Abstract
The microstructure and mechanical properties of a heat-treated biomedical ASTM F90 Co-20Cr-15W-10Ni (mass pct) alloy were investigated. The alloy was heat-treated at temperatures of 673 K to 1623 K (400 °C to 1450 °C) for holding times of 0.6 to 259.2 ks. The formation of M23X6-type (M: metallic element and X: C and N) and η-phase (M6X-M12X type) precipitates was detected in the heat-treated alloys using a combination of electrolytic extraction and X-ray diffraction. The formation of precipitates deteriorated the ductility of the heat-treated alloys. On the other hand, both the tensile strength and elongation were improved by heat treatment at low temperatures of 673 K to 873 K (400 °C to 600 °C). In this heat-treated alloy, the density of stacking faults was higher than that of the as-received alloy, and the formation of the ε-phase was detected.
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Abbreviations
- BSE:
-
Backscattered electron
- EBSD:
-
Electron backscatter diffraction
- SEM:
-
Scanning electron microscopy
- TRIP:
-
Transformation-induced plasticity
- XRD:
-
X-ray diffraction
References
R. V. Marrey, R. Butgermeister, R. B. Grishaber and R. O. Ritchie: Biomaterials, 2006, vol. 27, pp. 1988–2000.
J. Favre, Y. Koizumi, A. Chiba, D. Fabregue and E. Maire: Meta// Mater. Trans. A, 2013, vol. 44, pp. 2819–2830.
P. Poncin and J. Proft: Proc. Mater. Process. Med. Devices Conf., 2003. pp. 253–59.
F.R. Morral: J. Mater., 1966, vol. 1, pp. 384–412.
R. K. Gupta, M. K. Karthikeyan, D. N. Bhalia, B. R. Ghosh and P. P. Sinha: Met. Sci. heat treat., 2008, vol. 50, pp. 175–178.
J. Teague, E. Cerreta and M. Stout: Meta//, Mater. Trans. A, 2004, vol. 35, pp. 2767–2781.
N. Yukawa and K. Sato: Mater. Trans. JIM, 1968, vol. 9, pp. 680–686.
M. Tanaka and H. Iizuka: Meta//. Mater. Trans. A, 1992, vol. 23, pp. 609–616.
P. Poncin, B. Gruez, P. Missillier, and P. Comte-Gaz: Proc. Mater. Process. Med. Devices Conf., 2006. pp. 85–90.
P. Poncin, C. Millet, and J. Chevy: Proc. Mater. Process. Med. Devices Conf., 2004. pp. 279–83.
K. Ueki, K. Ueda and T. Narushima: Key. Eng. Mater., 2014, vol. 616, pp. 258-262.
S. Mineta, S. Namba, T. Yoneda, K. Ueda and T. Narushima: Meta//, Mater. Trans. A, 2010, vol. 41, pp. 2129–2138.
S. Mineta, Alfirano, S. Namba, T. Yoneda, K. Ueda, and T. Narushima: Metall. Mater. Trans. A, 2013, vol. 44A, pp. 494–503.
S. Mineta, Alfirano S. Namba, T. Yoneda, K. Ueda and T. Narushima: Meta//, Mater. Trans. A, 2012, vol. 43, pp. 3351–3358.
F. Kurosawa, I. Taguchi and R. Matsumoto: J. Japan Inst. Metals, 1976, vol. 40, pp. 834–838.
A.J.T. Clemow and B.L. Daniell: J. Biomed. Mater. Res., 1979, vol. 13, pp. 265–279.
Alfirano, S. Mineta, S. Namba, T. Yoneda, K. Ueda and T. Narushima: Meta//, Mater. Trans. A, 2011, vol. 42, pp. 1941–1949.
Alfirano, S. Mineta, S. Namba, T. Yoneda, K. Ueda and T. Narushima: Meta//, Mater. Trans. A, 2012, vol. 43, pp. 2125–2132.
E. Bettini, T. Eriksson, M. Boström, C. Leygraf and J. Pan: Electrochim. Acta, 2011, vol. 56, pp. 9413–9419.
T. Narushima, S. Mineta, Y. Kurihara and K. Ueda: JOM, 2013, vol. 65(4), pp. 489–504.
D. Sorensen, B. Q. Li, W. W. Gerberich and K. A. Mkhoyan: Acta Mater., 2014, vol. 63, pp. 63–72.
M. Assefpour-Dezfuly and W. Bonfield: J. Mater. Sci., 1984, vol. 19, pp. 2815–2836.
L. Remy and A. Pineau: Mater. Sci. Eng., 1976, vol. 26, pp. 123-132.
I. Tamura: Met. Sci., 1982, vol. 16, pp. 245–253.
T. Maki, T. Furuhara, N. Tsuji, S. Morita, G. Miyamoto and A. Shibata: Tetsu-to-Hagane, 2014, vol. 100, pp.1062-1075.
A. K. Srivastava, G. Jha, N. Gope and S.B. Singh: Mater. Charact. 2006, vol. 57, pp. 127-135.
Acknowledgment
This study was financially supported by a Grant-in-Aid for Scientific Research from the Ministry of Education, Culture, Sports, Science and Technology (MEXT), Japan, under Contract No. 25249094.
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Manuscript submitted October 2, 2015.
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Ueki, K., Ueda, K. & Narushima, T. Microstructure and Mechanical Properties of Heat-Treated Co-20Cr-15W-10Ni Alloy for Biomedical Application. Metall Mater Trans A 47, 2773–2782 (2016). https://doi.org/10.1007/s11661-016-3488-5
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DOI: https://doi.org/10.1007/s11661-016-3488-5