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Nickel nanoparticles generated by pulsed laser ablation in liquid CO2

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Abstract

Nickel nanoparticles with various structures were synthesized by a pulsed laser ablation process in liquid CO2 at 17 °C and 5.2 MPa. A nickel plate immersed in liquid CO2 was used as a target. This was irradiated by a laser beam with a fundamental wavelength of 1064 nm at 2.46 mJ for 15 min. The generated particles were deposited on a silicon wafer after natural evaporation of the liquid CO2, and analyzed by field emission scanning electron microscopy, scanning electron microscopy with energy-dispersive X-ray spectroscopy, and transmission electron microscopy. Nickel and carbon particles with sphere-like structures or apple-shaped structures were observed. Furthermore, characteristic nickel/carbon particles with core/shell structures were also produced. The generated particles ranged in size between 5 and 350 nm in diameter, with dominant sizes under 50 nm.

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Acknowledgments

This work was supported by a Grant-in-Aid for Scientific Research (No. 21246119 and No. 21110009) from the Ministry of Education, Culture, Sports, Science and Technology, Japan.

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Authors and Affiliations

  1. Department of Chemical Engineering, Nagoya University, Nagoya, 464-8603, Japan

    Mardiansyah Mardis,  Wahyudiono, Hideki Kanda & Motonobu Goto

  2. Technical Center, Nagoya University, Nagoya, 464-8603, Japan

    Noriharu Takada

  3. Department of Chemical Engineering, Sepuluh Nopember Institute of Technology, Surabaya, 60111, Indonesia

    Siti Machmudah

  4. Division of Quantum Science and Engineering, Hokkaido University, Sapporo, 060-8628, Japan

    Koichi Sasaki

Authors
  1. Mardiansyah Mardis
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  2. Noriharu Takada
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  3. Siti Machmudah
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  4. Wahyudiono
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  5. Koichi Sasaki
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  6. Hideki Kanda
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  7. Motonobu Goto
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Correspondence to Motonobu Goto.

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Mardis, M., Takada, N., Machmudah, S. et al. Nickel nanoparticles generated by pulsed laser ablation in liquid CO2 . Res Chem Intermed 42, 4581–4590 (2016). https://doi.org/10.1007/s11164-015-2299-4

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  • DOI: https://doi.org/10.1007/s11164-015-2299-4

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