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Tetrazoles: XLVIII. 3H-Naphtho[2,1-e]-and 3H-Naphtho[1,2-e][1,2,4]triazepines from 5-Aryltetrazoles. Physical and Chemical Properties

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Abstract

Thermolysis of N-imidoyltetrazoles generated under conditions of phase-transfer catalysis from 5-aryltetrazoles and N-(2-naphthyl)benzimidoyl chloride yields 3H-naphtho[2,1-e][1,2,4]triazepines, and acid hydrolysis of the latter leads to formation of 3-arylbenz[e]indazoles. Acid hydrolysis of 3H-naphtho[1,2-e]-[1,2,4]triazepine gives the corresponding amino ketone.

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Authors and Affiliations

  1. St. Petersburg State Institute of Technology, Moskovskii pr. 26, St. Petersburg, 190013, Russia

    V. V. Nikulin, T. V. Artamonova & G. I. Koldobskii

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  1. V. V. Nikulin
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  2. T. V. Artamonova
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  3. G. I. Koldobskii
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Dedicated to Full Member of the Russian Academy of Sciences V.I. Minkin on his 70th Anniversary

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Translated from Zhurnal Organicheskoi Khimii, Vol. 41, No. 3, 2005, pp. 451–456.

Original Russian Text Copyright © 2005 by Nikulin, Artamonova, Koldobskii.

For communication XLVII, see [1].

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Nikulin, V.V., Artamonova, T.V. & Koldobskii, G.I. Tetrazoles: XLVIII. 3H-Naphtho[2,1-e]-and 3H-Naphtho[1,2-e][1,2,4]triazepines from 5-Aryltetrazoles. Physical and Chemical Properties. Russ J Org Chem 41, 444–449 (2005). https://doi.org/10.1007/s11178-005-0185-z

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  • DOI: https://doi.org/10.1007/s11178-005-0185-z

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