Abstract
Shear-Assisted Processing and Extrusion (ShAPE) is an advanced manufacturing technique that allows for many unique processes, and this work focuses on the ability of the ShAPE process to solutionize alloying elements by high-temperature severe plastic deformation, followed quickly by quenching, to skip a conventional solutionization heat treatment. Here, this solutionization during processing of an Al–Mg–Si alloy 6082 was studied using microhardness and microscopy. It was found that the plastic deformation increased the degree of solutionization at a given temperature, allowing for large supersaturations at temperatures well below conventional solutionization heat treatments. In addition, an air quench immediately after ShAPE processing was found to be fast enough to produce a good supersaturated solid solution in this alloy, and the as-artificially aged hardness was within specifications for a conventionally processed material that underwent a solutionization treatment followed by a water quench. This new processing pathway allows for high-quality material to be produced at a much lower energy cost.
Similar content being viewed by others
References
R.N. Harsha, V. Mithun Kulkarni, and B. Satish Babu: Mater. Today Proc., 2018, vol. 5, pp. 22340–49.
R.Z. Valiev, R.K. Islamgaliev, and I.V. Alexandrov: Prog. Mater. Sci., 2000, vol. 45, pp. 103–89.
S. Dadbakhsh, A. Karimi Taheri, and C.W. Smith: Mater. Sci. Eng. A, 2010, vol. 527, pp. 4758–66.
Yu. Ivanisenko, R. Kulagin, V. Fedorov, A. Mazilkin, T. Scherer, B. Baretzky, and H. Hahn: Mater. Sci. Eng. A, 2016, vol. 664, pp. 247–56.
C.C. Koch: Annu. Rev. Mater. Sci., 1989, vol. 19, pp. 121–43.
S.M. Ghalehbandi, M. Malaki, and M. Gupta: Appl. Sci., 2019, vol. 9, p. 3627.
R. Valiev: Nat. Mater., 2004, vol. 3, pp. 511–16.
S.H. Lee, Y. Saito, T. Sakai, and H. Utsunomiya: Mater. Sci. Eng. A, 2002, vol. 325, pp. 228–35.
S.R. Agnew, AYu. Vinogradov, S. Hashimoto, and J.R. Weertman: J. Electron. Mater., 1999, vol. 28, pp. 1038–044.
K. Bryła: Mater. Sci. Eng. A, 2020, vol. 772, p. 138750.
M. Komarasamy, X. Li, S.A. Whalen, X. Ma, N. Canfield, M.J. Olszta, T. Varga, A.L. Schemer-Kohrn, A. Yu, N.R. Overman, S.N. Mathaudhu, and G.J. Grant: J. Mater. Sci., 2021, vol. 56, pp. 12864–80.
V.V. Stolyarov, R. Lapovok, I.G. Brodova, and P.F. Thomson: Mater. Sci. Eng. A, 2003, vol. 357, pp. 159–67.
W.J. Kim, H.G. Jeong, and H.T. Jeong: Scripta Mater., 2009, vol. 61, pp. 1040–43.
Y. Estrin and A. Vinogradov: Acta Mater., 2013, vol. 61, pp. 782–817.
S.A. Whalen, D.R. Herling, X. Li, M. Reza-E-Rabby, B.S. Taysom, and G.J. Grant: U.S. Patent 20210053100A1.
B. S. Taysom, N. Overman, M. Olszta, M. Reza-E-Rabby, T. Skszek, M. DiCiano, and S. Whalen: Int. J. Mach. Tools Manuf. https://doi.org/10.1016/j.ijmachtools.2021.103798.
S. Whalen, M. Olszta, Md. Reza-E-Rabby, T. Roosendaal, T. Wang, D. Herling, B.S. Taysom, S. Suffield, and N. Overman: J. Manuf. Process., 2021, vol. 71, pp. 699–710.
R.E. Rabby, T. Wang, N.L. Canfield, T.J. Roosendaal, B.S. Taysom, D.D. Graff, D.R. Herling, and S.A. Whalen: CIRP J. Manuf. Sci. Technol. https://doi.org/10.1016/j.cirpj.2022.02.025.
B.S. Taysom, N. Overman, M. Olszta, M. Reza-E-Rabby, T. Skszek, M. DiCiano, and S. Whalen: Int. J. Mach. Tools Manuf, 2021, vol. 169, p. 103798.
T. Wang, J.E. Atehortua, M. Song, M. Reza-E-Rabby, B.S. Taysom, J. Silverstein, T. Roosendaal, D. Herling, and S. Whalen: Mater. Des., 2022, vol. 213, p. 110374.
G. Mrówka, J. Sieniawski, and A. Nowotnik: J. Achiev. Mater. Manuf. Eng., 2009, vol. 32, pp. 162–70.
C.D. Marioara, S.J. Andersen, J. Jansen, and H.W. Zandbergen: Acta Mater., 2001, vol. 49, pp. 321–28.
C. Cayron and P.A. Buffat: Acta Mater., 2000, vol. 48, pp. 2639–53.
R. Vissers, M.A. van Huis, J. Jansen, H.W. Zandbergen, C.D. Marioara, and S.J. Andersen: Acta Mater., 2007, vol. 55, pp. 3815–23.
