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Fabrication and physicochemical characterization of graphene oxide derived from thermally expanded graphite

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Abstract

Graphene oxide was obtained from expanded graphite according to the modified Hummers method. The reaction time was significantly reduced (from 24 to 8 h) by applying the expanded graphite in the oxidation process. The interlayer distance in obtained samples was equal to 0.70–0.74 nm. Structural features of the material were studied by the powder X-ray diffraction, thermogravimetric analysis, scanning electron microscopy, transmission electron microscopy, XPS spectroscopy, and NMR spectroscopy.

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Authors and Affiliations

  1. Federal Research Center for Coal and Coal Chemistry, Siberian Branch of the Russian Academy of Sciences, 18 Sovetskiy prosp., 650000, Kemerovo, Russian Federation

    L. V. Ilkevich, S. A. Sozinov, L. M. Hitsova, A. N. Popova, Ch. N. Barnakov & A. P. Kozlov

  2. Kemerovo State University, 6 ul. Krasnaya, 650043, Kemerovo, Russian Federation

    T. B. Tkachenko

  3. Department of Chemistry, M. V. Lomonosov Moscow State University, Build. 9, 1 Leninskie Gory, 119991, Moscow, Russian Federation

    A. V. Samarov & A. A. Burtsev

Authors
  1. L. V. Ilkevich
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  2. T. B. Tkachenko
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  3. A. V. Samarov
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  4. A. A. Burtsev
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  5. S. A. Sozinov
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  6. L. M. Hitsova
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  7. A. N. Popova
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  8. Ch. N. Barnakov
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  9. A. P. Kozlov
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Correspondence to L. V. Ilkevich.

Additional information

Published in Russian in Izvestiya Akademii Nauk. Seriya Khimicheskaya, No. 6, pp. 0986–0990, June, 2018.

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Ilkevich, L.V., Tkachenko, T.B., Samarov, A.V. et al. Fabrication and physicochemical characterization of graphene oxide derived from thermally expanded graphite. Russ Chem Bull 67, 986–990 (2018). https://doi.org/10.1007/s11172-018-2168-6

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  • DOI: https://doi.org/10.1007/s11172-018-2168-6

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