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Biogenic CuO NPs for synthesis of coumarin derivatives in hydrotropic aqueous medium

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Abstract

In this work, we explored the catalytic activity of CuO NPs prepared by gum of the Acacia Senegal plant for the multicomponent synthesis of Coumarin derivatives in an aqueous medium. The morphology of Bi–CuO NPs was characterized by FTIR, XRD, SEM, EDX, and TGA–DTA tools. It has been shown that Bi–CuO NPs not only act as an efficient and green catalyst for the synthesis of Coumarin derivatives in an aqueous medium but also recover easily and is recycled many times without significant loss in their catalytic activity. High efficiency, short reaction time, high TOF, green solvent, and chromatography-free separation of the product are the key features of this work.

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Acknowledgements

The authors are thankful to Yashawantrao Chavan Institute of Science, Satara (Autonomous) for providing laboratory and characterization facilities in Common Facility Center (CFC), which is sponsored by different grants of (RUSA-component-8, DST-FIST, UGC-CPE, and DBT-STAR) Government of India. One of the authors S. R. Attar gratefully acknowledges the Government of Maharashtra, India for the Mahatma Jyotiba Phule Research Fellowship (MJPRF 2021) from Mahatma Jyotiba Phule Research and Training Institute (MAHAJYOTI).

Funding

Mahatma Jyotiba Phule Research Fellowship (MJPRF 2021), Government of Maharashtra, India.

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Authors and Affiliations

  1. Yashawantrao Chavan Institute of Science, Lead College of K. B. P. University, Satara, Maharashtra, 415001, India

    S. R. Attar, A. C. Sapkal, V. B. Ghanwat & S. B. Kamble

  2. Department of Agrochemical and Pest Management, Shivaji University, Kolhapur, Maharashtra, 416004, India

    C. S. Bagade

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  1. S. R. Attar
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  2. A. C. Sapkal
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  3. C. S. Bagade
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  4. V. B. Ghanwat
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  5. S. B. Kamble
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Contributions

S. R. Attar conceptualized and wrote the manuscript text. A. C. Sapkal and C. S. Bagade helped to interpret the data. V. B. Ghanwat helped to prepare figures as well as an analysis. Design, supervision, and implementation were performed by S. B. Kamble.

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Correspondence to S. B. Kamble.

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Attar, S.R., Sapkal, A.C., Bagade, C.S. et al. Biogenic CuO NPs for synthesis of coumarin derivatives in hydrotropic aqueous medium. Res Chem Intermed 49, 2989–3004 (2023). https://doi.org/10.1007/s11164-023-05034-2

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  • DOI: https://doi.org/10.1007/s11164-023-05034-2

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