Skip to main content
Log in

Influence of Annealing Treatment on Microstructure Evolution and Mechanical Property of Friction Stir Weld AZ31 Mg Alloys

  • Metallic materials
  • Published:
Journal of Wuhan University of Technology-Mater. Sci. Ed. Aims and scope Submit manuscript

Abstract

In order to improve microstructure distribution and mechanical properties of Mg alloy joint by annealing treatment, die-casting AZ31 Mg alloy was successfully welded at rotation speed of 1 400 rpm and travel speed of 200 mm/min. The welded joints were annealed at 150–300 °C for 15–120 min and then were subjected to transverse tensile. The microstructure of annealed joints was analyzed by optical microscopy and electron backscatter diffraction. The experimental results indicate that (0001) texture intensity in stir zone significantly reduces and sharp transition of grain size is relieved in the interface between stir zone and thermo-mechanically affected zone after annealed at 200 °C for 30 min. Meanwhile, the elongation is increased from 7.5% to 13.0% and strength is increased slightly. It is because that annealing treatment can inhibit twin transformation and retain its ability to coordinate deformation during tensile deformation, which contributes to the improvement of plasticity. In addition, annealing treatment can increase the width of interfacial transition zone and lead to gradual transition of grain size between the SZ and TMAZ, which balances dislocation diffusion rate in different zone.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Similar content being viewed by others

References

  1. Luo AA. Magnesium Casting Technology for Structural Applications[ J]. Jounal of Magnesium Alloys, 2013, 1(1): 2–22

    Article  Google Scholar 

  2. Chen XP, Wang LX, Xiao R, et al. Comparison of Annealing on Microstructure and Anisotropy of Magnesium Alloy AZ31 Sheets Processed by Three Different Routes[J]. Jounal of Alloys and Compounds, 2014, 604(9): 112–116

    Article  Google Scholar 

  3. Taylor GI. Plastic Strain in Metals[J]. Jounal of the Institute of Metals, 1938, 62: 307–324

    Google Scholar 

  4. Hector JLG, Trinkle DR, Yasi JA. First–principles Data for Solid–solution Strengthening of Magnesium: From Geometry and Chemistry to Properties[J]. Acta Materialia, 2010, 58(17): 5 704–5 713

    Article  Google Scholar 

  5. Zhao B, Debroy T. Pore Formation during Laser Beam Welding of Die–Cast Magnesium Alloy AM60B Mechanism and Remedy[J]. Welding Journal Research Suppliment, 2001, 204–210

    Google Scholar 

  6. Yang J, Wang D, Xiao BL, et al. Effects of Rotation Rates on Microstructure, Mechanical Properties, and Fracture Behavior of Friction Stir–welded (FSW) AZ31 Magnesium Alloy[J]. Metallurgical and Materials Transactions A, 2013, 44(1): 517–530

    Article  Google Scholar 

  7. Mishra RS, Mahoney MW. Friction Stir Welding and Processing[J]. Materials Science & Engineering R Reports, 2005, 50(1–2): 1–78

    Article  Google Scholar 

  8. Templeman Y, Hamu GB, Meshi L. Friction Stir Welded AM50 and AZ31 Mg Alloys: Microstructural Evolution and Improved Corrosion Resistance[J]. Materials Characterization, 2017, 126: 86–95

    Article  Google Scholar 

  9. Park SHC, Sato YS, Kokawa H. Effect of Micro–texture on Fracture Location in Friction Stir Weld of Mg Alloy AZ61 during Tensile Test[J]. Scripta Materialia, 2003, 49(2): 161–166

    Article  Google Scholar 

  10. Chang CI, Lee CJ, Huang JC. Relationship between Grain Size and Zener–Holloman Parameter during Friction Stir Processing in AZ31 Mg Alloys[J]. Scripta Materialia, 2004, 51(6): 509–514

    Article  Google Scholar 

  11. Suhuddin UFHR, Mironov S, Sato YS, et al. Grain structure evolution during friction–stir welding of AZ31 magnesium alloy[J]. Acta Materialia, 2009, 57(18): 5 406–5 418

    Article  Google Scholar 

  12. Mironov S, Onuma T, Sato YS, et al. Microstructure Evolution during Friction–stir Welding of AZ31 Magnesium Alloy[J]. Acta Mateialia., 2015, 100: 301–312

    Article  Google Scholar 

  13. Liu DJ, Xin RL, Xiao Y, et al. Strain Localization in Friction Stir Welded Magnesium Alloy during Tension and Compression Deformation[ J]. Materials Science and Engineering A, 2014, 609: 88–91

    Article  Google Scholar 

  14. Liu DJ, Xin RL, Yu HN, et al. Comparative Examinations on the Activity a Variant Section of Twinning during Tension and Compression of Magnesium Alloys[J]. Materials Science and Engineering A, 2016, 658: 229–236

    Article  Google Scholar 

  15. Chowdhury SH, Chen DL, Bhole SD, et al. Friction Stir Welded AZ31 Magnesium Alloy: Microstructure, Texture, and Tensile Properties[J]. Metallurgical and Materials Transactions A, 2012, 44(1): 323–336

