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Microstructural characterization of secondary-phase particles in a hot-deformed Al-Cu-Mg-Zr alloy

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Abstract

Torsion tests, on a 2014 + 0.13Zr alloy, were performed at temperatures in the range 573 to 773 K under strain rates ranging from 10−3 to 10 s−1. Transmission electron microscopy (TEM) inspection was performed in order to establish the role of the hot deformation on the hardening second-phase particles. The pinning effect of Al3Zr particles was also investigated. At the testing temperatures, the Al3Zr particles were stable, and no significant statistic changes, in terms of density and mean size, occurred during the tests. Small Al3Zr dispersoid particles inhibit recrystallization by pinning the grain and subgrain boundaries during hot deformation. Yet, they are particularly resistant to dislocation shear microstructure mechanism. Grains were elongated and contained a large number of sub-grains a few microns in width.

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References

  1. G.B. Burger, A.K. Gupta, P.W. Jeffrey, and D.J. Lloyd: Mater. Characterization, 1995, vol. 35, p. 23.

    Article  CAS  Google Scholar 

  2. Y.A. Bagaryatsky: Dokl. Akad. SSSR, 1952, vol. 87, p. 397.

    Google Scholar 

  3. C.R. Hutchinson and S.P. Ringer: Metall. Mater. Trans. A, 2000, vol. 31A, p. 2721.

    CAS  Google Scholar 

  4. A.K. Gupta, P. Gaunt, and M.C. Chaturvedi: Phil. Mag. A, 1987, vol. 55A, p. 375.

    Google Scholar 

  5. C. Wolverton: Acta Mater., 2001, vol. 49, p. 3129.

    Article  CAS  Google Scholar 

  6. S.P. Ringer, S.K. Caraher, and I.J. Polmear: Scripta Mater., 1998, vol. 39 (11), p. 1559.

    Article  CAS  Google Scholar 

  7. S.P. Ringer, K. Hono, T. Sakurai, and I.J. Polmear: Scripta Mater., 1997, vol. 36 (5), p. 517.

    Article  CAS  Google Scholar 

  8. S. Abis, M. Massazza, P. Mengucci, and G. Riontino: Scripta Mater., 2001, vol. 45, p. 685.

    Article  CAS  Google Scholar 

  9. P. Wouters, B. Verlinden, H.J. McQueen, E. Aernoudt, L. Delaey, and S. Cauwenberg: Mater. Sci. Eng. A, 1990, vol. 123A, p. 239.

    Google Scholar 

  10. P.I. Gouma, D.J. Lloyd, and M.J. Mills: Mater. Sci. Eng. A, 2001, vols. 319A–321A, p. 439.

    Google Scholar 

  11. P. Ratchev, B. Verlinden, P. De Smet, and P. Van Houtte: Acta Mater., 1998, vol. 46 (10), p. 3523.

    Article  CAS  Google Scholar 

  12. V. Randomilovic, R. Kilaas, U. Dahmen, and G.J. Shiflet: Acta Mater., 1999, vol. 47 (15), p. 3987.

    Article  Google Scholar 

  13. L.M. Wang, H.M. Flower, and T.C. Lindley: Scripta Mater., 1999, vol. 41 (4), p. 391.

    Article  CAS  Google Scholar 

  14. B.Q. Li and F.E. Wawner: Acta Mater., 1998, vol. 46 (15), p. 5483.

    Article  CAS  Google Scholar 

  15. H. Fujita and C. Lu: Mater. Trans., JIM, 1992, vol. 33 (10), p. 892.

    CAS  Google Scholar 

  16. C. Cayron and P.A. Buffat: Acta Mater., 2000, vol. 48, p. 2639.

    Article  CAS  Google Scholar 

  17. K. Satya Prasad, A.A. Gokhale, A.K. Mukhopadhyay, D. Banejee, and D.B. Goel: Acta Mater., 1999, vol. 47 (8), p. 2581.

    Article  Google Scholar 

  18. N. Ryum: Acta Mater., 1969, vol. 17 (3), p. 269.

    Article  CAS  Google Scholar 

  19. E. Nes: Acta Mater., 1972, vol. 20 (4), p. 499.

    Article  CAS  Google Scholar 

  20. M. Furukawa, Y. Iwahashi, Z. Horita, M. Remoto, N.K. Tsenev, R.Z. Valiev, and T.G. Langdon: Acta Mater., 1997, vol. 45 (11), p. 4751.

    Article  CAS  Google Scholar 

  21. J.D. Robson and P.B. Pragnell: Acta Mater., 2001, vol. 49 (10), p. 599.

    Article  CAS  Google Scholar 

  22. A. Deschamps and Y. Bréchet: Mater. Sci. Eng. A, 1998, vol. 251A, p. 200.

    Google Scholar 

  23. G. Avramovic-Cingara, D.D. Perovic, and H.J. McQueen: Metall. Mater. Trans. A, 1996, vol. 27A, pp. 3478–90.

    Article  CAS  Google Scholar 

  24. K.I. Moon, K.Y. Chang, and K.S. Lee: J. Alloys Compounds, 2000, vol. 312, p. 273.

    Article  CAS  Google Scholar 

  25. F. Bardi, M. Cabibbo, E. Evangelista, S. Spigarelli, and M. Vuckevic: Mater. Sci. Eng. A, 2003, vol. 339A (1–2), p. 43.

    Google Scholar 

  26. E. Cerri, E. Evangelista, A. Forcellese, and H.J. McQueen: Mater. Sci. Eng. A, 1995, vol. 197A, p. 181.

    Google Scholar 

  27. M. Cabibbo, E. Evangelista, and S. Spigarelli: Mater. Sci. Forum, 2002, vols. 396–402, p. 807.

    Article  Google Scholar 

  28. R.D. Doherty: Met. Sci., 1982, vol. 16, p. 1.

    Article  Google Scholar 

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Cabibbo, M., Spigarelli, S. & Evangelista, E. Microstructural characterization of secondary-phase particles in a hot-deformed Al-Cu-Mg-Zr alloy. Metall Mater Trans A 35, 293–300 (2004). https://doi.org/10.1007/s11661-004-0130-8

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  • DOI: https://doi.org/10.1007/s11661-004-0130-8

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