Summary
This study aimed to assess the measurement uncertainty of a new method for determination of allura redin food by high performance liquid chromatography (HPLC). The uncertainty of mathematical model of allura red is based on Europe for Analytical Chemistry(EURACHEM) guidelines. The sources and components of uncertainty were calculated, including recovery, working solution, sample mass, final volume, response of standard solution, response of sample solution. The expanded uncertainty was 0.0024 (k=2). Uncertainty of working solution was the most significant factor contributing to the total uncertainty, accounting for 86.2%. The uncertainty of volume accounted for the minimum at 0.025%. The developed method is simple and accurate, which can be used for the determination of allura redin puffed samples.
Similar content being viewed by others
References
Pourreza N, Rastegarzadeh S, Larki A. Determination of Allura red in food samples after cloud point extraction using mixed micelles. Food Chemistry, 2011,126(3):1465–1469
Yu Y, Fan Z. Magnetic solid-phase extraction coupled with HPLC for the determination of Allura Red in food and beverage samples. Food Addit Contam Part A Chem Anal Control Expo Risk Assess, 2016,33(10):1527–1534
Shi Y, Li C, Liu S, et al. A novel method for detecting allura red based on triple-wavelength overlapping resonance Rayleigh scattering, Rsc Advances, 2014,4(70):37100–37106
Zhang J, Zhang S, Wang X, et al. Simultaneous determination of Ponceau-4R and Allura Red in soft drinks based on the ionic liquid modified expanded graphite paste electrode. Int J Environ An Ch, 2015,95(7):581–591
Claramunt I, Perez L. Estimation of measurement uncertainty in the determination of orthophosphates in seawater by continuous flow analysis (CFA). Accred Qual Assur, 2014,19(3):205–212
Chen Y, He C, Cheng JJ, et al. Measurement uncertainty assessment of magnesium trisilicate column for determination of sudan colorants in food by HPLC using C8 column. J Huazhong Univ Sci Technolog Med Sci, 2016,36(5)752–757
Ramsey MH, Ellison SLR. Uncertainty factor: an alternative way to express measurement uncertainty in chemical measurement. Accred Qual Assur, 2015,20(2):153–155
Ramser MH, Ellison SL. Ellison uncertainty factor: an alternative way to express measurement uncertainty in chemical measurement. Accred Qual Assur, 2015,20(2):153–155
Yu ZR, Ning Y, YuH, et al. A HPLC-Q-TOFMS-based urinary metabolomic approach to identification of potential biomarkers of metabolic syndrome. J Huazhong Univ Sci Technolog Med Sci, 2014,34(2):276–283
Liu YN, Huang JG, Liu JM, et al. A simple and sensitive liquid chromatographic technique for the determination of cefotetan disodium in human plasma and its application in a pharmacokinetic study. J Huazhong Univ Sci Technolog Med Sci, 2012,32(5):779–784
Chen Y, Shao SW, Shen GX, et al. Determination of Fancy red in Puffing Food by HPLC. Zhong Guo Min Kang Yi Xue (Chinese), 2006,18(10):837–838
Kristiansen J. Description of a generally applicable model for the evaluation of uncertainty of measurement in clinical chemistry. Clin Chem Lab Med, 2005,39(10):920–931
Maroto A, Boque R, Rius FX. Estimating uncertainties of analytical results using information from the validation process. Analytica Chimica Acta, 1999, 391(99):173–185
Ma ZD, Wang FC, Hao DS. The uncertainty evaluation of determination of aflatoxin by HPLC post-column derivation method. Acta Metrologica Sinica, 2002,23(3):229–240
Basak S, Kundu D. Evaluation of measurement uncertainty components associated with the results of complexometric determination of calcium in ceramic raw materials using EDTA. Accred Qual Assur, 2013,18(3):235–241
Author information
Authors and Affiliations
Corresponding author
Additional information
The paper is supported by the Foundation of Study on Early Damage and Markers of Atmospheric Particulates in Hubei province (No. WJ2015MB123).
Rights and permissions
About this article
Cite this article
Chen, Y., Zhao, Y., Wang, HM. et al. Measurement Uncertainty Assessment for Determination of Allura Red in Puffed Food by HPLC. CURR MED SCI 38, 324–328 (2018). https://doi.org/10.1007/s11596-018-1882-5
Received:
Revised:
Published:
Issue Date:
DOI: https://doi.org/10.1007/s11596-018-1882-5