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Synthesis, crystal structures, and antibacterial studies of silver(I) complexes with reduced Schiff base amino acid ligands

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Abstract

Three Ag(I) complexes of reduced Schiff base amino acid ligands, [Ag2(Hshis)2]·3H2O (1), Ag(Hcgly) (2), and Ag(cala) (3) (H2shis = N-(2-hydroxybenzyl)-l-histidine, H2cgly = N-(2-hydroxy-5-chlorobenzyl)-glycine, Hcala = N-(4-chlorobenzyl)-d,l-alanine), have been synthesized and characterized by X-ray crystallography. Complex 1 shows a dimeric structure, while complex 2 shows one-dimensional zigzag chains, which are extended into a two-dimensional supramolecular sheet by hydrogen bonds. Complex 3 exhibits a 2D sheet structure with dangling arms. The antimicrobial activities of the complexes have been investigated.

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Acknowledgments

This work was supported by the National Natural Science Foundation of China (Grant No. 21201128) and the Science Research Funds of education department of Liaoning Province (L2014596).

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Authors and Affiliations

  1. Department of Chemical Engineering, YingKou Institute of Technology, Yingkou, 115014, People’s Republic of China

    Hai-Yan Liu, Peng Du & Hong Chen

  2. Department of Chemistry and Pharmaceutical Engineering, Suihua University, Suihua, 152061, People’s Republic of China

    Hai-Yan Liu & Jun Tian

  3. Animal Science and Technology College, Jilin Agricultural University, Changchun, 130118, People’s Republic of China

    Qing-Hua Guan

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  1. Hai-Yan Liu
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  2. Qing-Hua Guan
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  3. Jun Tian
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  4. Peng Du
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Correspondence to Hai-Yan Liu.

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Liu, HY., Guan, QH., Tian, J. et al. Synthesis, crystal structures, and antibacterial studies of silver(I) complexes with reduced Schiff base amino acid ligands. Transit Met Chem 41, 615–622 (2016). https://doi.org/10.1007/s11243-016-0060-5

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  • DOI: https://doi.org/10.1007/s11243-016-0060-5

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