,627, Nov. 29, 1988.

  6. E. Kny: Proc. 12th Int. Plansee Sem. ’89 Conf., Reutte, Tirol, Austria, 1989, vol. 1, pp. 763–72.

    Google Scholar 

  7. K.V. Sebastian: Int. J. Powder Metall. Powder Technol., 1981, vol. 17 (4), pp. 297–303.

    CAS  Google Scholar 

  8. R.V. Minakova, A.P. Kresanova, N.D. Lesnik, A.A. Malyshenko, and S.O. Antonov: Poroshkovaya Metall., 1988, vol. 302 (2), pp. 48–53 (English translation).

    Google Scholar 

  9. I.N. Frantsevich: Poroshkovaya Metall., 1980, vol. 212 (8), pp. 36–47 (English translation).

    Google Scholar 

  10. W. Neumann and E. Kny: High Temp.-High Pressure, 1989, vol. 21 (5), pp. 525–32.

    CAS  Google Scholar 

  11. C. Scorey: U.S. Patent 5,292,478, Mar. 8, 1994.

  12. M. Osada, Y. Amano, N. Ogasa, and A. Ohtsuka: U.S. Patent 5,086,333, Feb. 4, 1992.

  13. T.W. Kirk, S.G. Caldwell, and J.J. Oakes: Advances in Powder Metallurgy and Particulate Materials—1992, compiled by J.M. Capus and R.M. German, MPIF, Princeton, NJ, 1992, vol. 9, pp. 115–22.

    Google Scholar 

  14. V.B. Rabkin and R.F. Kozlova: Poroshkovaya Metall., 1968, vol. 63 (3), pp. 64–70 (English translation).

    Google Scholar 

  15. W.D. Kingery: J. Am. Ceram. Soc., 1957, vol. 40 (10), pp. 351–52.

    Article  CAS  Google Scholar 

  16. R.M. German: Metall. Trans. A, 1993, vol. 24A, pp. 1745–52.

    CAS  Google Scholar 

  17. M.F. Ashby: Acta Metall., 1974, vol. 22, pp. 275–89.

    Article  CAS  Google Scholar 

  18. L.H. VanVlack: Elements of Material Science and Engineering, 6th ed., Addison-Wesley Co., New York, NY, 1989, p. 399.

    Google Scholar 

  19. D.S. McLachlan, M. Blaszkiewicz, and R.E. Newnham: J. Am. Ceram. Soc., 1990, vol. 73 (8), pp. 2187–2203.

    Article  CAS  Google Scholar 

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Wang, W.S., Hwang, K.S. The effect of tungsten particle size on the processing and properties of infiltrated W-Cu compacts. Metall Mater Trans A 29, 1509–1516 (1998). https://doi.org/10.1007/s11661-998-0366-9

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  • DOI: https://doi.org/10.1007/s11661-998-0366-9

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