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Synthesis of nanorods FePO4 via a facile route

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Abstract

Iron phosphate nanorods were synthesized via a novel facile route. The structure, composition, and morphology of the prepared material were characterized by X-ray diffraction (XRD) and transmission electron microscope (TEM), respectively. The diffraction lines were indexed to the hexagonal structure. The diameter of these nanorods is about in the range of 20–30 nm and the length 50–100 nm. The preferential growth direction of the prepared material was the [100]. The reaction mechanism for the synthesis of FePO4 nanorods was also primarily discussed. Compared to the bulky and the irregular nanoparticles, the nanometer ones will be more fascinating for application in many areas.

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References

  • Balmer P, Frederiksen OF (1975) A pilot plant scale evaluation of potential precipitants in the secondary precipitation process. Water Res 9:721–725

    Article  CAS  Google Scholar 

  • Beale AM, Sankar G (2002) Following the structural changes in iron phosphate catalysts by in situ combined XRD/QuEXAFS technique. J Mater Chem 12:3064–3072

    Article  CAS  Google Scholar 

  • Boras CA, Romagnoli R, Lezna RO (2000) In-situ spectroelectrochemistry (UV–visible and infrared) of anodic films on iron in neutral phosphate solutions. Electrochim Acta 45:1717–1725

    Article  Google Scholar 

  • Cui W, Liu H, Wang C, Xia Y (2008) Highly ordered three-dimensional macroporous FePO4 as cathode materials for lithium-ion batteries. Electrochem Commun 10:1587–1589

    Article  CAS  Google Scholar 

  • Du N, Zhang H, Ma X, Li DS, Yang D (2009) Controllable chemical reaction synthesis of Tb(OH)3 nanorods and their photoluminescence property. Mater Lett 63:1180–1182

    Article  CAS  Google Scholar 

  • Fuhrer MS, Nygard J, Shih L, Forero M, Yoon YG, Mazzoni MSC et al (2000) Crossed nanotube junctions. Science 288:494–497

    Article  CAS  PubMed  ADS  Google Scholar 

  • Kandori K, Kuwae T, Ishikawa T (2006) Control on size and adsorptive properties of spherical ferric phosphate particles. J Colloid Interface Sci 300:225–231

    Article  CAS  PubMed  Google Scholar 

  • Kickuth R, Tubail K (1976) Defektverbindung und fremdionen-dotierung bei der ausfällung von eisen(II)- und eisen(III)-phosphaten. Geoderma 16:219–235

    Article  CAS  Google Scholar 

  • Okada S, Yamamoto T, Okazaki Y, Yamaki JI, Tokunaga M, Nishida T (2005) Cathode properties of amorphous and crystalline FePO4. J Power Sources 146:570–574

    Article  CAS  Google Scholar 

  • Sides CR, Croce F, Young VY, Martin CR, Scrosati B (2005) A high-rate, nanocomposite LiFePO4/carbon cathode. Electrochem Solid-State Lett 8:A484–A487

    Article  CAS  Google Scholar 

  • Wang L, Liang GC, Ou XQ, Zhi XK, Zhang JP, Cui JY (2009) Effect of synthesis temperature on the properties of LiFePO4/C composites prepared by carbothermal reduction. J Power Sources 189:423–428

    Article  CAS  Google Scholar 

  • Wilhelmy RB, Matijevic E (1987) Preparation and growth kinetics of monodispersed ferric phosphate hydrosols. J Colloids Surf 22:111–131

    Article  CAS  Google Scholar 

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Correspondence to Haowen Liu.

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Liu, H. Synthesis of nanorods FePO4 via a facile route. J Nanopart Res 12, 2003–2006 (2010). https://doi.org/10.1007/s11051-010-9891-8

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  • DOI: https://doi.org/10.1007/s11051-010-9891-8

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