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High-Temperature Tensile Properties of Nano-Oxide Dispersion Strengthened Ferritic Steels Produced by Mechanical Alloying and Spark Plasma Sintering

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Abstract

Oxide-dispersion strengthened (ODS) ferritic steels were produced by mechanical alloying and subsequent spark plasma sintering. Very fast heating rates were used to minimize porosity when controlling grain size and precipitation of dispersoids within a compacted material. Sintering cycles performed at 1373 K (1100 °C) induced heterogeneous, but fine grain size distribution and high density of nano-oxides. Yield strengths at room temperature and at 923 K (650 °C) are 975 MPa and 298 MPa, respectively. Furthermore, high-temperature ductility is much increased: total strain of 28 pct at 923 K (650 °C).

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The authors gratefully thank F. Mercier and G. Bonnefont for their assistance in SPS compaction and D. Hamon, P. Wident and A. Bougault for their contribution in materials characterization. The current study was performed with financial support of the French CNRS GdR GEDEPEON and for the MATTER project within the seventh European framework. The current study was made in the frame of a tripartite agreement between the CEA, AREVA NP, and EDF.

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Authors and Affiliations

  1. CEA, DEN, Service de Recherches Métallurgiques Appliquées, 91191, Gif-sur-Yvette, France

    Xavier Boulnat (Ph.D. Student) & Yann de Carlan (Researcher)

  2. INSA-Lyon, MATEIS UMR CNRS 5510, Université de Lyon, 69621, Villeurbanne, France

    Xavier Boulnat (Ph.D. Student), Damien Fabregue (Associate Professor) & Michel Perez (Professor)

  3. Laboratoire Léon Brillouin, CEA-CNRS, CEA/Saclay, 91191, Gif-sur-Yvette, France

    Marie-Hélène Mathon (Researcher)

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  1. Xavier Boulnat
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  2. Damien Fabregue
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  4. Marie-Hélène Mathon
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Correspondence to Xavier Boulnat.

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Manuscript submitted January 7, 2013.

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Boulnat, X., Fabregue, D., Perez, M. et al. High-Temperature Tensile Properties of Nano-Oxide Dispersion Strengthened Ferritic Steels Produced by Mechanical Alloying and Spark Plasma Sintering. Metall Mater Trans A 44, 2461–2465 (2013). https://doi.org/10.1007/s11661-013-1719-6

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