Abstract
Positron annihilation spectroscopy and microhardness measurements were performed for pure iron samples after dry sliding. Well-defined depth profiles of edge dislocations decorated by vacancies and vacancy clusters were observed in the subsurface zone (SZ) of the samples studied. The vacancy clusters contained more than ten vacancies and their concentration decreased with the depth from the worn surface. Like in other metals studied, the depth profile of the defects detected exhibited the exponential decay with the depth. The total depth of the SZ was correlated with the load applied during sliding but did not exceed 220 μm. The defect profile in the SZ was revealed also in raw iron samples after dry sliding and blasted iron samples. In the case of raw iron, the profile induced by sliding overlaps defect structure which already exists in a raw material.





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Hirth, J.P., Rigney, D.A.: Crystal plasticity and the delamination theory of wear. Wear 39, 133–141 (1976)
Dryzek, J., Dryzek, E.: Subsurface zone studies in the AK 12 alloy and metal matrix composite AK 12 with Al2O3 using positron annihilation spectroscopy. Wear 261, 549–555 (2006)
Park, Yong-Ki, Waber, T.: Positron annihilation study of mechanically polished iron single crystals. Scr. Metall. 19, 1095–1100 (1985)
Dryzek, J., Polak, A.: Subsurface zone studied by positron lifetime measurements. Tribol. Lett. 7, 57–60 (1999)
Dryzek, J., Dryzek, E.: Subsurface zone in aluminium studied by positron lifetime spectroscopy. Tribol. Lett. 17, 147–153 (2004)
Dryzek, J., Dryzek, E., Suzuki, T., Yu, R.: Subsurface zone in pure magnesium studied by positron lifetime spectroscopy. Tribol. Lett. 20, 91–97 (2005)
Dryzek J.: Positron studies of subsurface zone created in sliding wear in bismuth. Tribol. Lett. 40, 175–180 (2010)
Kamimura, Y., Tsutsumi, T., Kuramoto, E.: Calculations of positron lifetimes in a jog and vacancies on an edge dislocation line in Fe. Phys. Rev. B 52, 879–885 (1995)
Puska, M.J., Nieminen, R.M.: Defect spectroscopy with positrons: a general calculated method. J. Phys. F Met. Phys. 13, 333–346 (1983); Phys. Rev. B 25, 762–780 (1982)
Campillo Robles, J.M., Ogando, E., Plazaola, F.J.: Positron lifetime calculation for the elements of the periodic table. J. Phys. Condens. Matter 19, 176222 (20 pp) (2007)
Dryzek, J., Dryzek, E.: The subsurface zone in magnesium alloy studied by positron annihilation techniques. Tribol. Int. 40, 1360–1368 (2007)
Vehanen, A., Hautojärvi, P., Johansson, J., Yli-Kauppila, J.: Vacancies and carbon impurities in α-iron: electron irradiation. Phys. Rev. B 25, 762–780 (1982)
Kuriplach, J., Melikhova, O., Domain, C., Becquart, C.S., Kulikov, D., Malerba, L., Hou, M., Almazouzi, A., Duque, C.A., Morales, A.L.: Vacancy-solute complexes and their clusters in iron. Appl. Surf. Sci. 252, 3303–3308 (2006)
Hori, K., Koike, K., Oshima, R.: Investigation of lattice defects in the early stage of fatigue in iron by positron annihilation techniques. Appl. Surf. Sci. 242, 304–312 (2005)
Somieski, B., Krause-Rehberg, R.: Application of the positron lifetime spectroscopy as a method of non-destructive testing. Mater. Sci. Forum 175–178, 989–992 (1995)
Dryzek, J.: Scattering and trapping of positrons at vacancies in solids. J. Phys. Condens. Matter 7, L383–L392 (1995)
Dryzek, J., Dryzek, E.: Application of positron annihilation studies of the subsurface zones beneath the surface exposed to the normal loading. Tribol. Lett. 15, 309–317 (2003)
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The author expresses his gratitude to the Ministry of Science and Higher Education (Poland) which supports this work by grant No. N N507 478637.
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Dryzek, J. Positron Studies of Subsurface Zone in Pure Iron Induced by Sliding. Tribol Lett 42, 9–15 (2011). https://doi.org/10.1007/s11249-010-9742-x
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DOI: https://doi.org/10.1007/s11249-010-9742-x


