Skip to main content
Log in

Determination of Modulus of Metal Films Using Thermoreflectance

  • Published:
Metallurgical and Materials Transactions A Aims and scope Submit manuscript

Abstract

The acoustic displacements in a film of indium pressed on to a sapphire wafer were generated by incidence of a Q-switched Nd-YAG laser beam. Acoustic displacements from tungsten film deposited on silicon substrate were also measured by the same technique. Thermoreflectance from a continuous red laser incident on the surface was used simultaneously to measure the acoustic oscillations. The acoustic oscillations were simulated using the solution to the modified wave equation. The acoustic velocity and the modulus of the metal film were determined from the simulation of the experimental results. It is shown that this technique provides a nondestructive method of determination of acoustic velocity and modulus in the metal films.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Fig. 1
Fig. 2
Fig. 3
Fig. 4
Fig. 5
Fig. 6

Similar content being viewed by others

References

  1. M. Radovic, E. Lara-Curzio and L. Riester, Mat. Sci. Eng., 2004, vol. 368A, pp. 56-70.

    Article  Google Scholar 

  2. ASTM E 1876-09, Standard Test Method for Dynamic Young’s Modulus, Shear Modulus and Poisson’s Ratio by Impulse Excitation, Annual book of ASTM Standards, ASTM International, 100 Barr Harbor Dr, P. O. Box C 700, West Conshohocken, PA 19428-2959.

  3. P. A. Bosom Worth, J. ASTM Int., 2010, vol. 7, pp. 1–15.

    Google Scholar 

  4. A. S. Maxwell, S. Owen-Jones and N. M. Jennet, Rev. Sci. Instrum., 2004, v. 75, pp. 970-975.

    Article  Google Scholar 

  5. ASTM E 756-10, Standard Test Method for Measuring Vibration-Damping Properties of Materials, Annual book of ASTM Standards, ASTM International, 100 Barr Harbor Dr, P. O. Box C 700, West Conshohocken, PA 19428-2959.

  6. J. R. Hutchinson and C. M. Percival, J. Acoust. Soc. America, 1968, vol. 44, pp. 1204-1210.

    Article  Google Scholar 

  7. C. M. Percival and J. A. Cheney, Experimental Mech., 1969, vol. 9, pp. 49-57.

    Article  Google Scholar 

  8. S. Krishnaswamy: in Nondestructive Evaluation, T. Kundu, ed., CRC Press, Washington, DC, 2003, chapt. 7, pp. 436–39.

  9. T. W. Murray, S. Krishnaswamy and J. D. Achenbach, Appl. Phys. Lett., 1999, vol. 74, pp. 3561-3563.

    Article  Google Scholar 

  10. H.-N. Lin, R. J. Stoner, H. J. Marris and J. Tauc, J. Appl. Phys., 1991, vol. 69, pp. 3816-3822.

    Article  Google Scholar 

  11. C. Thomson, H. T. Grahn, H. J. Marris, and J. Tauc, Phys. Rev. B., 1986, vol. 34, pp. 4129-4138.

    Article  Google Scholar 

  12. O. B. Wright, J. Appl. Phys., 1992, vol. 71, pp. 1617-1629.

    Article  Google Scholar 

  13. G. L. Eesley, B. M. Clemens and C. A. Paddock, Appl. Phys. Lett., 1987, vol. 50, pp. 717-720.

    Article  Google Scholar 

  14. M.A. Panzer, G. Zhang, D. Mann, X. Hu, E. Pop, H. Dai, and K.E. Goodson: J. Heat Trans. 2008, vol. 130, pp. 052401-1-9.

  15. H. Zheng and K. Jagannadham, Met. Mat. Trans., 2014, vol. 45A, pp. 2480-2486.

    Article  Google Scholar 

  16. J. P. Hirth and J. Lothe, 2nd edition, Theory of dislocations, Krieger Publishing Company, Malabar, Fl, 1992, p. 183.

    Google Scholar 

  17. A.E. H. Love, A treatise on mathematical theory of elasticity, 1944, Dover publications, New York, 1944, p. 428.

    Google Scholar 

  18. Properties of Indium Given in Metals Hand Book, Desk Edition, Engineering Tables 1–45, 1985, Metals Park, Ohio 44073.

  19. S. Kim and H. Ledbetter, Mat. Sci. Engng., 1998, vol. A32, pp. 139-143.

    Article  Google Scholar 

  20. B. S. Chandrasekhar and J. A. Raine, Phys. Rev., 1961, vol. 124, pp. 1011-1014.

    Article  Google Scholar 

  21. D. R. Winder and C. S. Smith, J. Phys. Chem. Solids,1958, vol. 4, pp. 128-134.

    Article  Google Scholar 

  22. J. P. Hirth and J. Lothe, 2nd edition, Theory of dislocations, Krieger Publishing Company, Malabar, Fl, 1992, p. 837.

    Google Scholar 

  23. C. Thomsen, H. J. Maris and J. Tauc, Thin Solid Films, 1987, vol. 154, pp. 217-223.

    Article  Google Scholar 

Download references

Acknowledgments

The author acknowledges partial support of this work from NSF-CMMI.

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to K. Jagannadham.

Additional information

Manuscript submitted May 10, 2014.

Rights and permissions

Reprints and permissions

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Jagannadham, K. Determination of Modulus of Metal Films Using Thermoreflectance. Metall Mater Trans A 46, 229–234 (2015). https://doi.org/10.1007/s11661-014-2598-1

Download citation

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s11661-014-2598-1

Keywords

Navigation