Skip to main content
Log in

Effect of Thermal Aging on the Corrosion and Microstructure of Friction-Stir Welded Alloy 22

  • Published:
Metallurgical and Materials Transactions A Aims and scope Submit manuscript

Abstract

The effect of thermal aging on the corrosion and microstructure of friction-stir welded (FSW) alloy 22 was investigated. Successful welds were produced with a polycrystalline cubic BN pin tool at a rotational speed of 200 rev min−1 and travel speed of 12.7 mm min−1. Topologically closed packed (TCP) phases of ~50 to 300 nm size were identified in the weld nugget. The area fraction of the TCP phases in the weld nugget increased with aging temperature and time. General corrosion rates measured from the weight loss experiments for welds were relatively higher than for parent material. The corrosion rates increased with the increased aging temperature and time. Intergranular corrosion (IGC) resistance is greater in friction-stir welds compared with the parent material at all aging temperatures and times. The IGC depth increased with the aging temperature and time in the parent material. The IGC depth for the FSW weld nugget was minimal and did not change with thermal aging.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Fig. 1
Fig. 2
Fig. 3
Fig. 4
Fig. 5
Fig. 6
Fig. 7
Fig. 8
Fig. 9
Fig. 10
Fig. 11
Fig. 12

Similar content being viewed by others

References

  1. V. Desai: JOM, 2005, vol. 57, pp. 18–19.

    Article  Google Scholar 

  2. T.S.E. Summers, R.B. Rebak, T.A. Palmer, and P. Crook: Scientific Basis for Nuclear Waste Management XXV, Materials Research Society, Warrendale, PA, 2002, vol. 713, pp. 45–52.

  3. B.S. El-Dasher, T.S. Edgecumbe, and S.G. Torres: Metall. Mater. Trans. A, 2006, vol. 37A, pp. 1027-38.

    Article  CAS  Google Scholar 

  4. M.J. Cieslak, T.J. Headley, and A.D. Romig: Metall. Trans. A, 1986, vol. 17A, pp. 2035-47.

    CAS  Google Scholar 

  5. S.G. Torres, B. El-Dasher, M. McGregor, R. Etien, T.S. Edgecumbe, G. Gdowski, N. Yang, T. Headley, J. Chames, J.L. Yio, and A. Gardea: Lawrence Livermore National Laboratory (LLNL), UCRL-TR-217339, Livermore, CA, 2005.

  6. Y.M. Pan, D.S. Dunn, and G.A. Cragnolino: Metall. Mater. Trans. A, 2005, vol. 36A, pp 1143-51.

    Article  CAS  Google Scholar 

  7. W.M. Thomas, E.D. Nicholas, J.C. Needham, M.G. Murch, P. Templesmith, and C.J. Dawes: Patent U.K. 9125978.8, 1991.

  8. W.M. Thomas: Proc. of the 1st Int. Symp. on Friction Stir Welding, Thousand Oaks, CA, 1999.

    Google Scholar 

  9. W.J. Arbegast: Hot Deformation of Aluminum Alloys III, TMS, Warrendale, PA, 2003, pp. 313-27.

    Google Scholar 

  10. T.J. Lienert and J.E. Gould: Proc. of the 1 st Int. Symp. on Friction Stir Welding, Thousand Oaks, CA, 1999.

    Google Scholar 

  11. W.J. Arbegast and P.J. Hartley: Trends in Welding Research, Proc. of the Fifth Int. Conf., ASM International, Materials Park, OH, 1999, pp. 541-46.

    Google Scholar 

  12. T.U. Seidel and A.P. Reynolds: Metall. Mater. Trans. A, 2001, vol. 32A, pp. 2879-84.

    Article  CAS  Google Scholar 

  13. M. Sutton, B. Yang, A. Reynolds, and R. Taylor: Mater. Sci. Eng. A, 2002, vol. 323, pp. 160-66.

    Article  Google Scholar 

  14. J.Q. Su, T. Nelson, R. Mishra, and M. Mahoney: Acta Mater., 2003, vol. 51, pp. 713-29.

    Article  CAS  Google Scholar 

  15. B.M. Tweedy, W.J. Arbegast, and C.D. Allen: Friction Stir Welding and Processing-III, The Minerals, Metals and Materials Society, San Francisco, CA, 2005, pp. 97-104.

    Google Scholar 

  16. R.L. Goetz and K.V. Jata, Friction Stir Welding and Processing, The Minerals, Metals and Materials Society, Indianapolis, IN, 2001, pp. 35-42.

