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Reduction of Anisotropy in Cold-Rolled Duplex Stainless Steel Sheets by Using Sigma Phase Transformation

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Abstract

The mechanical properties of rolled duplex stainless steel (DSS) products manufactured by the current industrial process exhibit a strong anisotropy. This fact is evidently due to the two-phase nature of DSSs. During industrial rolling, not only the morphology of the microstructure changes from coarse-grained isotropic in the cast slab to fine-grained anisotropic in the coil, with both phases elongated in the rolling direction (RD), but also clear and intense crystallographic rolling textures develop, especially in the ferritic phase. The objective of the present work was to modify the industrial processing route and parameters in such a way that the strong anisotropy of DSS coils and sheets is decreased and the amount of potential applications made from DSSs by deep drawing or roll forming operations is increased. To achieve this goal, after the industrial cold rolling, a heat treatment is proposed with the aim of modifying the morphology and crystallographic texture of the ferritic grains by the assistance of an enforced transformation to sigma phase. The final product obtained by this modified route showed a microstructure with grains of austenite and ferrite randomly distributed and a significant decrease of the texture intensities due to the retransformation of sigma into ferrite. As a result, DSS EN 1.4462 displayed an almost isotropic mechanical behavior and an improved aptitude to deep drawing operations.

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References

  1. J.O. Nilsson: Mater. Sci. Technol., 1992, vol. 8, pp. 685–700.

    CAS  Google Scholar 

  2. P. Lovland: Stainless Steel Europe, 1993, pp. 28–37.

  3. K. Johansson: Proc. 6th Duplex Stainless Steels Conf., Associazione Italiana Metallurgia, Venezia, 2000, pp. 13–20.

    Google Scholar 

  4. M. Liljas: Proc. 6th Duplex Stainless Steel Science and Market Conf., Pentti Karjalainen and Staffan Hertman, eds., Helsinki, 2008, pp. 535–40.

  5. M.P. Esteban, A. Iza-Mendia, and I. Gutiérrez: Proc. 6th Duplex Stainless Steel Science and Market Conf., Pentti Karjalainen and Staffan Hertman, eds., Helsinki, 2008, pp. 547–53.

  6. I. Gutiérrez and A. Iza-Mendia: Duplex Stainless Steels, 1st ed., John Wiley & Sons Inc., London, 2009.

    Google Scholar 

  7. W.B. Hutchinson, K. Ushiola, and G. Runnsjö: Mater. Sci. Technol., 1985, vol. 1, pp. 728–31.

    CAS  Google Scholar 

  8. W.B. Hutchinson, U.V. Schlippenbach, and J. Jonsson: Proc. Duplex Stainless Steels ’86, Anon, The Netherlands, 1986, pp. 326–30.

    Google Scholar 

  9. J.L. Song and P.S. Bate: Acta Mater., 1997, vol. 45 (7), pp. 2747–57.

    Article  CAS  Google Scholar 

  10. A. Mateo, L. Llanes, N. Akdut, J. Stolarz, and M. Anglada: Int. J. Fat., 2003, vol. 25, pp. 481–88.

    Article  CAS  Google Scholar 

  11. G. Dieter: Mechanical Metallurgy, SI Metric edn., McGraw-Hill Book Company, London, 1988.

  12. A. Ul-Haq, H. Weiland, and H.J. Bunge: Mater. Sci. Technol.,1994, vol. 10, pp, 289–98.

    CAS  Google Scholar 

  13. L. Duprez, B.C. De Cooman, and N. Akdut: Steel Res., 2001, vol. 72, pp. 311–16.

    CAS  Google Scholar 

  14. G. Fargas, N. Akdut, M. Anglada, and A. Mateo: ISIJ Int., 2008, vol. 48 (11), pp. 1596–1602.

    Article  CAS  Google Scholar 

  15. X.G. Wang, D. Dumortier, and Y. Riquier: Proc. Duplex Stainless Steels ’91, Editions de Physique, Beaune, France, 1991, pp. 127–34.

    Google Scholar 

  16. T. Mori, K. Kondo, M. Igarashi, Y. Murata, and K. Horiuchi: Proc. 5th World Conf. on Duplex Stainless Steels, KCI Publishing BV, Maastricht, The Netherlands, 1997, pp. 55–61.

