The paper presents a plasma-assisted generation of nanodisperse powder obtained from diatomite, a natural high-silica material. The structure and properties of the obtained material are investigated using the transmission electron microscopy, energy dispersive X-Ray spectroscopy, infrared and X-ray photoelectron spectroscopies, and Brunauer–Emmett–Teller method. It is clearly shown that the obtained SiO2 nanoparticles are spherical, polydisperse and represented in the form of agglomerates. The specific surface of this nanopowder is 32 m2/g. Thermodynamic modeling of the plasma-assisted process is used to obtain the equilibrium compositions of condensed and gaseous reaction products. The plasma process is performed within the 300–5000 K temperature range.
Similar content being viewed by others
References
P. V. Grishin, V. E. Katnov, S. N. Stepin, in: Proc. 12th Int. Sci. Conf. “Modern Development Systems, Information Technologies and Innovations” [in Russian], ed. A. A. Gorokhov, Kursk (2015), 1, pp. 351–354.
A. I. Sviridenok, A. V. Krautsevich, and V. I. Lysenko, et al., J. Frict. W., 35 (3), 225-235 (2014).
L. Zhai, F. C. Cebeci, R. E. Cohen, et al. Nano Lett., 4, 1349–1353 (2004).
K. L. Lin, W. C. Chang, D. F. Lin, et al. J. Env. Manag., 88, 708–714 (2008).
B. G. Quercia and H. J. H. Brouwers, Proc. 8th fib Int. PhD Symp. Civil Engineering, Lyngby (2010), pp. 431–436.
N. A. Shabanova and P. D. Sarkisov, Bases of Sol Gel Technology of Nanodisperse Silica [in Russian]. Akademkniga, Moscow (2004).
I. A. Rahman, P. Vejayakumaran, C. S. Sipaut, et al., Coll. Surf. A., 294 (1–3), 102–110 (2007).
S. P. Bardakhanov, V. A. Volodin, and M. D. Efremov, Jpn. J. Appl. Phys., 47 (9), 7019–7022 (2008).
R. V. Sazonov, G. E. Kholodnaya, D. V. Ponomarev, et al., Izv. Vyssh. Uchebn. Zaved., Fiz. [in Russian], 55, No. 6/2, 72–76 (2012).
A. J. Gröhn, S. E. Pratsinis, A. Sanchez-Ferrer, et al., The High-Temp. Part. Res. T., Ind. & Eng. Chem. Res., V. 53, 10734−10742 (2014).
A. B. Vorozhtsov, A. S. Zhukov, T. D. Malinovskaya, et al., Synthesis of Disperse Metal-Oxide Materials, in Book 2: Plasma-Chemical Production Method for Titanium and Zirconium Oxides [in Russian], Izd-vo NTL, Tomsk (2014).
A. V. Ushakov, V. N. Veselovskii, and V. E. Red’kin, in: Proc. All-Russian Conf. “Achievements of Science and Technology to Siberian Regions Development” [in Russian], KGTU, Krasnoyarsk (2003), pp. 75–79.
A. A. Lepeshev, A. V. Ushakov, and I. V. Karpov, Plasma-Chemical Synthesis of Nanopowders and Polymer Nanocomposites [in Russian], SibFU, Krasnoyarsk (2012).
J. T. Nell, J. L. Havenga, J. Swanepoel, et al., J. S. Afr. Inst. Min. Met., 10, 231– 234 (2010).
P. V. Kosmachev, V. A. Vlasov, and N. K. Skripnikova, AIP Conf. Proc., 800, 020016 (2017).
S. Brunauer, P. H. Emmett, and E. J. Teller, Am. Chem. Soc., 60, 309–319 (1938).
E. I. Karpenko, V. E. Messerle, B. G. Trusov, et al., Gorenie i plazmokhim. [in Russian], 1, No. 4, 291–310 (2003).
Author information
Authors and Affiliations
Corresponding author
Additional information
Translated from Izvestiya Vysshikh Uchebnykh Zavedenii, Fizika, No. 2, pp. 46–50, February, 2017.
Rights and permissions
About this article
Cite this article
Kosmachev, P.V., Vlasov, V.A. & Skripnikova, N.K. Structure and Properties of Sio2 Nanopowder Obtained From High-Silica Raw Materials by Plasma Method. Russ Phys J 60, 249–253 (2017). https://doi.org/10.1007/s11182-017-1068-9
Received:
Published:
Issue Date:
DOI: https://doi.org/10.1007/s11182-017-1068-9