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Mechanochemical Behavior of NiO-Al-Fe Powder Mixtures to Produce (Ni, Fe)3Al-Al2O3 Nanocomposite Powder

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Abstract

(Ni, Fe)3Al-30 vol pct Al2O3 nanocomposite powder was synthesized by mechanochemical reaction of Fe-NiO-Al powder mixtures. Structural evolution during mechanical alloying was studied by employing X-ray diffractometry (XRD), differential thermal analysis (DTA), and transmission electron microscopy (TEM). After 78 minutes of milling, the (Ni, Fe)3Al-30 vol pct Al2O3 nanocomposite can be synthesized by reaction 3Fe + 7Al + 6NiO with a combustion mode. DTA results revealed that milling for 60 minutes decreases the temperature of reaction from 1040 K to 898 K (767 °C to 625 °C). TEM images corroborate a homogenous dispersion of reinforcements in the matrix of the nanocomposite proving that the reduction in the crystallite size of both reinforcements and matrix is within the nanometer range.

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Authors and Affiliations

  1. Department of Materials Engineering, Isfahan University of Technology, Isfahan, 84156-83111, Iran

    Z. Adabavazeh (MSc Graduate Student), F. Karimzadeh (Associate Professor, Supervisor) & M. H. Enayati (Associate Professor, Supervisor)

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  1. Z. Adabavazeh
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  2. F. Karimzadeh
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  3. M. H. Enayati
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Correspondence to Z. Adabavazeh.

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Manuscript submitted August 3, 2011.

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Adabavazeh, Z., Karimzadeh, F. & Enayati, M.H. Mechanochemical Behavior of NiO-Al-Fe Powder Mixtures to Produce (Ni, Fe)3Al-Al2O3 Nanocomposite Powder. Metall Mater Trans A 43, 3359–3365 (2012). https://doi.org/10.1007/s11661-012-1138-0

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