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Development of a Sample-Preparation Procedure for Quantitative Determination of Lead in Sugars by Inductively Coupled-Plasma—Atomic-Emission Spectrometry (ICP-AES)

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Pharmaceutical Chemistry Journal Aims and scope

A sample-preparation procedure for the determination of lead in sugars by inductively coupled-plasma—atomic-emission spectrometry was developed and validated using glucose and sucrose as examples. The characteristic detection wavelength and sugar decomposition conditions were selected. The suitability was assessed using a validation protocol for specificity, calibration curve linearity, limits of detection and quantitation, accuracy, precision, and intralaboratory precision.

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Authors and Affiliations

  1. Scientific Center for Expert Evaluation of Medicinal Products, Ministry of Health of the Russian Federation, 8/2 Petrovskii Blvd., 127051, Moscow, Russia

    Yu. V. Olefir, E. I. Sakanyan, L. A. Ladygina & V. M. Shchukin

Authors
  1. Yu. V. Olefir
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  2. E. I. Sakanyan
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  3. L. A. Ladygina
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  4. V. M. Shchukin
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Corresponding author

Correspondence to L. A. Ladygina.

Additional information

Translated from Khimiko-Farmatsevticheskii Zhurnal, Vol. 52, No. 2, pp. 59 – 62, February, 2018.

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Olefir, Y.V., Sakanyan, E.I., Ladygina, L.A. et al. Development of a Sample-Preparation Procedure for Quantitative Determination of Lead in Sugars by Inductively Coupled-Plasma—Atomic-Emission Spectrometry (ICP-AES). Pharm Chem J 52, 171–174 (2018). https://doi.org/10.1007/s11094-018-1785-6

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  • DOI: https://doi.org/10.1007/s11094-018-1785-6

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