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Influence of Deformation Temperature On Flow Stress and Dislocation Structure of 2A12 Aluminum Alloy Under Quasi-Static and Dynamic Compression

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Abstract

Background

In many constitutive models for dynamic strain aging of aluminum alloys, the athermal component of flow stress was commonly assumed to be independent of temperature and strain rate. However, the assumption has not been examined experimentally due to lacking of a reliable and quantitative method to obtain statistical information of dislocation structure in the deformed aluminum alloys.

Objective

Develop a novel X-ray diffraction procedure to characterize the evolution of dislocation structure in aluminum alloys over a wide range of temperatures and strain rates, and further clarify the contributions arising from the structural and thermal components of flow stress.

Methods

The quasi-static and dynamic compression of artificial aged 2A12 aluminum alloy was carried out at the strain rates of 5×10-3 and 1×103 s-1 and within a temperature range of 173-673 K. The dislocation structure in the deformed aluminum alloy was determined by the newly developed X-ray line profile analysis procedure (CMWP). In combination with mechanical and X-ray diffraction tests, the correlation between the flow stress and microstructure for the aluminum alloy was established.

Results

X-ray diffraction measurements showed the dislocation density in the deformed 2A12 aluminum alloy is temperature and strain rate dependence. Besides the structural or athermal component of flow stress calculated from the measured microstructure parameters, a bell-shaped flow stress was revealed clearly in the total flow stress, which can be attributed primarily to the dynamic strain aging mechanism.

Conclusions

In this work, a fairly concise routine was proposed to characterize the microstructure and estimate the deformation mechanism for the 2A12 aluminum alloy, and the methodology could be easily extended to other alloys.

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Data Availability

The data that support the findings of this study are available from the corresponding author upon reasonable request.

References

  1. Chen GQ, Liu JP, Shu X, Gu H, Zhang BG, Feng JC (2019) Beam scanning effect on properties optimization of thick-plate 2A12 aluminum alloy electron-beam welding joints. Mater Sci Eng A 744:583–592

    Google Scholar 

  2. Jiang JF, Zhang Y, Wang Y, Xiao GF, Liu YZ, Zeng L (2020) Microstructure and mechanical properties of thixoforged complex box-type component of 2A12 aluminum alloy. Mater Des 193:108859

    Google Scholar 

  3. Zhang HJ, Zhao XH, Liu Y (2021) Effect of high frequency impacting and rolling on fatigue crack growth of 2A12 aluminum alloy welded joint Int. J Fatigue 147:106172

    Google Scholar 

  4. Nakai M, Eto T (2000) New aspect of development of high strength aluminum alloys for aerospace applications. Mater Sci Eng A 285:62–68

    Google Scholar 

  5. Dursun T, Soutis C (2014) Recent developments in advanced aircraft aluminium alloys. Mater Design 56:862–871

    Google Scholar 

  6. Barlat F, Glazov MV, Brem JC, Lege DJ (2002) A simple model for dislocation behavior, strain and strain rate hardening evolution in deforming aluminum alloys. Int J Plast 18:919–939

    MATH  Google Scholar 

  7. Horváth G, Chinh NQ, Gubicza J, Lendvai J (2007) Plastic instabilities and dislocation densities during plastic deformation in Al-Mg alloys. Mater Sci Eng A 445–446:186–192

    Google Scholar 

  8. Fribourg G, Bréchet Y, Deschamps A, Simar A (2011) Microstructure-based modelling of isotropic and kinematic strain hardening in a precipitation-hardened aluminium alloy. Acta Mater. 59:3621–3635

    Google Scholar 

  9. Lin YC, Li QF, Xia YC, Li LT (2012) A phenomenological constitutive model for high temperature flow stress prediction of Al-Cu-Mg alloy. Mater Sci Eng A 534:654–662

    Google Scholar 

  10. Khan AS, Liu HW (2012) Variable strain rate sensitivity in an aluminum alloy: Response and constitutive modeling. Int J Plast 36:1–14

    Google Scholar 

  11. Kabirian F, Khan AS, Pandey A (2014) Negative to positive strain rate sensitivity in 5xxx series aluminum alloys: Experiment and constitutive modeling. Int J Plast 55:232–246

    Google Scholar 

  12. Kreyca J, Kozeschnik E (2018) State parameter-based constitutive modelling of stress strain curves in Al-Mg solid solutions. Int J Plast 103:67–80

