Skip to main content
Log in

Tribological Properties of Borided AISI 4140 Steel with the Powder Pack-Boriding Method

  • Original Paper
  • Published:
Tribology Letters Aims and scope Submit manuscript

Abstract

The present study evaluates the tribological properties of boride layers on the surface of AISI 4140 steel, formed using the pack-boriding method. Commercial EKabor®2 was used as the boronizing agent and the treatment was carried out at 900, 950, 1000, and 1050 °C for 2, 4, and 6 h, respectively. X-ray diffraction (XRD), scanning electron microscopy (SEM), and microhardness tests were used to characterize the phase composition, microstructure, and local hardness, respectively, of the borided steel samples. Block-on-disc tests were used to investigate tribological properties. Abrasive wear tests were carried out using emery paper at a fixed sliding speed and three different loads. Adhesive wear tests were executed against AISI 52100 steel at a fixed load and distance. The coefficient of friction values (COF) of the samples were determined simultaneously during the tests. The weight loss and COF of the borided samples were compared with untreated samples and the results suggest that both wear resistance and friction properties of the AISI 4140 steel improve with boriding.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Fig. 1
Fig. 2
Fig. 3
Fig. 4
Fig. 5
Fig. 6
Fig. 7
Fig. 8
Fig. 9
Fig. 10
Fig. 11
Fig. 12

Similar content being viewed by others

References

  1. Keddam, M., Chentouf, S.M.: A diffusion model for describing the bilayer growth (FeB/Fe2B) during the iron powder-pack boriding. Appl. Surf. Sci. 252, 393–399 (2005)

    Article  CAS  ADS  Google Scholar 

  2. Sen, U., Sen, S., Yilmaz, F.: An evaluation of some properties of borides deposited on boronized ductile iron. J. Mater. Process. Technol. 148, 1–7 (2004)

    Article  CAS  Google Scholar 

  3. Kulka, M., Pertek, A.: The importance of carbon content beneath iron borides after boriding of chromium and nickel-based low-carbon steel. Appl. Surf. Sci. 214, 161–171 (2003)

    Article  CAS  ADS  Google Scholar 

  4. Cabeo, E.R., Laudien, G., Biemer, S., Rie, K.T., Hoppe, S.: Plasma-assisted boriding of industrial components in a pulsed D.C. glow discharge. Surf. Coat. Technol. 116–119, 229–233 (1999)

    Article  Google Scholar 

  5. Campos, I., Ramírez, G., Figueroa, U., Martínez, J., Morales, O.: Evaluation of boron mobility on the phases FeB, Fe2B and diffusion zone in AISI 1045 and M2 steels. Appl. Surf. Sci. 253, 3469–3475 (2007)

    Article  CAS  ADS  Google Scholar 

  6. Ozdemir, O., Omar, M.A., Usta, M., Zeytin, S., Bindal, C., Ucisik, A.H.: An investigation on boriding kinetics of AISI 316 stainless steel. Vacuum 83, 175–179 (2009)

    Article  Google Scholar 

  7. Lin, Y.C., Chen, M.-S., Zhong, J.: Effects of deformation temperatures on stress/strain distribution and microstructural evolution of deformed 42CrMo steel. Mater. Des. 30, 908–913 (2009)

    CAS  Google Scholar 

  8. Sen, S., Sen, U., Bindal, C.: Tribological properties of oxidised boride coatings grown on AISI 4140 steel. Mater. Lett. 60, 3481–3486 (2006)

    Article  CAS  Google Scholar 

  9. Küper, A., Qiao, X., Stock, H.R., Mayr, P.: A novel approach to gas boronizing. Surf. Coat. Technol. 130, 87–94 (2000)

    Article  Google Scholar 

  10. Sen, S., Sen, U., Bindal, C.: The growth kinetics of borides formed on boronized AISI 4140 steel. Vacuum 77, 195–202 (2005)

