Skip to main content
Log in

Analysis of the Anomalous Effect of Heat Treatment on the Structure and Phase Transformations in High-Chromium Tool Steel

  • FUNCTIONAL STEELS AND ALLOYS
  • Published:
Metal Science and Heat Treatment Aims and scope

The effect of various heat treatments with heating to 1030 – 1250°C on the structure and microhardness of high-chromium tool steel 160Kh12MF is studied. The chemical composition is determined, the microhardness is measured, and the microstructure of the steel is analyzed after quenching, normalizing and annealing. It is shown that the customary heat treatments (quenching from the austenitic range for hardening and annealing for softening) may have an effect opposite to the expected one. This phenomenon may be caused by phase transformations of the austenite during its cooling due to precipitation of carbides. It is established that super-cooled austenite is resistant to martensitic transformation, deformation, and cold treatment after rapid cooling. Aging of the martensite and its decomposition into martensite and carbides with growth of the microhardness are observed at the temperatures no lower than 750°C.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Fig. 1.
Fig. 2.
Fig. 3.
Fig. 4.

Similar content being viewed by others

Notes

  1. The x-ray phase analysis was performed by D. A. Kozlov (MISiS).

References

  1. Yu. A. Geller, Tool Steels [in Russian], Metallurgiya, Moscow (1975), 584 p.

  2. A. P. Gulyaev, High-Speed Steels [in Russian], Mashinostroenie, Moscow (1975), 272 p.

  3. V. P. Shveikin, V. P. Kuznetsov, I. S. Kamantsev, et al., “Effect of heat treatment on the structure and mechanical properties of tool steel 1.6% C – 12% Cr – 0.8% Mo – 0.9% V,” Metalloved. Term. Obrab. Met., No. 8(806), 21 – 26 (2022).

  4. Gong Wei, Jiang Zhouhua, Zhang Lixian, et al., “Influence of Mg addition on inclusions and mechanical properties of Cr12Mo1V1 steel under high pressure,” Mater. Sci. Eng. A, 791, 139410 (2020).

    Article  Google Scholar 

  5. D. Alireza, D. Ariya, S. Alikhusein, and A. Mahdi, “Effect of double austenitization on the microstructure and hardness of steel 1.4% C – 11.7% Cr,” Metalloved. Term. Obrab. Met., No. 6(804), 16 – 19 (2022).

  6. A. P. Gulyaev, Metal Science [in Russian], Metallurgiya, Moscow (1976), 544 p.

  7. GOST 5950–73. Bars and Strips from Tool Alloy Steel [in Russian].

  8. V. S. Kovalenko, Metallographic Reagents [in Russian], Metallurgiya, Moscow (1981), 120 p.

  9. M. Yu. Belomytsev, E. I. Kuz’ko, and P. A. Prokof’ev, “Application of magnetometric technique to investigation of ferriticmartensitic steels,” Zavod. Lab., Diagn. Mater., 83(11), 41 – 46 (2017).

  10. C. R. Jonson and S. J. Rosenberg, “Constitution diagram for 16% Cr – 2% Ni stainless steel,” Trans. ASM, 55, 277 – 286 (1962).

    Google Scholar 

  11. M. Yu. Belomytsev, E. I. Kuz’ko, P. A. Prokof’ev, and T. D. Sulyaev, “Determination of critical temperatures and structural state of 13% chromium steel by magnetometric method,” Izv. Vysh. Uchebn. Zaved., Chern. Metall., 60(9), 732 – 738 (2017).

  12. M. Yu. Belomytsev, S. M. Obraztsov, and A. V. Molyarov, “Effect of ferrite content on the heat resistance of 12% chromium steels with ferrite-martensite structure,” Metallurg, No. 9, 46 – 51 (2017).

Download references

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to M. Yu. Belomytsev.

Additional information

Translated from Metallovedenie i Termicheskaya Obrabotka Metallov, No. 7, pp. 17 – 21, July, 2023.

Rights and permissions

Springer Nature or its licensor (e.g. a society or other partner) holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law.

Reprints and permissions

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Belomytsev, M.Y. Analysis of the Anomalous Effect of Heat Treatment on the Structure and Phase Transformations in High-Chromium Tool Steel. Met Sci Heat Treat 65, 410–414 (2023). https://doi.org/10.1007/s11041-023-00948-5

Download citation

  • Received:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s11041-023-00948-5

Keywords

Navigation