Skip to main content
Log in

Studies on injector pump-ultrasonic nebulizer feeding sample system for MPT-AES

  • Research Article
  • Published:
Frontiers of Chemistry in China

Abstract

The feeding-sample system used by microwave plasma torch atomic emission spectroscopy (MPT-AES) is the pneumatic nebulization system; its efficiency, however, is not good. A newly built injector pump-ultrasonic nebulizer combination feeding-sample system has been designed. Its performance was tested and compared with that of the pneumatic nebulization system. It can be concluded that the newly built feeding-sample system can increase the spectral line intensity by about two to three times and decrease the detection limit by about 2 to 10 times. Moreover, this newly built system can reduce the time taken washing the sample cell from 30 min or so to about 10 min.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Similar content being viewed by others

References

  1. Gong Z., Liang F. and Yang P., Atomic/ionic fluorescence in microwave plasma torch discharge excited by high current microsecond-pulsed hollow cathode lamp-Europium atomic/ionic fluorescence spectrometry, Spectrosc. Spectr. Anal., 1999, 19(3): 356–359 (in Chinese)

    CAS  Google Scholar 

  2. Barnes J. H., Gron O. A. and Hieftje G. M., Characterization of an argon microwave plasma torch coupled to a Mattauch-Herzog geometry mass spectrometer, J. Anal. At. Spectrom., 2002, 17: 1132–1136

    Article  CAS  Google Scholar 

  3. Shi Y., Zheng J. and Wang M., Studies on argon microwave plasma torch as gas chromatographic ionization detector, J. Jilin Univ. (Science Edition), 2003, 41(3): 378–383 (in Chinese)

    CAS  Google Scholar 

  4. Liang F., Zhang D., Lei Y., Zhang H. and Jin Q., Determination of selected noble metals by MPT-AES using a pneumatic nebulizer, Microchem. J., 1995, 52(2): 181–187

    Article  CAS  Google Scholar 

  5. Jankowski K., Karmasz D., Starski L., Ramsza A. and Waszkiewicz A., Characteristics of nebulizers for microwave-induced plasma atomic emission spectrometry: I. Pneumatic nebulizers, Spectrochim. Acta, 1997, 52B(12): 1801–1812

    CAS  Google Scholar 

  6. Wendt R. H. and Fassel V. A., Induction-coupled plasma spectrometric excitation source, Anal. Chem., 1965, 37(7): 920–922

    Article  CAS  Google Scholar 

  7. West C. D. and Jume D. N., Rapidfrequency plasma emission spectrophotometer, Anal. Chem., 1964, 36(2): 412–415

    Article  CAS  Google Scholar 

  8. Goulden P. D. and Anthony D. H. J., Modified ultrasonic nebulizer for inductively coupled argon plasma atomic emission spectrometry, Anal. Chem., 1984, 56(13): 2327–2329

    Article  CAS  Google Scholar 

  9. Li Y., Duan Y. and Zhang H., Studies on microwave plasma torch-atomic fluorescence spectrometry with an ultrasonic nebulization introduction system, Chinese J. Anal. Lab., 1996, 15(3): 24–27 (in Chinese)

    Google Scholar 

  10. Zhang J., Yang W. and Wei J., Study on the ultrasonic nebulizer for ICP-AES, J. Instrumental Anal., 1995, 14(6): 82–85 (in Chinese)

    CAS  Google Scholar 

  11. Jin Q., Zhu C., Brushwyler K., Hieftje G. M., An efficient and inexpensive ultrasonic nebulizer for atomic spectrometry, Appl. Spectrosc., 1990, 44: 183–186

    Article  CAS  Google Scholar 

  12. Clifford R. H., Montaser A., Dotan S. P. and Capar S. G., Conversion of an ultrasonic humidifier to a continuous-type ultrasonic nebulizer for atomic spectrometry, Anal. Chem., 1990, 62: 2745–2749

    Article  CAS  Google Scholar 

  13. Petrucci G. A. and van Loon J. C., Studies of ultrasonic nebulizer parameters in search of a simple, reliable system, Spectrochim. Acta, 1990, 45B: 959–968

    CAS  Google Scholar 

Download references

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to Feng Guodong.

Additional information

__________

Translated from Journal of JiLin University(Science edition), 2005, 43(4)(in Chinese)

About this article

Cite this article

Feng, G., Han, S. & Yu, A. Studies on injector pump-ultrasonic nebulizer feeding sample system for MPT-AES. Front. Chem. China 1, 232–237 (2006). https://doi.org/10.1007/s11458-006-0010-4

Download citation

  • Issue Date:

  • DOI: https://doi.org/10.1007/s11458-006-0010-4

Keywords

Navigation