Advertisement

Research on Chemical Intermediates

, Volume 44, Issue 5, pp 3365–3374 | Cite as

Magnetic ordered mesoporous carbon composites incorporating Ag nanoparticles as SERS substrate for enrichment and detection of trace mercaptan compounds

  • Lei Zhang
  • Wen-Bin Miu
  • Jianlei Yao
  • Lin Sun
  • Bohao Yu
Article

Abstract

Fe3O4 magnetic nanoparticles and Ag nanoparticles reduced by reductant were incorporated on ordered mesoporous carbon to form magnetic ordered mesoporous carbon composites incorporating Ag nanoparticles (magnetic OMC–Ag). The prepared magnetic OMC–Ag as a surface-enhanced Raman scattering (SERS) substrate not only exhibited a clearly enhanced effect but also showed enrichment ability for the detection of 4-nitrothiphenol. Ag nanoparticles-incorporated magnetic carbon composites as SERS substrate displayed Raman enhancement phenomenon for the detection of 4-nitrothiphenol and showed high stability.

Keywords

SERS Magnetic OMC Ag nanoparticles Enrichment Carbon 4-Nitrothiphenol 

Notes

Acknowledgements

This work was financially supported by the General Administration of Quality Supervision, Inspection and Quarantine of the People’s Republic of China (2016IK227), the Project of Inspection and Quarantine of Shanghai (HK015-2016), and the National Natural Science Foundation of China (21707034).

References

  1. 1.
    M. Fleischmann, P.J. Hendra, A.J. McQuillan, Chem. Phys. Lett. 26, 63 (1974)CrossRefGoogle Scholar
  2. 2.
    S.E. Deprimo, J. Cao, M.N. Hersh, J.R. Stringer, J. Phys. Chem. C 115, 17829 (2011)CrossRefGoogle Scholar
  3. 3.
    Q. An, P. Zhang, J.M. Li, W.F. Ma, J. Guo, C.C. Wang, Nanoscale 4, 5210 (2012)CrossRefGoogle Scholar
  4. 4.
    B.C. Qiu, M.Y. Xing, Q.Y. Yi, J.L. Zhang, Angew. Chem. Int. Ed. 54, 10643 (2015)CrossRefGoogle Scholar
  5. 5.
    Y. Zeng, J.Q. Ren, A.G. Shen, J.M. Hu, A.C.S. Appl, Mater. Interfaces 8, 27772 (2016)CrossRefGoogle Scholar
  6. 6.
    Y. Kang, T. Wu, B.X. Liu, X. Wang, Y.P. Du, Microchim. Acta 181, 1333 (2014)CrossRefGoogle Scholar
  7. 7.
    Y.X. Yuan, L. Ling, X.Y. Wang, M. Wang, R.A. Gu, J.L. Yao, J. Raman Spectrosc. 38, 1280 (2007)CrossRefGoogle Scholar
  8. 8.
    E. Hao, G.C. Schatz, J. Chem. Phys. 120, 357 (2004)CrossRefGoogle Scholar
  9. 9.
    A.M. Michaels, A.M. Nirmal, L.E. Brus, J. Am. Chem. Soc. 121, 9932 (1999)CrossRefGoogle Scholar
  10. 10.
    S. Lee, H. Chon, J. Lee, J. Ko, B.H. Chung, D.W. Lim, J. Choo, Biosens. Bioelectron. 51, 238 (2014)CrossRefGoogle Scholar
  11. 11.
    W. Fan, Y.H. Lee, S. Pedireddy, Q. Zhang, T.X. Liu, X.Y. Ling, Nanoscale 6, 4843 (2014)CrossRefGoogle Scholar
  12. 12.
    Q.L. Li, B.W. Li, Y.Q. Wang, RSC Adv. 3, 13015 (2013)CrossRefGoogle Scholar
  13. 13.
    S. Tokonami, K. Nishida, Y. Nishimura, S. Hidaka, Y. Yamamoto, T. Lida, Res. Chem. Intermed. 40, 2337 (2014)CrossRefGoogle Scholar
  14. 14.
    L. Zhang, Z.C. Xiong, Y.J. Chen, L. Peng, H.B. Yu, R.S. Zhang, L.Y. Zhang, W.B. Zhang, RSC Adv. 6, 30014 (2016)CrossRefGoogle Scholar
  15. 15.
    L. Zhang, Y.Y. Gan, H.F. Sun, B.H. Yu, X.F. Jin, L.Y. Zhang, W.B. Zhang, Microchim. Acta 184, 547 (2017)CrossRefGoogle Scholar
  16. 16.
    Z.K. Sun, B. Sun, M.H. Qiao, J. Wei, Q. Yue, C. Wang, D.Y. Zhao, J. Am. Chem. Soc. 134, 17653 (2012)CrossRefGoogle Scholar
  17. 17.
    N. Li, J.X. Xu, L.J. Xu, J.J. Du, X.Y. Wang, J. Nanosci. Nanotechnol. 15, 4961 (2015)CrossRefGoogle Scholar
  18. 18.
    P.B. Liu, Y. Huang, L. Wang, Mater. Lett. 97, 173 (2013)CrossRefGoogle Scholar
  19. 19.
    S. Mondal, U. Rana, S. Malik, A.C.S. Appl, Mater. Interfaces 7, 10457 (2015)CrossRefGoogle Scholar
  20. 20.
    M.H. Cao, L. Zhou, X.Q. Xu, S. Cheng, J.L. Yao, L.J. Fan, J. Mater. Chem. A 1, 8942 (2013)CrossRefGoogle Scholar

Copyright information

© Springer Science+Business Media B.V., part of Springer Nature 2018

Authors and Affiliations

  • Lei Zhang
    • 1
  • Wen-Bin Miu
    • 2
  • Jianlei Yao
    • 1
  • Lin Sun
    • 1
  • Bohao Yu
    • 1
  1. 1.School of Chemistry and Molecular EngineeringEast China University of Science and TechnologyShanghaiChina
  2. 2.Technical Center for Industrial Products and Raw Materials Inspection and TestingShanghai Entry-Exit Inspection and Inspection and Quarantine BureauShanghaiChina

Personalised recommendations