    Google Scholar 

  13. Johnson GR, Cook WH (1985) Fracture characteristics of three metals subjected to various strains, temperatures and pressures. Eng Fract Mech 21:31–48

    Google Scholar 

  14. Kubin LP, Estrin Y (1990) Evolution of dislocation densities and the critical conditions for the Portevin-Le Chateliereffect. Acta Metall Mater 38:697–708

    Google Scholar 

  15. Warren BE (1959) X-ray studies of deformed metals. Prog Met Phys 8:147–202

    Google Scholar 

  16. Groma I (1998) X-ray line broadening due to an inhomogeneous dislocation distribution. Phys Rev B 57:7535–7542

    Google Scholar 

  17. Ungár T, Dragomir I, Révész Á, Borbély A (1999) The contrast factors of dislocations in cubic crystals: the dislocation model of strain anisotropy in practice. J Appl Crystallogr 32:992–1002

    Google Scholar 

  18. Ungár T, Ribárik G, Balogh L (2010) Defect-related physical-profile-based X-ray and neutron line profile analysis. Met Mater Transact A41:1202–1209

    Google Scholar 

  19. Ribárik G, Jóni B, Ungár T (2019) Global optimum of microstructure parameters in the CMWP line-profile analysis method by combining Marquardt-Levenberg and Monte-Carlo procedures. J Mater Sci Technol 35:1508–1514

    Google Scholar 

  20. Gubicza J, Kassem M, Ribárik G, Ungár T (2004) The microstructure of mechanically alloyed Al–Mg determined by X-ray diffraction peak profile analysis. Mater Sci Eng A 372:115–122

    Google Scholar 

  21. Fátay D, Bastarash E, Nyilas K, Dobatkin S, Gubicza J, Ungár T (2003) X-ray diffraction study on the microstructure of an Al-Mg-Sc-Zr alloy deformed by high-pressure torsion. Z Metallkd 94:842–847

    Google Scholar 

  22. Yuan H, Chen Z, Buslaps T, Honkimäki V, Borbély A (2018) Combined texture and microstructure analysis of deformed crystals by high-energy X-ray diffraction. J Appl Cryst 51:883–894

    Google Scholar 

  23. Klepaczko JR (1975) Thermally activated flow and strain rate history effects for some polycrystalline FCC metals. Mater Sci Eng 18:121–135

    Google Scholar 

  24. Tsuji N, Toyoda T, Minamino Y, Koizumi Y, Yamane T, Komatsu M, Kiritani M (2003) Microstructural change of ultrafine-grained aluminum during high-speed plastic deformation. Mater Sci Eng A 350:108–116

    Google Scholar 

  25. Zhang B, Shim VPW (2010) Effect of strain rate on microstructure of polycrystalline oxygen-free high conductivity copper severely deformed at liquid nitrogen temperature. Acta Mater 58:6810–6827

    Google Scholar 

  26. Williamson GK, Hall WH (1953) X-ray line broadening from filed aluminium and wolfram. Acta Metall 1:22–31

    Google Scholar 

  27. Ungár T, Gubicza J, Ribárik G, Borbély A (2001) Crystallite size distribution and dislocation structure determined by diffraction profile analysis: principles and practical application to cubic and hexagonal crystals. J Appl Cryst 34:298–310

    Google Scholar 

  28. Hinds WC (1982) Aerosol Technology: Properties, Behavior and Measurement of Airborne Particles. Wiley, New York

  29. Krivoglaz MA (1996) X-ray and Neutron Diffraction in Non-ideal Crystals. Springer, Berlin, New York

    Google Scholar 

  30. Wilkens M (1970) Theoretical aspects of kinematical X-ray diffraction profiles from crystals containing dislocation distributions. in: J.A. Simmons, R. de Wit, R. Bullough (Eds.), NBS Fundamental Aspects of Dislocation Theory, Spec. Publ. 317, II, Washington, DC, USA, pp. 1195-1221

  31. Ungár T, Tichy G (1999) The effect of dislocation contrast on X-ray line profiles in untextured polycrystals. Phys Status Solidi 147:425–434

    Google Scholar 

  32. Borbély A, Dragomir-Cernatescu J, Ribárik G, Ungár T (2003) Computer program ANIZC for the calculation of diffraction contrast factors of dislocations in elastically anisotropic cubic, hexagonal and trigonal crystals J. Appl Crystallogr 36:160–162

