Skip to main content
SpringerLink
Log in

Quality Control Methods for Group D Vitamins

  • Structure of Chemical Compounds, Methods of Analysis and Process Control
  • Published:
Pharmaceutical Chemistry Journal Aims and scope

Determination of the content of vitamin D is a rather difficult problem. In the present study, we have compared methods that are most widely used for determining group D vitains. In recent years, physical and chemical methods of analysis have found increasing use due to their simplicity, sensitivity, and information value. Various methods of quality control are currently used but the future in the analysis of calciferols undoubtedly belongs to HPLC. This method is capable of simultaneously solving all problems encountered in the analysis of group D vitamins.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Log in via an institution

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Institutional subscriptions

References

  1. G. A. Melent(eva, Pharmaceutical Chemistry of Certain Natural Substances with Strong Biological Action [in Russian], Izd. I. M. Sechenov Med. Inst., Moscow (1984), pp. 73–78.

    Google Scholar 

  2. M. D. Mashkovskii, Medicinal Agents [in Russian], Moscow (2002), Vol. 2, pp. 105–107.

    Google Scholar 

  3. Yu. M. Ostrovskii, Experimental Vitaminology [in Russian], Nauka i Tekhnika, Minsk (1979), pp. 18–53.

    Google Scholar 

  4. R. Strohecker and H. M. Henning, Vitamin-Bestimmungen, Verlag, Chemil. Weinheim (1963), pp. 264–290.

    Google Scholar 

  5. R. Adamsky and J. Sawicka, Herba Pol., 20, 57 (1974).

    Google Scholar 

  6. H. Galecka, Acta Pol. Pharm., 32, 529 (1975).

    Google Scholar 

  7. T. Kobayashi and A. Adachi, J. Nutr. Sci. Vitaminol., 19, 303 (1973).

    PubMed  CAS  Google Scholar 

  8. K. A. Tartivita, J. P. Sciarello, and B. C. Rudy, J. Pharm. Sci., 65, 1024 (1976).

    Article  PubMed  CAS  Google Scholar 

  9. T. Kobayashi and A. Adachi, J. Nutr. Sci. Vitaminol., 22, 41 (1976).

    PubMed  CAS  Google Scholar 

  10. D. Sklan, P. Budowski, and M. Katz, J. Anal. Biochem., 56, 606 (1973).

    Article  CAS  Google Scholar 

  11. W. W. Morris, J. B. Wilkie, S. W. Jones, et al., J. Anal. Chem., 34, 381 (1962).

    Article  CAS  Google Scholar 

  12. S. Görög and D. Durham, Quantitative Analysis of Steroids, Elsevier Scientific Pub. Co., New York, Amsterdam (1983).

    Google Scholar 

  13. V. V. Mishchenko, G. K. Shostakovskaya, N. A. Bogoslovskii, et al., Khim.-farm. Zh., 10, 136 (1960).

    Google Scholar 

  14. T. H. Campion and S. Dilley, Anal. Lett., 6, 139 (1973).

    CAS  Google Scholar 

  15. A. Gergely, G. Milch, Vargak, et al., Acta Pharm. Hung., 51, 168 (1981).

    PubMed  CAS  Google Scholar 

  16. F. S. Hom, S. A. Veresh, and W. R. Ebert, J. Assoc. Off. Anal. Chem., 60, 48 (1977).

    PubMed  CAS  Google Scholar 

  17. S. A. Gharbo and L. A. Gosser, Analyst, 99, 222 (1974).

    Article  PubMed  CAS  Google Scholar 

  18. S. A. Gharbo and L. A. Gosser, J. Pharm. Sci., 64, 1196 (1975).

    Article  PubMed  CAS  Google Scholar 

  19. S. M. Hassan, J. Anal. Chem., 293, 416 (1978).

    CAS  Google Scholar 

  20. USSR State Pharmacopoeia [in Russian], 10th Ed., Meditsina, Moscow (1968), p. 707.

  21. J. G. Kirchner, Techniques of Chemistry, Vol. 14: Thin-Layer Chromatography, 2nd Ed., Wiley-Interscience, New York (1978).

