Abstract
Polyetheretherketones with various molecular weights were obtained by high-temperature polycondensation using the nucleophilic substitution reaction by varying the temperature-time mode of synthesis. The thermal, physico-mechanical properties, bulk density, shape and size of particles were studied. The polyetheretherketone synthesis conditions, which make it possible to obtain a polymer powder with a set of properties necessary for high-quality 3D printing using selective laser sintering technology, were determined.
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Svetlana Yurievna Khashirova, born in 1974, Head of the Department of Organic Chemistry and Macromolecular Compounds, Director of the Center for Advanced Materials and Additive Technologies, Federal State Budgetary Educational Institution of Higher Education Kabardino-Balkarian State University named after H. M. Berbekov (Nalchik), Doctor of Chemical Sciences, Professor, Honored Scientist of the KBR, recipient of the State Prize of the Kabardino-Balkarian Republic in the Field of Science and Technology, National Prize of the Russian Professorial Assembly «Vice-Rector of the Year for Research». S. Yu. Khashirova is a leading specialist in the field of chemistry of macromolecular compounds, the author of 516 scientific works, including 2 monographs and 101 patents for inventions. The main scientific results of S. Yu. Khashirova are: the development of a new scientific direction in the physical chemistry of guanidine-containing polymers and methods for the directed synthesis of new biocidal polyelectrolytes and nanocomposite materials with valuable practical properties; the solution of the problem of toxicity of synthetic guanidine-containing compounds for use in living systems; breakthroughs in the field of new advanced high performance polymers and technologies for their 3D printing, which are of fundamental importance for the development of polymer additive technologies in our country and import substitution. S. Yu. Khashirova is a leading professor, has formed a research team, including more than 30 young scientists, has supervised 15 PhDs. She is a Chairman of the Dissertation Council 24.2.308.03 at KBSU; editor-in-chief of the journal “News of the Kabardino-Balkarian State University”, a member of the editorial board of international journals “Materials Science Forum”, “Key Engineering Materials”, an expert of scientific funds, is included in the Federal Register of Experts of the Scientific and Technical Sphere, a member of the Scientific Council of the Russian Academy of Sciences on Materials and Nanomaterials. S. Yu. Khashirova was nominated as a candidate for Corresponding Member of the Russian Academy of Sciences for the Chemistry and Materials Sciences Branch of the Russian Academy of Sciences in the specialty “Chemical Sciences” by the Academic Council of KBSU.
Published in Russian in Izvestiya Akademii Nauk. Seriya Khimicheskaya, Vol. 72, No. 2, pp. 546–552, February, 2023.
No human or animal subjects were used in this research.
The authors declare no competing interests.
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Khashirova, S.Y., Zhansitov, A.A., Shakhmurzova, K.T. et al. Synthesis and properties of polyetheretherketone for applications in additive technologies. Russ Chem Bull 72, 546–552 (2023). https://doi.org/10.1007/s11172-023-3818-9
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DOI: https://doi.org/10.1007/s11172-023-3818-9