The paper proposes a new approach to gradient porous composites based on the Ti3Al(Si)C2 MAX phase. This approach is based on the production of preceramic paper with the different content of the powder filler based on MAX phases and their spark plasma sintering. The analysis of the microstructure and phase composition is conducted for these composites. It is shown that the obtained composites have a clear interface between layers with different porosity. It is found that the content of organic components in preceramic paper affects the phase composition of the fabricated composites. The MAX phase content in dense and porous layers is 86 and 56 vol.%, respectively. Microhardness measurements performed in the composite cross-section show the hardness of 600 to 800 HV, depending on the layer porosity and phase composition.
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Translated from Izvestiya Vysshikh Uchebnykh Zavedenii, Fizika, No. 12, pp. 132–138, December 2022
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Krotkevich, D.G., Kashkarov, E.B., Mingazova, Y.R. et al. Fabrication of Max Phase-Based Gradient Porous Materials from Preceramic Paper. Russ Phys J 65, 2186–2192 (2023). https://doi.org/10.1007/s11182-023-02888-2
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DOI: https://doi.org/10.1007/s11182-023-02888-2