    Google Scholar 

  22. M. M. Amer, A. M. Wahbi, and S. M. Hassan, Analyst, 100, 238 (1975).

    Article  PubMed  CAS  Google Scholar 

  23. V. S. Kartashov, V. S. Shorshnev, A. N. Shchavlinskii, et al., Farmatsiya, No. 5, 24–26 (1992).

  24. V. S. Kartashov, Vopr. Biol. Med. Farm. Khim., No. 3, 44–46 (1998).

  25. K. Tsukida and K. Sakai, Int. J. Vitam. Nutr. Res., 42, 242 (1972).

    PubMed  CAS  Google Scholar 

  26. British Pharmacopeia, CD 2001, Vol. 2, System Simulation Ltd. (2001).

  27. A. I. Luttseva, L. G. Maslov, and V. I. Seredenko, Khim.-farm. Zh., 35(10), 41–45 (2001).

    Google Scholar 

  28. P. S. Chen, A. R. Terepka, and K. Lane, J. Anal. Biochem., 8, 34 (1964).

    Article  Google Scholar 

  29. V. G. Mairanovskii and G. I. Samokhvalov, Electrochemistry [in Russian], Vol. 1 (1965), p. 996.

    CAS  Google Scholar 

  30. V. G. Mairanovskii, N. A. Bogoslovskii, and G. I. Samokhvalov, Med. Promst. SSSR, 20, 39 (1966).

    CAS  Google Scholar 

  31. V. G. Mairanovskii and G. I. Samokhvalov, Zh. Vses. Khim. O'va im. D. I. Mendeleeva, 9, 358 (1964).

    CAS  Google Scholar 

  32. V. G. Mairanovskii and G. I. Samokhvalov, Zh. Anal. Khim., 21, 210 (1966).

    CAS  Google Scholar 

  33. D. Sklan and P. Budowski, J. Anal. Chem., 49, 200 (1973).

    Google Scholar 

  34. R. Mermet-Bouvier, J. Chromatogr., 59, 226 (1973).

    Article  Google Scholar 

  35. M. Sarsunova, V. Shvarts, and Ch. Mikhalets, Thin-Layer Chromatography in Pharmacy and Clinical Biochemistry [in Russian], Mir, Moscow (1980), Vol. 2, p. 610.

    Google Scholar 

  36. P. P. Nair and S. De Leor, Arch. Biochem. Biophys., 128, 663 (1968).

    Article  PubMed  CAS  Google Scholar 

  37. E. I. Kozlov, I. A. Solunina, M. L. Lyubareva, et al., Khim.-farm. Zh., 37(10), 50–53 (2003).

    Google Scholar 

  38. G. K. Budnikov and G. K. Ziyatdinova, Zh. Anal. Khim., 60(7), 678–691 (2005).

    Google Scholar 

  39. L. V. Denisova, V. N. Filimonov, L. N. Balyatinskaya, et al., Zh. Anal. Khim., 52(9), 967–969 (1997).

    Google Scholar 

  40. E. L. Styskin, L. B. Itsikson, and E. V. Braude, Practical HPLC [in Russian], Khimiya, Moscow (1986), pp. 253–256.

    Google Scholar 

  41. V. D. Shats and O. V. Sakhartova, HPLC: Theoretical Principles [in Russian], Zinante, Riga (1988), p. 390.

    Google Scholar 

  42. A. P. Arbatskii, G. N. Afon(shin, and V. M. Vostokov, Zh. Anal. Khim., 59(12), 1304–1307 (2004).

    Google Scholar 

  43. United States Pharmacopoeia, 24th Ed., Rockville (1999).

  44. D. F. Tompkins and R. Tscherne, J. Anal. Chem., 46, 1602 (1974).

    Article  Google Scholar 

  45. D. O. Edlund, F. A. Fillipini, and I. K. Datson, J. Assoc. Off. Anal. Chem., 57, 1089 (1974).

    PubMed  CAS  Google Scholar 

  46. J. Green, Biochem. J., 49, 34 (1961).

    Google Scholar 

  47. Pharmacopoeia of Japan VIII, Engl. Ed., Soc. Jpn. Pharmacopoeia (1973), Part 1, p. 153.

  48. USSR State Pharmacopoeia [in Russian], 11th Ed., Meditsina, Moscow (1987).

  49. A. I. Luttseva and L. G. Maslov, Khim.-farm. Zh., 35(10), 30–37 (2001).

    Google Scholar 

Download references

Author information

Authors and Affiliations

  1. Voronezh State University, Novonezh, Russia

    O. V. Rybakova, E. F. Safonova & A. I. Slivkin

Authors
  1. O. V. Rybakova
    View author publications

    You can also search for this author in PubMed Google Scholar

  2. E. F. Safonova
    View author publications

    You can also search for this author in PubMed Google Scholar

  3. A. I. Slivkin
    View author publications

    You can also search for this author in PubMed Google Scholar

Additional information

Translated from Khimiko-Farmatsevticheskii Zhurnal, Vol. 42, No. 7, pp. 38–44, July, 2008.

Rights and permissions

Reprints and permissions

About this article

Cite this article

Rybakova, O.V., Safonova, E.F. & Slivkin, A.I. Quality Control Methods for Group D Vitamins. Pharm Chem J 42, 419–425 (2008). https://doi.org/10.1007/s11094-008-0140-8

Download citation

  • Received:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s11094-008-0140-8

Search

Navigation