Abstract
The single crystals of [UO2SO4{(CH3)HNCONH(CH3)}2] (I) were synthesized and studied by X-ray diffraction. The crystals are monoclinic, a = 6.847(1) Å, b = 14.259(3) Å, c = 14.297(3) Å, β = 93.451(4)°, space group P21/n, Z = 4. The main structural units of crystals I are ribbons whose composition coincides with the composition of the compound. The crystal chemical formula of the complex is AT3M 12 (A = UO 2+2 ).
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REFERENCES
Demchenko, E.A., Mit'kovskaya, E.V., Mikhailov, Yu.N., et al., Zh. Neorg. Khim., 2002, vol. 47, no.11, p. 1826 [Russ. J. Inorg. Chem. (Engl. Transl.), vol. 47, no. 11, p. 1677].
Mit'kovskaya, E.V., Mikhailov, Yu.N., Gorbunova, Yu.E., et al., Zh. Neorg. Khim., 2004, vol. 49, no.12, p. 2074 [Russ. J. Inorg. Chem. (Engl. Transl.), vol. 49, no. 12, p. 1923].
Mit'kovskaya, E.V., Demchenko, E.A., Mikhailov, Yu.N., et al., Zh. Neorg. Khim., 2002, vol. 47, no.9, p. 1432 [Russ. J. Inorg. Chem. (Engl. Transl.), vol. 47, no. 9, p. 1306].
Porai-Koshits, M.A. and Serezhkin, V.N., Zh. Neorg. Khim., 1994, vol. 39, no.7, p. 1109.
Serezhkin, V.N., Blatov, V.A., and Shevchenko, A.P., Koord. Khim., 1995, vol. 21, no.3, p. 163.
Serezhkin, V.N., Shishkina, O.V., Serezhkina, L.B., et al., Zh. Neorg. Khim., 1999, vol. 44, no.4, p. 616 [Russ. J. Inorg. Chem. (Engl. Transl.), vol. 44, no. 4, p. 562].
Shchelokov, R.N., Khimiya platinovykh i tyazhelykh metallov (The Chemistry of Platinum and Heavy Metals), Moscow: Nauka, 1975.
Perez-Folch, J., Subirana, J.A., and Aymami, J., J. Chem. Crystallogr., 1997, vol. 27, no.6, p. 367.
Fairlie, D.P., Tai Chin Woon, Wickramasinghe, W.A., and Willis, A.C., Inorg. Chem., 1994, vol. 33, no.26, p. 6425.
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Translated from Koordinatsionnaya Khimiya, Vol. 31, No. 12, 2005, pp. 936–940.
Original Russian Text Copyright © 2005 by Serezhkina, Mit'kovskaya, Medrish, Grechishnikova, Dolgushin, Antipin, Serezhkin.
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Serezhkina, L.B., Mit'kovskaya, E.V., Medrish, I.V. et al. Crystal Structure of [UO2SO4{(CH3)HNCONH(CH3)}2]. Russ J Coord Chem 31, 889–893 (2005). https://doi.org/10.1007/s11173-005-0187-y
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DOI: https://doi.org/10.1007/s11173-005-0187-y