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Study of electrochemical behavior of the Fe3O4 nanoparticles in aprotic media

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Abstract

Peculiarities of electrochemical behavior of the Fe3O4 magnetic nanoparticles immobilized on the surface of a platinum electrode in aprotic organic media were investigated. Possible scheme of electrochemical behavior of nanoparticles depending on pre-electrolysis potential (–1.3,–2.5 V) was suggested. The effect of pre-electrolysis time, potential scan rate and nature of supporting electrolyte on the processes investigated was determined. A linear dependence of electrochemical oxidation signal versus the concentration of nanoparticles in modifying suspension in the concentration range of 0.05—0.5 g L–1 was observed. The results of the performed research allow using magnetite nanoparticles as a direct signal-generating label in electrochemical immunoassay.

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Authors and Affiliations

  1. Ural Federal University named after the first President of Russia B. N. Yeltsin, 19 ul. Mira, 620000, Ekaterinburg, Russian Federation

    A. N. Kozitsina, T. S. Svalova, T. A. Glazyrina, A. V. Ivanova & A. I. Matern

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  1. A. N. Kozitsina
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  2. T. S. Svalova
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  3. T. A. Glazyrina
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  4. A. V. Ivanova
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  5. A. I. Matern
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Correspondence to A. N. Kozitsina.

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Published in Russian in Izvestiya Akademii Nauk. Seriya Khimicheskaya, No. 3, pp. 0697—0703, March, 2016.

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Kozitsina, A.N., Svalova, T.S., Glazyrina, T.A. et al. Study of electrochemical behavior of the Fe3O4 nanoparticles in aprotic media. Russ Chem Bull 65, 697–703 (2016). https://doi.org/10.1007/s11172-016-1359-2

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  • DOI: https://doi.org/10.1007/s11172-016-1359-2

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