Skip to main content
Log in

Synthesis of graphene-like materials by graphite oxide reduction

  • Full Articles
  • Published:
Russian Chemical Bulletin Aims and scope

Abstract

Graphene-like materials were produced by the reduction of graphite oxide with a series of chemical reagents and high-temperature treatment. Hydrazine hydrate, hydroxylamine hydro-chloride, sodium borohydride, and sodium sulfite were used as reducing agents. The obtained materials were studied by elemental and thermal gravimetric analyses, scanning electron microscopy, X-ray diffraction, and IR and Raman spectroscopy. Depending on the used reducing agents, the graphene-like materials contained different amounts of residual oxygen.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Similar content being viewed by others

References

  1. K. S. Novoselov, A. K. Geim, S. V. Morozov, D. Jiang, Y. Zhang, S. V. Dubonos, I. V. Grigorieva, A. A. Firso, Science, 2004, 306, 666.

    Article  CAS  Google Scholar 

  2. M. Orlita, C. Faugeras, P. Plochocka, P. Neugebauer, G. Martinez, D. K. Maude, A.-L. Barra, M. Sprinkle, C. Berger, W. A. de Heer, M. Potemski, Phys. Rev. Lett., 2008, 101, 267601.

    Article  CAS  Google Scholar 

  3. A. A. Balandin, S. Ghosh, W. Bao, I. Calizo, D. Teweldebrhan, F. Miao, Ch. N. Lau, Nano Lett., 2008, 8, 902.

    Article  CAS  Google Scholar 

  4. C. G. Lee, X. D. Wei, J. W. Kysar, J. Hone, Science, 2008, 321, 385.

    Article  CAS  Google Scholar 

  5. M. J. McAllister, J.-L. Li, D. H. Adamson, H. C. Schniepp, A. A. Abdala, J. Liu, M. Herrera-Alonso, D. L. Milius, R. Car, R. K. Prud’homme, I. A. Aksay, Chem. Materials, 2007, 19, 4396.

    Article  CAS  Google Scholar 

  6. Y. Zhu, S. Murali, M. D. Stoller, A. Velamakanni, R. D. Piner, R. S. Ruoff, Carbon, 2010, 48, 2118.

    Article  CAS  Google Scholar 

  7. V. A. Smirnov, A. A. Arbuzov, Yu. M. Shul’ga, S. A. Baskakov, V. M. Martynenko, V. E. Muradyan, E. I. Kresova, High Energy Chem. (Engl. Transl.), 2011, 45, 57 [Khim. Vys. Energ., 2011, 45, 60].

    Article  CAS  Google Scholar 

  8. S. Stankovich, D. A. Dikin, R. D. Piner, K. A. Kohlhaas, A. Kleinhammes, Y. Jia, Y. Wu, S. T. Nguyen, R. S. Ruoff, Carbon, 2007, 45, 1558.

    Article  CAS  Google Scholar 

  9. Y. Si, E. T. Samulski, Nano Lett., 2008, 8, 1679.

    Article  CAS  Google Scholar 

  10. S. Stankovich, D. A. Dikin, G. H. B. Dommett, K. M. Kohlhaas, E. J. Zimney, E. A. Stach, R. D. Piner, S. T. Nguyen, R. S. Ruoff, Nature, 2006, 442, 282.

    Article  CAS  Google Scholar 

  11. M. J. Fernandez-Merino, L. Guardia, J. I. Paredes, S. Villar-Rodil, P. Solis-Fernandez, A. Martinez-Alonso, J. M. D. Tasco’n, J. Phys. Chem., C, 2010, 114, 6426.

    Article  CAS  Google Scholar 

  12. S. Pei, J. Zhao, J. Du, W. Ren, H.-M. Cheng, Carbon, 2010, 48, 4466.

    Article  CAS  Google Scholar 

  13. V. E. Muradyan, V. S. Romanova, A. P. Moravskii, Z. N. Parnes, Yu. N. Novikov, Russ. Chem. Bull. (Int. Ed.), 2000, 49, 1017 [Izv. Akad. Nauk, Ser. Khim., 2000, 1023].

    Article  CAS  Google Scholar 

Download references

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to A. A. Arbuzov.

Additional information

Published in Russian in Izvestiya Akademii Nauk. Seriya Khimicheskaya, No. 9, pp. 1962–1966, September, 2013.

Rights and permissions

Reprints and permissions

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Arbuzov, A.A., Muradyan, V.E. & Tarasov, B.P. Synthesis of graphene-like materials by graphite oxide reduction. Russ Chem Bull 62, 1962–1966 (2013). https://doi.org/10.1007/s11172-013-0284-x

Download citation

  • Received:

  • Revised:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s11172-013-0284-x

Key words

Navigation