    Google Scholar 

  17. A.P. Reynolds, E. Hood, and W. Tang: Scripta Mater., 2005, vol. 52, pp. 491-94.

    Article  CAS  Google Scholar 

  18. W.B. Lee, C.Y. Lee, W.S. Chang, Y.M. Yeon, and S.B. Jung: Mater. Lett., 2005, vol. 59, pp. 3315-18.

    Article  CAS  Google Scholar 

  19. D. Sanders, M. Ramulu, E. Klock-McCook, P. Edwards, A. Reynolds, and T. Trapp: J. Mater. Eng. Perform., 2008, vol. 17, pp. 187-92.

    Article  CAS  Google Scholar 

  20. J. Esparza, W. Davis, E. Trillo, and L. Murr: J. Mater. Sci. Lett., 2002, vol. 21, pp. 917-20.

    Article  CAS  Google Scholar 

  21. W. Xunhong and W. Kuaishe: Mater. Sci. Eng. A, 2006, vol. 431, pp. 114-17.

    Article  Google Scholar 

  22. S.H.C. Park, Y.S. Sato, and H. Kokawa: Metall. Mater. Trans. A, 2003, vol. 34A, pp. 987-94.

    Article  CAS  Google Scholar 

  23. W.B. Lee and S.B. Jung: Mater. Lett., 2004, vol. 58, pp. 1041-46.

    Article  CAS  Google Scholar 

  24. G. Xie, Z. Ma, and L. Geng: Scripta Mater., 2007, vol. 57, pp. 73–76.

    Article  CAS  Google Scholar 

  25. K. Oh-Ishi and T.R. McNelley: Metall. Mater. Trans. A, 2004, vol. 35A, pp. 2951-61.

    Article  CAS  Google Scholar 

  26. B.K. Jasthi, S.M. Howard, W.J. Arbegast, G.J. Grant, S. Koduri, and D.R. Herling: Friction Stir Welding and Processing III, The Minerals, Metals and Materials Society, San Francisco, CA, 2005, pp. 75-79.

    Google Scholar 

  27. P. Miao, G. Odette, J. Gould, J. Bernath, R. Miller, M. Alinger, and C. Zanis: J. Nucl. Mater., 2007, vol. 367, pp. 1197-1202.

    Article  Google Scholar 

  28. M. West, B.K. Jasthi, P. Hosemann, and V. Sodesetti: Friction Stir Welding and Processing VI, The Minerals, Metals and Materials Society, San Diego, CA, 2011, pp. 33-40.

    Book  Google Scholar 

  29. R.A. Prado, L.E. Murr, D.J. Shindo, and K.F. Soto: Scripta Mater., 2001, vol. 45, pp. 75-80.

    Article  CAS  Google Scholar 

  30. J. Ouyang, E. Yarrapareddy, and R. Kovacevic: J. Mater. Process. Technol., 2006, vol. 172, pp. 110-22.

    Article  CAS  Google Scholar 

  31. A. Somasekharan and L. Murr: Mater. Charact., 2004, vol. 52, pp. 49-64.

    Article  CAS  Google Scholar 

  32. P. Venkateswaran, Z.H. Xu, X. Li, and A. Reynolds: J. Mater Sci., 2009, vol. 44, pp. 4140-47.

    Article  CAS  Google Scholar 

  33. B.K. Jasthi, W.J. Arbegast, and S.M. Howard: J. Mater. Eng. Perform., 2009, vol. 18, pp. 925-34.

    Article  CAS  Google Scholar 

  34. C.D. Sorensen, B. Nelson, and S. Sanderson: Friction Stir Welding and Processing-IV, The Minerals, Metals and Materials Society, Orlando, FL, 2007, pp. 285-93.

    Google Scholar 

  35. F. Ye, H. Fujii, T. Tsumura, and K. Nakata: J. Mater. Sci., 2006, vol. 41, pp. 5376-79.

    Article  CAS  Google Scholar 

  36. B.K. Jasthi, E.Y. Chen, W.J. Arbegast, M. Heringer, D.R. Bice, and S.M. Howard: Friction Stir Welding and Processing VI, The Minerals, Metals and Materials Society, San Diego, CA, 2011, pp. 25-32.

    Book  Google Scholar 

  37. B.K. Jasthi, W.J. Arbegast, and S.M. Howard: Friction Stir Welding and Processing VI, The Minerals, Metals and Materials Society, San Diego, CA, 2011, pp. 11-18.