M. Cooper and K. Robinson: Acta Crystallogr., 1966, vol. 20, pp. 614–17.
A. Aginagalde, X. Gomez, L. Galdos, and C. García: J. Eng. Mater. Technol., 2009, vol. 131, p. 044501.
C. Suryanarayana: Prog. Mater. Sci., 2001, vol. 46, pp. 1–84.
S.C. Bergsma, M.E. Kassner, X. Li, and R.S. Rosen: Quench Sensitivity of Hot Extruded 6061-T6 and 6069-T6 Aluminum Alloys, Lawrence Livermore National Lab. (LLNL), Livermore, 2000.
A. Güzel, A. Jäger, N. Ben Khalifa, and A.E. Tekkaya: Key Eng. Mater., 2010, vol. 424, pp. 51–56.
V. Noseda Grau, A. Cuniberti, A. Tolley, V. Castro Riglos, and M. Stipcich: J. Alloys Compd., 2016, vol. 684, pp. 481–87.
A. Mauduit and H. Gransac: Ann. Chim. Sci. Matér., 2020, vol. 44, pp. 141–49.
European Committee for Standardization: EN 573–3: Aluminium and Aluminium Alloys—Chemical Composition and Form of Wrought Products—Part 3: Chemical Composition and Form of Products, 2007.
W.Z. Misiolek and R.M. Kelly: in ASM Handbook, Volume 14A: Bulk Forming, vol. 14A, ASM, Materials Park, 2005, pp. 522–27.
ASTM International: ASTM E384: Standard Test Method for Microindentation Hardness of Materials, ASTM International, West Conshohocken, 2021.
ASTM International: 2016.
M. Tercelj, M. Fazarinc, G. Kugler, and I. Perus: Constr. Build. Mater., 2013, vol. 44, pp. 781–91.
G. Mrówka-Nowotnik, J. Sieniawski, and M. Wierzbińska: Arch. Mater. Sci. Eng., 2007, vol. 28(2), pp. 69–76.
Y.-L. Chang, F.-Y. Hung, and T.-S. Lui: J. Market. Res., 2019, vol. 8, pp. 173–79.
H. Fröck, B. Milkereit, P. Wiechmann, A. Springer, M. Sander, O. Kessler, and M. Reich: Metals, 2018, vol. 8, p. 265.
X. He, Q. Pan, H. Li, Z. Huang, S. Liu, K. Li, and X. Li: Metals, 2019, vol. 9, p. 173.
Y. Birol: J. Therm. Anal. Calorim., 2006, vol. 83, pp. 219–22.
S. Bikass, B. Andersson, A. Pilipenko, and H.P. Langtangen: Int. J. Therm. Sci., 2012, vol. 52, pp. 50–58.
K. Anderson, J. Weritz, and J.G. Kaufman: ASM Handbook, Volume 2B: Properties and Selection of Aluminum Alloys, ASM International, Materials Park, 2019.
B. Milkereit and M.J. Starink: Mater. Des., 2015, vol. 76, pp. 117–29.
N. Kumar, S. Goel, R. Jayaganthan, and H.-G. Brokmeier: Metallogr. Microstruct. Anal., 2015, vol. 4, pp. 411–22.
G. Mrówka-Nowotnik and J. Sieniawski: J. Mater. Process. Technol., 2005, vol. 162–163, pp. 367–72.
B.C. Shang, Z.M. Yin, G. Wang, B. Liu, and Z.Q. Huang: Mater. Des., 2011, vol. 32, pp. 3818–22.
D. Schwen, M. Wang, R. Averback, and P. Bellon: J. Mater. Res., 2013, vol. 28, pp. 2687–93.
J. Lendvai, H.-J. Gudladt, and V. Gerold: Scripta Metall., 1988, vol. 22, pp. 1755–60.
H. Luo, J. Sietsma, and S. Van Der Zwaag: Metall. Mater. Trans. A, 2004, vol. 35A, pp. 1889–98.
N.X. Sun, X.D. Liu, and K. Lu: Scripta Mater., 1996, vol. 34, pp. 1201–07.
F.L. Cumbrera and F. Sánchez-Bajo: Thermochim. Acta, 1995, vol. 266, pp. 315–30.
Acknowledgments
The authors thank the U.S. Department of Energy Vehicle Technologies Office (DOE/VTO) Lightweight Metals Core Program for supporting this work. The authors are grateful for the dedication of Anthony Guzman for the excellent preparation of specimens for microstructural characterization and to Maura Zimmerschied for technical editing of this manuscript. Pacific Northwest National Laboratory is operated by the Battelle Memorial Institute for the DOE under contract DE-AC05-76RL01830.
Author Contributions
BM: Investigation, formal analysis, data curation, writing—original draft, writing—review and editing. XM: Investigation. BST: Investigation. SW: Supervision and funding acquisition.
Conflict of interest
On behalf of all authors, the corresponding author states that there is no conflict of interest.
Author information
Authors and Affiliations
Corresponding author
Additional information
Publisher's Note
Springer Nature remains neutral with regard to jurisdictional claims in published maps and institutional affiliations.
Rights and permissions
About this article
Cite this article
Milligan, B.K., Ma, X., Taysom, B.S. et al. Solutionization via Severe Plastic Deformation: Effect of Temperature and Quench Method in a ShAPE-Processed Al–Mg–Si Alloy. Metall Mater Trans A 54, 2576–2584 (2023). https://doi.org/10.1007/s11661-023-07034-8
Received:
Accepted:
Published:
Issue Date:
DOI: https://doi.org/10.1007/s11661-023-07034-8