Skip to main content
Log in

Study on Raman Spectroscopy and Purification of B-C-N Compound

  • Communication
  • Published:
Metallurgical and Materials Transactions A Aims and scope Submit manuscript

Abstract

Electrophoretic technology is used to purify BC3.3N in an amorphous carbon and hexagonal boron nitride sample. The results are acquired using Raman spectroscopy and field emission scanning electron microcopy with energy dispersive spectroscopy, which show that pure BC3.3N is obtained from graphite and hexagonal boron nitride. The structural characteristics of this compound are studied by Fourier transform infrared spectroscopy. A simple method for purifying B-C-N compounds is presented.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Fig. 1
Fig. 2
Fig. 3
Fig. 4

Similar content being viewed by others

References

  1. A.Y. Liu, R.M. Wentzcovitch, and M.L. Cohen: Phys. Rev. B, 1989, vol. 39, pp. 1760–65.

    Article  CAS  Google Scholar 

  2. V.L. Solozhenko, D. Andrault, G. Fiquet, M. Mezouar, and D.C. Rubie: Appl. Phys. Lett., 2001, vol. 78, pp. 1385–87.

    Article  CAS  Google Scholar 

  3. Y. Zhao, D.W. He, L.L. Daemen, T.D. Shen, R.B. Schwarz, Y. Zhu, D.L. Bish, J. Huang, J. Zhang, G. Shen, J. Qian, and T.W. Zerda: J. Mater. Res., 2002, vol. 17, pp. 3139–45.

    Article  CAS  Google Scholar 

  4. X.G. Luo, X.J. Guo, Z.Y. Liu, J.L. He, D.L. Yu, B. Xu, H.T. Wang, and Y.J. Tian: J. Appl. Phys., 2009, vol. 105, pp. 043509.

    Article  Google Scholar 

  5. S. Kumar, N. Kamaraju, K.S. Vasu, A. Nag, A.K. Sood, and C.N.R. Rao: Chem. Phys. Lett., 2010, vol. 499, pp. 152-57.

    Article  CAS  Google Scholar 

  6. M.A. Mannan, M. Nagano, T. Kida, N. Hirao, and Y. Baba: J. Phys. Chem. Solids, 2009, vol. 70, pp. 20–25.

    Article  Google Scholar 

  7. K. Raidongia, Kpss. Hembram, U.V. Waghmare, M. Eswaramoorthy, and C.N.R. Rao: Z. Anorg. Allg. Chem., 2010, vol. 636, pp. 30–35.

  8. J.L. He, Y.J. Tian, D.L. Yu, T.S. Wang, S.M. Liu, L.C. Guo, D.C. Li, X.P. Jia, L.X. Chen, G.T. Zou, and O. Yanagisawa: Chem. Phys. Lett., 2001, vol. 340, pp. 431–36.

    Article  CAS  Google Scholar 

  9. S. Nakano, M. Akaishi, T. Sasaki, and S. Yamaoka: Chem. Mater., 1994, vol. 6, pp. 2246–51.

    Article  CAS  Google Scholar 

  10. T. Sasaki, M. Akaishi, S. Yamaoka, Y. Fujiki, and T. Oikawa: Chem. Mater., 1993, vol. 5, pp. 695–99.

    Article  CAS  Google Scholar 

  11. Y.H. Wang, Q.Z. Chen, J. Cho, and A.R. Boccaccini: Surf. Coat. Technol., 2007, vol. 201, pp. 7645–51.

    Article  CAS  Google Scholar 

  12. D.X. Li, D.L. Yu, B. Xu, J.L. He, Z.Y. Liu, P. Wang, and Y.J. Tian: Cryst. Growth Des., 2008, vol. 8, pp. 2096–2100.

    Article  CAS  Google Scholar 

  13. Y. Kobayashi and T. Akasaka: J. Cryst. Growth, 2008, vol. 310, pp. 5044–47.

    Article  CAS  Google Scholar 

  14. V. Pokropivny, S. Kovrygin, V. Gubanov, R. Lohmus, A. Lohmus, and U. Vesi: Physica E, 2008, vol. 40, pp. 2339–42.

    Article  CAS  Google Scholar 

  15. M. Ben el Mekki, M.A. Djouadi, E. Guiot, V. Mortet, J. Pascallon, V. Stambouli, D. Bouchier, N. Mestres, and G. Nouet: Surf. Coat. Tech., 1999, vols. 116–119, pp. 93–99.

  16. F. Tuinstra and J.L. Koenig: J. Chem. Phys., 1970, vol. 53, pp. 1126–30.

    Article  CAS  Google Scholar 

  17. R.J. Nemanich and S.A. Solin: Phys. Rev. B, 1979, vol. 20, pp. 392–401.

    Article  CAS  Google Scholar 

  18. Y.K. Yap, M. Yoshimura, Y. Mori, and T. Sasaki: Appl. Phys. Lett., 2002, vol. 80, pp. 2559–61.

    Article  CAS  Google Scholar 

  19. J. Yu, J. Ahn, S.F. Yoon, Q. Zhang, Rusli, B. Gan, K. Chew, M.B. Yu, X.D. Bai, and E.G. Wang: Appl. Phys. Lett., 2000, vol. 77, pp. 1949–51.

  20. C.Y. Zhi, X.D. Bai, and E.G. Wang: Appl. Phys. Lett., 2002, vol. 80, pp. 3590–92.

    Article  CAS  Google Scholar 

  21. C.Y. Zhi, X.D. Bai, and E.G. Wang: Appl. Phys. Lett., 2004, vol. 84, pp. 1549–51.

    Article  CAS  Google Scholar 

  22. S.Z. Bai, B. Yao, B.K. Huang, S.J. Zhang, Z.H. Ding, X.Y. Guo, X.D. Zhou, and W.H. Su: Chem. J. Chinese U., 2005, vol. 26, pp. 811–15.

    CAS  Google Scholar 

  23. A.R. Phani: Bull. Mater. Sci., 1994, vol. 17, pp. 219–24.

    Article  CAS  Google Scholar 

  24. Z.F. Zhou, I. Bello, M.K. Lei, K.Y. Li, C.S. Lee, and S.T. Lee: Surf. Coat. Technol., 2000, vols. 128–129, pp. 334–40.

  25. Y.M. Chen, Z.X. Zeng, S.R. Yang, and J.Y. Zhang: Diamond Relat. Mater., 2009, vol. 18, pp. 20–26.

    Article  Google Scholar 

  26. H.S. Kim, I.H. Choi, and Y.J. Baik: Surf. Coat. Technol., 2000, vols. 133-134, pp. 473–77.

Download references

The authors acknowledge financial support from Huaqiao University (grants 09BS503 and 10BS112) and MMST (grants 201102).

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to Dongxu Li.

Additional information

Manuscript submitted March 23, 2011.

Rights and permissions

Reprints and permissions

About this article

Cite this article

Li, D., Lu, J., Yu, D. et al. Study on Raman Spectroscopy and Purification of B-C-N Compound. Metall Mater Trans A 42, 2527–2529 (2011). https://doi.org/10.1007/s11661-011-0819-4

Download citation

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s11661-011-0819-4

Keywords

Navigation