    Book  Google Scholar 

  38. Y. Sato, P. Arkom, H. Kokawa, T. Nelson, and R. Steel: Mater. Sci. Eng. A, 2008, vol. 477, pp. 250-58.

    Article  Google Scholar 

  39. R.S. Mishra, M.W. Mahoney, S.X. McFadden, N.A. Mara, and A.K. Mukherjee: Scripta Mater., 1999, vol. 42, pp. 163-68.

    Article  Google Scholar 

  40. Z.Y. Ma, R.S. Mishra, and M.W. Mahoney: Acta Mater., 2002, vol. 50, pp. 4419-30.

    Article  CAS  Google Scholar 

  41. Z.Y. Ma and R.S. Mishra: Acta Mater., 2003, vol. 51, pp. 3551-69.

    Article  CAS  Google Scholar 

  42. I. Charit and R.S. Mishra: Mater. Sci. Eng. A, 2003, vol. 359, pp. 290-96.

    Article  Google Scholar 

  43. W.J. Arbegast: Weld J., 2006, vol. 85, pp. 28-35.

    CAS  Google Scholar 

  44. Z. Li, W. Arbegast, P. Hartley, and E. Meletis: Trends in Welding Research, Proc. of the 5 th Int. Conf., ASM International, Materials Park, OH, 1999, pp. 568-73.

    Google Scholar 

  45. J. Andersson, T. Helander, L. Höglund, P. Shi, and B. Sundman: CALPHAD, 2002, vol. 26, pp. 273-312.

    Article  CAS  Google Scholar 

  46. ASTM G28-02, Standard Test Methods of Detecting Susceptibility to Intergranular Corrosion in Wrought, Nickel-Rich, Chromium-Bearing Alloys, Annual Book of ASTM Standards, 2010, pp. 72–78.

  47. D.V. Fix and R.B. Rebak: J. ASTM Int., 2006, vol. 3 (10).

  48. K. Krishnan: Mater. Sci. Eng. A, 2002, vol. 327, pp. 246-51.

    Article  Google Scholar 

  49. R.B. Rebak and N.B. Koon: Corrosion, 1998, vol. 153.

  50. R.B. Rebak: T.S.E. Summers, and R.M. Carranza: Scientific Basis for Nuclear Waste Management XXIII, Materials Research Society, Warrendale, PA, 2000, pp. 109-14.

    Google Scholar 

  51. R. Mulford: Corrosion, 1983, vol. 39, pp. 132-43.

    Article  CAS  Google Scholar 

  52. C. Briant and R. Mulford: Corrosion, 1982, vol. 38, pp. 468-77.

    Article  CAS  Google Scholar 

  53. U. Heubner, E. Altpeter, M. Rockel, and E. Wallis: Corrosion, 1989, vol. 45, pp. 249-58.

    Article  CAS  Google Scholar 

  54. F. Hodge: Corrosion, 1973, vol. 29, pp. 375-83.

    CAS  Google Scholar 

  55. D. Gorhe, K. Raja, S. Namjoshi, V. Radmilovic, A. Tolly, and D. Jones: Metall. Mater. Trans. A, 2005, vol. 36A, pp. 1153-67.

    Article  CAS  Google Scholar 

  56. A. Di Schino and J. Kenny: J. Mater. Sci. Lett., 2002, vol. 21, pp. 1631-34.

    Article  CAS  Google Scholar 

  57. A. Di Schino and J. Kenny: J. Mater. Sci. Lett., 2002, vol. 21, pp. 1969-71.

    Article  CAS  Google Scholar 

  58. M. Hasegawa and M. Osawa: Corrosion, 1984, vol. 40, no. 7, pp. 371–74.

    Article  CAS  Google Scholar 

  59. A. Di Schino, M. Barteri, and J. Kenny: J. Mater. Sci., 2003, vol. 38, pp. 4725-33.

    Article  CAS  Google Scholar 

  60. E.L. Hall and C.L. Briant: Metall. Trans. A, 1984, vol. 15A, pp. 793-811.

    CAS  Google Scholar 

Download references

Acknowledgments

This research was sponsored by the Army Research Laboratory and performed under Cooperative Agreement Number DAAD19-02-2-0011. The authors gratefully acknowledge Michael West and Edward Duke, South Dakota School of Mines and Technology for their support regarding the microstructural analysis. Acknowledgements are extended to Glenn Grant of Pacific Northwest National Laboratories and to Raul Rebak of General Electric for their helpful suggestions.

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to Bharat K. Jasthi.

Additional information

Manuscript submitted July 21, 2011.

Rights and permissions

Reprints and permissions

About this article

Cite this article

Jasthi, B.K., Arbegast, W.J. & Howard, S.M. Effect of Thermal Aging on the Corrosion and Microstructure of Friction-Stir Welded Alloy 22. Metall Mater Trans A 43, 3192–3201 (2012). https://doi.org/10.1007/s11661-012-1141-5

Download citation

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s11661-012-1141-5

Keywords

Navigation