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New ways of synthesis of 1,2-dithiole-3-thione

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Abstract

Two new synthetic approaches to 1,2-dithiole-3-thione are proposed. The title compound is formed by thermolysis of dipropyl polysulfides (n-Pr)2Sx (x = 3–4) and thermal decomposition of polysulfide dendrimers under reduced pressure. The latter reaction may be recommended for utilization of organochlorine waste products in the manufacture of epichlorohydrin, which are used for the synthesis of dendrimers.

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Authors and Affiliations

  1. Favorskii Irkutsk Institute of Chemistry, Siberian Division, Russian Academy of Sciences, Irkutsk, Russia

    N. A. Korchevin, N. V. Russavskaya, G. A. Yakimova & E. N. Deryagina

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  1. N. A. Korchevin
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  2. N. V. Russavskaya
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  3. G. A. Yakimova
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  4. E. N. Deryagina
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Additional information

Translated from Zhurnal Obshchei Khimii, Vol. 74, No. 11, 2004, pp. 1884–1886.

Original Russian Text Copyright © 2004 by Korchevin, Russavskaya, Yakimova, Deryagina.

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Korchevin, N.A., Russavskaya, N.V., Yakimova, G.A. et al. New ways of synthesis of 1,2-dithiole-3-thione. Russ J Gen Chem 74, 1754–1756 (2004). https://doi.org/10.1007/s11176-005-0095-3

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  • DOI: https://doi.org/10.1007/s11176-005-0095-3

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