    Google Scholar 

  17. J.O. Nilsson, P. Kangas, T. Karlsson, and A. Wilson: Metall. Mater. Trans. A, 2001, vol. 31A, pp. 35–45.

    Google Scholar 

  18. W. Reick, M. Pohl, and A.F. Padihla: ISIJ Int., 1998, vol. 38 (6), pp. 567–71.

    Article  CAS  Google Scholar 

  19. T. Ito, R. Matsuki, and H. Aoyama: Proc. 3rd Eur. Conf. Stainless Steels Science and Market, AIM, Sardinia, Italy, 1999, pp. 1–9.

    Google Scholar 

  20. G. Fargas, M. Anglada, and A. Mateo: J. Mater. Process. Technol., 2009, vol. 209, pp. 1770–82.

    Article  CAS  Google Scholar 

  21. K. Forch, C.H. Gillessen, I. von Hagen, and W. Weißling: Stahl Eisen., 1992, vol. 112, pp. 53–62.

    CAS  Google Scholar 

  22. H.C. Lee and J. Gurland: Mater. Sci. Eng., 1978, vol. 41, pp. 125–33.

    Google Scholar 

  23. ASTM E517-81: Annual Book of ASTM Standards, Philadelphia, PA, p. 03.01.

  24. ISO 11531, International Standards, 1994.

  25. W.C. Oliver and G.M. Pharr: J. Mater. Res., 1992, vol. 7 (6), pp. 1564–82.

    Article  CAS  Google Scholar 

  26. L. Karlsson: Proc. Duplex Stainless Steel ’97, KCI Publishing BV, Maastricht, The Netherlands, 1997, pp. 43–58.

    Google Scholar 

  27. D. Villalobos, A. Arbiter, and C. Maldonado: Rev. Mater., 2009, vol. 14 (3), pp. 1061–69.

    Article  CAS  Google Scholar 

  28. A. Ul-Haq, H. Weiland, and H. Bunge: J. Mater. Sci., 1994, vol. 29, pp. 2168–76.

    Article  Google Scholar 

  29. J. Keichel, G. Gottstein, and J. Foct: Proc. High Nitrogen Steel ’98, Trans Tech Publications Ltd., Stockholm, 1998, pp. 785–92.

    Google Scholar 

  30. J. Hirsch and K. Lücke: Acta Metall., 1988, vol. 36, pp. 2863–81.

    Article  CAS  Google Scholar 

  31. H.P. Stüwe and J. Faustmann: Introducción a las Texturas de los Materiales Metálicos, Montecorvo, Madrid, 1969.

  32. F.H. Humphreys and M. Hatherly: Recrystallization and Related Annealing Phenomena, Pergamon Press, New York, NY, 1996.

    Google Scholar 

  33. W.F. Hosford and W.A. Backofen: Fundamentals of Deformation Processing, Syracuse University Press, New York, NY, 1964.

    Google Scholar 

  34. K. Lange: Handbook of Metal Forming, McGraw-Hill Book Company, New York, NY, 1985.

    Google Scholar 

  35. W.F. Hosford and R.M. Caddell: Metal Forming. Mechanics and Metallurgy, 2nd ed. PTR Prentice Hall, Englewood Cliffs, NJ, 1993.

    Google Scholar 

  36. S. Kalpakjian: Manufacturing Processes for Engineering Materials, 3rd ed., Addison Wesley, Denton, NC, 1997.

    Google Scholar 

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Acknowledgments

One of the authors (AM) acknowledges the Spanish Ministerio de Ciencia e Innovación for the concession of Project No. MAT2009-14461 and the Direcció General de Recerca del Comissionat per a Universitats i Recerca de la Generalitat de Catalunya for recognizing CIEFMA as Grup de Recerca Consolidat 2009SGR 1285. The authors owe their gratitude to ALZ (today UGINE and ALZ, ArcelorMittal Group) for providing the material, to OCAS (today, next to OCAS, also Arcelor Research Industry Ghent, ArcelorMittal Group) for carrying out the texture measurements, and to the Technologic Center of Manresa (CTM) for its technical support in forming tests.

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Correspondence to G. Fargas.

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Manuscript submitted December 1, 2010.

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Fargas, G., Akdut, N., Anglada, M. et al. Reduction of Anisotropy in Cold-Rolled Duplex Stainless Steel Sheets by Using Sigma Phase Transformation. Metall Mater Trans A 42, 3472–3483 (2011). https://doi.org/10.1007/s11661-011-0744-6

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