Abstract
Rosin glycerin ester and its bromide were prepared from natural renewable rosin, glycerin and liquid bromine which were first subjected to an esterification reaction, followed by an addition reaction. Their structures were characterized by an infrared (IR) spectrum and their thermal resistance was conducted with thermal gravity (TG) and differential scanning calorimetry (DSC). It showed that the bromide in the rosin glycerin ester decomposed faster than the ester; hence it may be used as fire-resistant material.
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Atta Ayman M., Mansour R., Abdou Mahmoud I. and Sayed Ashraf M., Polym. Adv. Technol., 2004, 15(9): 514–522
Zhang Y. and Hourston D. J., J. Appl. Polym. Sci., 1998, 69(2): 271–281
Zhang Y., Shang S., Zhang X., Wang D. and Hourston D. J., J. Appl. Polym. Sci., 1996, 59(7): 1167–1171
Jin Jian Feng, Chen Yong Ling, Wang De Ning, Hu Chun Pu, Zhu Stella, Vanoverloop Lieve and Randall David, J. Appl. Polym. Sci., 2002, 84(3): 598–604
Sánchez-Adsuar M. S., Papon E. and Villenave J.-J., J. Appl. Polym. Sci., 2001, 82(14): 3402–3408
Li Chuncheng, Li Wei, Wang Hui, Zhang Dong and Li Zhenyi, J. Appl. Polym. Sci., 2003, 88(12): 2804–2809
Mayer M. J. J., Meuldijk J. and Thoenes D., J. Appl. Polym. Sci., 1995, 56(2): 119–126
Mayer M. J. J., Meuldijk J. and Thoenes D., J. Appl. Polym. Sci., 1996, 59(6): 1047
Hayashi Shunji, Kim Hyun-Joong, Kajiyama Mikio, Ono Hirokuni, Mizumachi Hiroshi and Zufu Zhou, J. Appl. Polym. Sci., 1999, 71(4): 651–663
Wu Zong-Hua, Chen Shao-Ping and Tanaka Hiroo, J. Appl. Polym. Sci., 1997, 65(11): 2159–2163
Satturwar P. M., Mandaogade P. M., Fulzele S. V., Darwhekar G. N., Joshi S. B. and Dorle A. K., Drug Dev. Ind. Pharm., 2002, 28(4): 381–387
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Yu, C., Zhang, F. Preparation and characterization of rosin glycerin ester and its bromide. Front. Chem. China 1, 158–160 (2006). https://doi.org/10.1007/s11458-006-0006-0
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DOI: https://doi.org/10.1007/s11458-006-0006-0