In this research, AZ91 magnesium matrix composites reinforced with three weight fractions (10, 20, and 30 wt.%) of TiB2 particulates were fabricated by powder metallurgy using hot pressing technique. The microstructure, density, hardness, wear, and mechanical properties of the specimens were investigated. Microstructure studies showed that fairly uniform distribution of reinforcements was achieved, but partial agglomeration could be clearly seen at 30 wt.% TiB2. X-ray studies exhibited that phases of Mg, Mg17Al12, and TiB2 were found. As compared to AZ91, the hardness and wear resistance considerably increased with increasing reinforcement content. The presence of TiB2 particles improved 0.2% compressive yield strength and ultimate compressive strength (UCS); however, UCS decreased above 20 wt.% TiB2. Wear mechanisms are oxidative and abrasive.
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M. Gupta and N.M.L. Sharon, Magnesium, Magnesium Alloys, and Magnesium Composites, Wiley, New Jersey (2011), p. 5.
K.K. Deng, K. Wu, Y.W. Wu, et al., “Effect of submicron size SiC particulates on microstructure and mechanical properties of AZ91 magnesium matrix composites,” J. Alloys Compd., 504, 542–547 (2010).
M.Y. Zheng, K. Wua, S. Kamado, and Y. Kojima, “Aging behavior of squeeze cast SiCW/AZ91 magnesium matrix composite,” Mater. Sci. Eng. A, 348, 67–75 (2003).
A. Reyes, E. Bedolla, R. Perez, and A. Contreras, “Effect of heat treatment on the mechanical and microstructural characterization of Mg–AZ91E/TiC composites,” Compos. Interfaces, 24, No. 6, 593–609 (2017).
M.Y. Zheng, K. Wu, M. Liang, et al., “The effect of thermal exposure on the interface and mechanical properties of Al18B4O33w/AZ91 magnesium matrix composite,” Mater. Sci. Eng. A, 372, 66–74 (2004).
K.K. Deng, X.J. Wang, Y.W. Wu, et al., “Effect of particle size on microstructure and mechanical properties of SiCp/AZ91 magnesium matrix composite,” Mater. Sci. Eng. A., 543, 158–163 (2012).
W. Yu, X. Wang, H. Zhao, et al., “Microstructure, mechanical properties and fracture mechanism of Ti2AlC reinforced AZ91D composites fabricated by stir casting,” J. Alloys Compd., 702, 199–208 (2017).
A. Kandil, “Microstructure and mechanical properties of SiCp/AZ91 magnesium matrix composites processed by stir casting,” J. Eng. Sci., Assiut Univ., 40, No. 1, 255–270 (2012).
S.S. Zhou, K.K. Deng, J.C. Li, et al., “Hot deformation behavior and workability characteristics of bimodal size SiCp/AZ91 magnesium matrix composite with processing map,” Mater. Des., 64, 177–184 (2014).
X.J. Wang, X.S. Hu, W.Q. Liu, et al., “Ageing behavior of as-cast SiCp/AZ91 Mg matrix composites,” Mater. Sci. Eng. A., 682, 491–500 (2017).
D.M. Lee, B.K. Suh, B.G. Kim, et al., “Fabrication, microstructures and tensile properties of magnesium alloy AZ91/SiCp composites produced by powder metallurgy,” Mater. Sci. Technol., 13, No. 7, 590–595 (1997).
S.P. Rawal, “Metal-matrix composites for space applications,” JOM, 53, 14–17 (2001).
Q.C. Jiang, X.L. Li, and H.Y. Wang, “Fabrication of TiC particulate reinforced magnesium matrix composites,” Scripta Mater., 48, 713–717 (2003).
W. Yu, X. Wang, H. Zhao, et al., “Microstructure, mechanical properties and fracture mechanism of Ti2AlC reinforced AZ91D composites fabricated by stir casting,” J. Alloys Compd., 702, 199–208 (2017).
R.G. Munro, “Material properties of titanium diboride,” J. Res. Natl. Inst. Stand. Technol., 105, No. 5, 709–720 (2000).
Y. Wang, H.Y. Wang, Y.F. Yang, and Q.C. Jiang, “Solidification behavior of cast TiB2 particulate reinforced Mg composites,” Mater. Sci. Eng. A., 478, 9–15 (2008).
Y. Wang, H.Y. Wang, and K. Xiu, “Fabrication of TiB2 particulate reinforced magnesium matrix composites by two-step processing method,” Mater. Lett., 60, 1533–1537 (2006).
Z. Xiuqing, W. Haowei, and L. Lihua, “The mechanical properties of magnesium matrix composites reinforced with (TiB2+TiC) ceramic particulates,” Mater. Lett., 59, 2105–2109 (2005).
W.L.E. Wong, S. Karthik, and M. Gupta, “Development of high performance Mg–Al2O3 composites containing Al2O3 in submicron length scale using microwave assisted rapid sintering,” Mater. Sci. Technol., 21, No. 9, 1063–1070 (2005).
A.B. Spierings, M. Schneider, and R. Eggenberger, “Comparison of density measurement techniques for additive manufactured metallic parts,” Rapid Prototyping J., 17, No. 5, 380–386 (2011).
T.G. Feeman, “On the area of a parabolic sector,” Int. J. Math. Educ. Sci. Technol., 40, No. 8, 1118–1121 (2009).
Q.B. Nguyen, I. Quader, and M.L.S. Nai, “Enhancing hardness, CTE and compressive response of powder metallurgy magnesium reinforced with metastable Al90Y10 powder particles,” Powder Metall., 59, No. 3, 209–215 (2016).
H.Y. Wang, Q.C. Jiang, and Y. Wang, “Fabrication of TiB2 particulate reinforced magnesium matrix composites by powder metallurgy,” Mater. Lett., 58, 3509–3513 (2004).
M.K. Habibi, A.M.S. Hamouda, and M. Gupta, “Enhancing tensile and compressive strength of magnesium using ball milled Al+CNT reinforcement,” Compos. Sci. Technol., 72, 290–298 (2012).
M.K. Habibi, A.S. Hamouda, and M. Gupta, “Hybridizing boron carbide (B4C) particles with aluminum (Al) to enhance the mechanical response of magnesium based nanocomposites,” J. Alloys Compd., 550, 83–93 (2013).
C.S. Goha, J. Weia, L.C. Lee, and M. Gupta, “Simultaneous enhancement in strength and ductility by reinforcing magnesium with carbon nanotubes,” Mater. Sci. Eng. A., 423, 153–156 (2006).
S.V. Muley, S.P. Singh, and P. Sinha, “Microstructural evolution in ultrasonically processed in situ AZ91 matrix composites and their mechanical and wear behavior,” Mater. Des., 53, 475–481 (2014).
J.F. Archard, “Contact and rubbing of flat surfaces,” J. Appl. Phys., 24, 981–988 (1953).
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This work was supported by Karabuk University Coordinatorship of Research Projects (KBU-BAP No. 16/1-DR-077).
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Published in Poroshkova Metallurgiya, Vol. 57, Nos. 9–10 (523), pp. 84–93, 2018.
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Aydin, F., Sun, Y. & Emre Turan, M. The Effect of TiB2 Content on Wear and Mechanical Behavior of AZ91 Magnesium Matrix Composites Produced by Powder Metallurgy. Powder Metall Met Ceram 57, 564–572 (2019). https://doi.org/10.1007/s11106-019-00016-9
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DOI: https://doi.org/10.1007/s11106-019-00016-9