    Article  Google Scholar 

  16. Liu DJ, Xin RL, Li ZY, et al. The Activation of Twinning and Texture Evolution during Bending of Friction Stir Welded Magnesium Alloys[ J]. Materials Science and Engineering A, 2015, 646: 145–153

    Article  Google Scholar 

  17. Xin RL, Liu DJ, Xu ZR, et al. Changes in Texture and Microstructure of Friction Stir Welded Mg Alloy during Post–rolling and Their Effects on Mechanical Properties[J]. Materials Science and Engineering A, 2013, 582(11): 178–187

    Article  Google Scholar 

  18. Lee CJ, Huang JC, Du XH. Improvement of Yield Stress of Friction–stirred Mg–Al–Zn Alloys by Subsequent Compression[J]. Scripta Materialia, 2007, 56(10): 875–878

    Article  Google Scholar 

  19. Song B, Pan H, Chai LJ, et al. Evolution of Gradient Microstructure in an Extruded AZ31 Rod during Torsion and Annealing and Its Effects on Mechanical Properties[J]. Materials Science & Engineering A, 2017, 689: 78–88

    Article  Google Scholar 

  20. Qin FM, Zhu H, Wang ZX, et al. Dislocation and Twinning Mechanisms for Dynamic Recrystallization of As–cast Mn18Cr18N Steel[J]. Materials Science & Engineering A, 2017, 684: 634–644

    Article  Google Scholar 

  21. Mohan A, Yuan W, Mishra RS. High Strain Rate Superplasticity in Friction Stir Processed Ultrafine Grained Mg–Al–Zn Alloys[J]. Materials Science & Engineering A, 2013, 562: 69–76

    Article  Google Scholar 

  22. Yuan W, Mishra RS, Carlson B, et al. Material Flow and Microstructural Evolution during Friction Stir Spot Welding of AZ31 Magnesium Alloy[J]. Materials Science & Engineering A, 2012, 543: 200–209

    Article  Google Scholar 

  23. Wang XH, Wang KS. Microstructure and Properties of Friction Stir Butt–welded AZ31 Magnesium Alloy[J]. Materials Science & Engineering A, 2006, 431: 114–117

    Article  Google Scholar 

  24. Shan Q, Ni DR, Xue P, et al. Improving Joint Performance of Friction Stir Welded Wrought Mg Alloy by Controlling Non–uniform Deformation Behavior[J]. Materials Science & Engineering A, 2017, 707: 426–432

    Article  Google Scholar 

  25. Xin RL, Liu DJ, Shu XG, et al. Influence of Welding Parameter on Texture Distribution and Plastic Deformation Behavior of As–rolled AZ31 Mg alloys[J]. Journal of Alloys & Compounds, 2016, 670: 64–71

    Article  Google Scholar 

  26. Fong KS, Danno A, Tan MJ, et al. Tensile Flow Behavior of AZ31 Magnesium Alloy Processed by Severe Plastic Deformation and Post–annealing at Moderately High Temperatures[J]. Journal of Materials Processing Technology, 2017, 246: 235–244

    Article  Google Scholar 

  27. Kim WJ, Jeong HG, Jeong HT. Achieving High Strength and High Ductility in Magnesium Alloys Using Severe Plastic Deformation Combined with Low–temperature Aging[J]. Scripta Mateialia., 2009, 61(11): 1 040–1 043

    Article  Google Scholar 

  28. Ovid’ko IA, Langdon TG. Enhanced Ductility of Nanocrystalline and Ultrafine–grained Metals[J]. Reviews on Advanced Materials Science, 2012, 30: 103–115

    Google Scholar 

  29. Yoo MH. Slip, twinning, and Fracture in Hexagonal Close–packed Metals[J]. Metallurgical and Materials Transactions A, 1981, 12(3): 409–418

    Article  Google Scholar 

  30. Wu L, Agnew SR, Brown DW, et al. Internal Stress Relaxation and Load Redistribution during the Twinning–detwinning–dominated Cyclic Deformation of a Wrought Magnesium Alloy ZK60A[J]. Acta Materialia, 2008, 56(14): 3 699–3 707

    Article  Google Scholar 

  31. Barnett MR. Twinning and the Ductility of Magnesium Alloys Part I: “Tension” Twins[J]. Materials Science & Engineering A, 2007, 464(1): 1–7

    Article  Google Scholar 

  32. Liu Z, Xin RL, Wu X, et al. Improvement in the Strength of Friction–stir–welded ZK60 Alloys Via Post–weld Compression and Aging Treatment[J]. Materials Science & Engineering A, 2018, 712: 493–499

    Article  Google Scholar 

Download references

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to Zhisheng Wu  (吴志生).

Additional information

Funded by the Fund for Shanxi Key Subjects Construction, the National Natural Science Foundation of China (No. 51275332), and the Natural Science Foundation of Shanxi Province (No. 201601D011036)

Rights and permissions

Reprints and permissions

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Li, Y., Qin, F., Liu, C. et al. Influence of Annealing Treatment on Microstructure Evolution and Mechanical Property of Friction Stir Weld AZ31 Mg Alloys. J. Wuhan Univ. Technol.-Mat. Sci. Edit. 34, 417–425 (2019). https://doi.org/10.1007/s11595-019-2068-0

Download citation

  • Received:

  • Accepted:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s11595-019-2068-0

Key words

Navigation