    Google Scholar 

  33. Dieter GE (1988) Mechanical Metallurgy. McGraw-Hill, New York

    Google Scholar 

  34. Borbély A, Ungár T (2012) X-ray line profiles analysis of plastically deformed metals. C R Physique 13:293–306

    Google Scholar 

  35. Ungár T, Stoica AD, Tichy G, Wang X (2014) Orientation-dependent evolution of the dislocation density in grain populations with different crystallographic orientations relative to the tensile axis in a polycrystalline aggregate of stainless steel. Acta Mater 66:251–261

    Google Scholar 

  36. Meyers MA (1994) Dynamic Behavior of Materials. John Wiley & Sons, New York

    MATH  Google Scholar 

  37. Ungár T, Tichy G, Gubicza J, Hellmig RJ (2005) Correlation between subgrains and coherently scattering domains. J Powder Diffr 20:366–375

    Google Scholar 

  38. Fan Z, Jóni B, Ribárik G, Ódor É, Zs Fogarassy, Ungár T (2019) The Microstructure and strength of a V–5Cr–5Ti alloy processed by high pressure torsion. Mater Sci Eng A 758:139–146

    Google Scholar 

  39. Cordero ZC, Knight BE, Schuh CA (2007) Six decades of the Hall-Petch effect – a survey of grain-size strengthening studies on pure metals. Int Mater Rev 61:495–512

    Google Scholar 

  40. Taylor GI (1934) The mechanism of plastic deformation of crystals. Part I -Theoretical Proc R Soc Lond A 145:362–387

    MATH  Google Scholar 

  41. Gubicza J, Schiller I, Chinh NQ, Illy J, Horita Z, Langdon TG (2007) The effect of severe plastic deformation on precipitation in supersaturated Al-Zn-Mg alloys. Mater Sci Eng A 460–461:77–85

    Google Scholar 

  42. Guo WG, Gao XS (2013) On the constitutive modeling of a structural steel over a range of strain rates and temperatures. Mater Sci Eng A 561:468–476

    Google Scholar 

  43. Liu MP, Jiang TH, Wang J, Liu Q, Wu ZJ, Yu YD, Skaret PC, Roven HJ (2014) Aging behavior and mechanical properties of 6013 aluminum alloy processed by severe plastic deformation. Trans Nonferrous Met Soc China 24:3858–3865

    Google Scholar 

  44. Curtin WA, Olmsted DL, Hector LG (2006) A predictive mechanism for dynamic strain ageing in aluminium-magnesium alloys. Nat Mater 5:875–880

    Google Scholar 

  45. Guo WG (2007) Dynamic strain aging during the plastic flow of metals. Key Eng Mater 340–341:823–828

    Google Scholar 

  46. Keralavarma SM, Bower AF, Curtin WA (2014) Quantum-to-continuum prediction of ductility loss in aluminium-magnesium alloys due to dynamic strain aging. Nat Commun 5:4604

    Google Scholar 

  47. Wang JJ, Guo WG, Gao XS, Su J (2015) The third-type of strain aging and the constitutive modeling of a Q235B steel over a wide range of temperatures and strain rates. Int J Plast 65:85–107

    Google Scholar 

  48. Song Y, Garcia-Gonzalez D, Rusinek A (2020) Connstitutive models for dynamic strain aging in metals: strain rate and temperature dependences on the flow stress. Materials 13:1794

    Google Scholar 

  49. Yuan KB, Guo WG, Li DW, Li PH, Zhang Y, Wang PC (2021) Influence of heat treatments on plastic flow of laser deposited Inconel 718: Testing and microstructural based constitutive modeling. Int J Plast 136:102865

    Google Scholar 

Download references

Acknowledgements

Z.F. is grateful to the Director Foundation of China Academy of Engineering Physics (Grant No. YZ2019004) and the National Key Research and Development Program of China (No. 2021YFA1600604), Z.S. acknowledges the National Natural Science Foundation of China (Grant No. 11932018), G.R. & T.U. are grateful for the support of OTKA grant K124926 funded by the Hungarian National Research, Development and Innovation Office (NKFIH).

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Fan, Z., Song, Z., Xiao, D. et al. Influence of Deformation Temperature On Flow Stress and Dislocation Structure of 2A12 Aluminum Alloy Under Quasi-Static and Dynamic Compression. Exp Mech 63, 703–714 (2023). https://doi.org/10.1007/s11340-023-00950-1

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