    Article  CAS  Google Scholar 

  11. Atık, E., Yunker, U., Merıç, C.: The effects of conventional heat treatment and boronizing on abrasive wear and corrosion of SAE 1010, SAE 1040, D2 and 304 steels. Tribol. Int. 36, 155–161 (2003)

    Article  Google Scholar 

  12. Taktak, S.: Tribological behaviour of borided bearing steels at elevated temperatures. Surf. Coat. Technol. 201, 2230–2239 (2006)

    Article  CAS  Google Scholar 

  13. Ulutan, M.: Investigation of mechanical behaviours of AISI4140 steel after surface hardening and coating processes. Doctoral dissertation (in Turkish), Department of Mechanical Engineering, Eskişehir Osmangazi University (2007)

  14. Selçuk, B., Ipek, R., Karamış, M.B.: A study on friction and wear behaviour of carburized, carbonitrided and borided AISI 1020 and 5115 steels. J. Mater. Process. Technol. 141, 189–196 (2003)

    Article  Google Scholar 

  15. İpek, R., Selçuk, B., Karamiş, M.B., Kuzucu, V., Yücel, A.: An evaluation of the possibilities of using borided GG25 cast iron instead of chilled GG25 cast iron (surface properties). J. Mater. Process. Technol. 105, 73–79 (2000)

    Article  Google Scholar 

  16. Er, U., Par, B.: Wear of plowshare components in SAE 950C steel surface hardened by powder boriding. Wear 261, 251–255 (2006)

    Article  CAS  Google Scholar 

  17. Meric, C., Sahin, S., Backir, B., Koksal, N.S.: Investigation of the boronizing effect on the abrasive wear behavior in cast irons. Mater. Des. 27, 751–757 (2006)

    CAS  Google Scholar 

  18. Campos, I., Farah, M., López, N., Bermúdez, G., Rodríguez, G., VillaVelázquez, C.: Evaluation of the tool life and fracture toughness of cutting tools boronized by the paste boriding process. Appl. Surf. Sci. 254, 2967–2974 (2008)

    Article  CAS  ADS  Google Scholar 

  19. Martini, C., Palombarini, G., Poli, G., Prandstraller, D.: Sliding and abrasive wear behaviour of boride coatings. Wear 256, 608–613 (2004)

    Article  CAS  Google Scholar 

  20. Ozbek, I., Bindal, C.: Mechanical properties of boronized AISI W4 steel. Surf. Coat. Technol. 154, 14–20 (2002)

    Article  CAS  Google Scholar 

  21. Sinha, A.K.: Boriding (boronizing). In: Heat Treating (Section: Surface Hardening of Steel), vol. 4, ASM Handbook, pp. 437–447. ASM International, Materials Park, Ohio (1991)

  22. Petrova, R.S., Suwattananont, N., Samardzic, V.: The effect of boronizing on metallic alloys for automotive applications. J. Mater. Eng. Perform. 17(3), 340–345 (2008)

    Article  CAS  Google Scholar 

  23. Sedlǎcek, M., Podgornik, B., Vižintin, J.: Influence of surface preparation on roughness parameters, friction and wear. Wear 266, 482–487 (2009)

    Article  Google Scholar 

  24. Cho, C.-W., Lee, Y.-Z.: Friction transition diagram considering the effects of oxide layer formed on wear track of AISI 1045 steel disk against TiN coated AISI 52100 steel ball in sliding. Surf. Coat. Technol. 179, 1–9 (2004)

    Article  CAS  Google Scholar 

Download references

Acknowledgment

This study was supported by Eskisehir Osmangazi University Research Council, project number 200315015.

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to Mustafa Ulutan.

Rights and permissions

Reprints and permissions

About this article

Cite this article

Ulutan, M., Yildirim, M.M., Çelik, O.N. et al. Tribological Properties of Borided AISI 4140 Steel with the Powder Pack-Boriding Method. Tribol Lett 38, 231–239 (2010). https://doi.org/10.1007/s11249-010-9597-1

Download citation

  • Received:

  • Accepted:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s11249-010-9597-1

Keywords

Navigation