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Journal of Nanoparticle Research

, Volume 6, Issue 4, pp 369–376 | Cite as

Synthesis and characterization of S-Au interaction in gold nanoparticle bound polymeric beads

  • C.S.S.R. Kumar
  • M. Aghasyan
  • H. Modrow
  • E. Doomes
  • C. Henk
  • J. Hormes
Article

Abstract

A detailed X-ray Absorption Spectroscopic examination of S-Au interaction in gold nanoparticle bound to Polystyrene-Divinyl Benzene (PS-DVB) micro beads was carried out. Gold nanoparticles were bound to the surface of the commercially available PS-DVB beads using a simple one step procedure. Influence of polystyrene backbone on the electronic structure of the gold nanoparticles was observed through X-ray Absorption Near Edge Structure (XANES) spectra of Au at L III edge. An additional structure in the white line of the S K-edge XANES spectrum confirmed the presence of S-Au bonding. Transmission Electron Microscopy (TEM) studies coupled with Selected Area Electron Diffraction Pattern and X-ray Diffraction studies revealed the morphology of the Au nanoparticles bound to the micro beads.

nanoparticles composites multifunctional synthesis X-ray measurements 

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Copyright information

© Kluwer Academic Publishers 2004

Authors and Affiliations

  • C.S.S.R. Kumar
    • 1
  • M. Aghasyan
    • 1
  • H. Modrow
    • 2
  • E. Doomes
    • 1
  • C. Henk
    • 3
  • J. Hormes
    • 1
  1. 1.Center for Advanced Microstructures and DevicesLouisiana State UniversityUSA
  2. 2.Physikalisches InstitutUniversity of BonnGermany
  3. 3.The Socolofsky Microscopy Center, Department of Biological SciencesLouisiana State UniversityUSA

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